Bottom sizing agent for addition type liquid silicone rubber and preparation method of bottom sizing agent
A liquid silicone rubber, primer technology, applied in the direction of adhesives, adhesive additives, non-polymer adhesive additives, etc., can solve the problems of poor adhesion, can not meet the effective adhesion of silicone rubber, etc. Effect
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Embodiment 1-5
[0026] Example 1-5: Preparation of a primer for addition-type liquid silicone rubber.
[0027] Table 1. Composition and dosage of primer for addition-type liquid silicone rubber
[0028]
[0029] Prepare primer according to formula and consumption in table 1, concrete operation process is as follows:
[0030] 1) Preparation of raw materials:
[0031] Weigh silicone-modified polyurethane, siloxane containing active groups, silicone resin, silane coupling agent, rare metal catalyst and petroleum ether, and divide the petroleum ether into two equally;
[0032] 2) Preparation of component A:
[0033] Under the condition of mechanical stirring, add silicone-modified polyurethane to one part of petroleum ether and stir evenly, then add siloxane containing active groups and stir evenly to obtain component A;
[0034] 2) Preparation of component B:
[0035] Under the condition of mechanical stirring, add the silicone resin to another part of petroleum ether and stir evenly, the...
experiment example
[0038] Experimental example: performance test of primer for addition-type liquid silicone rubber.
[0039] After diluting the primer prepared in Examples 1-5 to a spray viscosity of 7.5 to 8.5S, spray them on PC / ABS substrates respectively, and perform injection molding of addition-type silicone rubber on them after baking. No air bubbles were observed in the silicone rubber during this process.
[0040] After the injection molding is completed, cool the sample and measure the tensile strength (the maximum tensile stress of the sample stretched to the fracture process), the elongation at break (the elongation of the sample when it is broken), the tear strength ( Divide the force required to tear the sample by the thickness of the sample) and 90° peel strength (the sample is prepared by bonding a strip of rubber to a hard plate, and peeled at a peeling angle of 90° to measure the peeling of the rubber and the hard plate The required force, the maximum peeling force that the sa...
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