Preparation method of composite deodorant containing natural plant extracts
A technology of plant extracts and natural plants, which is applied in the field of compound deodorant preparation, can solve the problems of destroying novelty and creativity, inapplicability, and the spray has no fragrance, etc., and achieves good product stability, reduced dosage, and reliable highly operable effect
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Embodiment 1
[0028] Step A: Rough extraction, take 3kg yucca, 2kg rosemary, 3kg magnolia officinalis, 2kg amomum, 3kg wood incense, 1kg green bark, 4kg mint, 3kg tea leaves, crush the plant materials, and pass the powder through a 50-mesh sieve , respectively placed in 420kg, 320kg, 250kg aqueous solution at a constant temperature of 70°C and stirred for 2 hours, after extraction for 3 times, suction filtration was performed, and the filtrate was collected to obtain a crude extract;
[0029] Step B: ultrafiltration to remove impurities, the crude extract obtained in step A is subjected to an ultrafiltration operation, and the ultrafiltration membrane with a molecular weight cut-off of 30KDa is subjected to ultrafiltration to obtain a filtrate;
[0030] Step C: Adsorption and analysis of organic acids, the filtrate obtained in step B is subjected to an anionic macroporous resin adsorption operation, and the adsorption operation is carried out on a 717 type macroporous resin at a speed of 48L...
Embodiment 2
[0036] Step A: Rough extraction, take 2kg yucca, 3kg rosemary, 2kg magnolia bark, 2kg amomum, 3kg woody, 2kg green bark, 3kg mint, 3kg tea leaves, crush the plant materials, and pass the powder through a 60-mesh sieve , respectively placed in 440kg, 360kg, 300kg aqueous solution at a constant temperature of 80°C and stirred for 2 hours, after extraction for 3 times, suction filtration was performed, and the filtrate was collected to obtain a crude extract;
[0037] Step B: ultrafiltration to remove impurities, the crude extract obtained in step A is subjected to an ultrafiltration operation, and the ultrafiltration membrane with a molecular weight cut-off of 35KDa is subjected to ultrafiltration to obtain a filtrate;
[0038] Step C: Adsorption and analysis of organic acids, the filtrate obtained in step B is subjected to an anionic macroporous resin adsorption operation, and the D201 type macroporous resin is adsorbed at a speed of 45L / h. The D201 type resin has a volume of 45...
Embodiment 3
[0044] Step A: Rough extraction, take 2kg yucca, 2kg rosemary, 1kg magnolia officinalis, 2kg amomum, 3kg wood incense, 3kg green bark, 3kg mint, 4kg tea leaves, crush the plant materials, and pass the powder through a 60-mesh sieve , respectively placed in 420kg, 380kg, and 300kg of aqueous solution at a constant temperature of 85°C for 1.5 hours of stirring and extraction, after extraction for 3 times, suction filtration was performed, and the filtrate was collected to obtain a crude extract;
[0045] Step B: ultrafiltration to remove impurities, the crude extract obtained in step A is subjected to an ultrafiltration operation, and the ultrafiltration membrane with a relative molecular weight of 40KDa is subjected to ultrafiltration to obtain a filtrate;
[0046] Step C: Adsorption and analysis of organic acids, the filtrate obtained in step B is subjected to an anionic macroporous resin adsorption operation, and the D201 type macroporous resin is used for adsorption operation...
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