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High-concentration non-ionic cellulose ether suspension dispersion liquid and preparation method thereof

A cellulose ether and non-ionic technology, which is applied in the preparation of high-concentration non-ionic cellulose ether suspension and dispersion, and in the field of high-concentration non-ionic cellulose ether suspension and dispersion, can solve low production efficiency and insufficient transportation capacity. Consumption, water (excessive mixing of medium, etc.) to achieve the effect of reducing transportation costs, increasing the difficulty of use, and reducing the efficiency of use

Active Publication Date: 2017-06-27
GUANGDONG LADOS NEW MATERIAL CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0010] ①. In the process of directly using cellulose ether solution to produce end products, when the concentration of the solution is low (0% to 1.5%), if the amount of cellulose ether (solute) is increased, the amount of water (medium) will be increased at the same time. ), which easily leads to the problem of excessive water (medium) mixing;
As a result, the production efficiency is low and the energy consumption is high;
[0012] ③. In the production process of some composite additives that require the use of cellulose ether solution, due to the limitation of the viscosity of the cellulose ether solution, it is difficult to increase the content of cellulose ether in the composite additive
When it is necessary to transport the composite additive to the end user's factory, most of the transported medium (water or other dispersion medium) is actually used, resulting in a serious waste of transportation capacity, resulting in an increase in the use cost of the composite additive The problem

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0034] A method for preparing a high-concentration nonionic cellulose ether suspension and dispersion liquid, comprising the preparation of a highly alkaline aqueous solution and the suspension dispersion liquid, calculated in parts by mass, the preparation process is as follows:

[0035] (1) Preparation of highly alkaline aqueous solution: under normal temperature and pressure, 10 parts of sodium hydroxide and 90 parts of water are made into highly alkaline aqueous solution. Under standard test environment, the pH value of the highly alkaline aqueous solution is measured to be 13.7 .

[0036] (2) Preparation of suspension dispersion: at normal temperature and pressure, mix 89.7 parts of the above-mentioned highly alkaline aqueous solution, 10 parts of hydroxypropyl methylcellulose ether with a viscosity of 100000mPa.s, and 0.3 part of xanthan gum evenly A high-concentration non-ionic cellulose ether suspension dispersion is obtained.

[0037] With reference to GB / T10247-2008...

Embodiment 2

[0039] A method for preparing a high-concentration nonionic cellulose ether suspension and dispersion liquid, comprising the preparation of a highly alkaline aqueous solution and the suspension dispersion liquid, calculated in parts by mass, the preparation process is as follows:

[0040] (1) Preparation of highly alkaline aqueous solution: under normal temperature and pressure, 10 parts of potassium hydroxide and 90 parts of water are made into highly alkaline aqueous solution. Under standard test environment, the pH value of the highly alkaline aqueous solution is measured to be 13.8 .

[0041] (2) Preparation of suspension dispersion: at normal temperature and pressure, mix 89.7 parts of the above-mentioned highly alkaline aqueous solution, 10 parts of hydroxypropyl methylcellulose ether with a viscosity of 100000mPa.s, and 0.3 part of xanthan gum evenly A high-concentration non-ionic cellulose ether suspension dispersion is obtained.

[0042]With reference to GB / T10247-20...

Embodiment 3

[0044] A method for preparing a high-concentration nonionic cellulose ether suspension and dispersion liquid, comprising the preparation of a highly alkaline aqueous solution and the suspension dispersion liquid, calculated in parts by mass, the preparation process is as follows:

[0045] (1) Preparation of highly alkaline aqueous solution: under normal temperature and pressure, 20 parts of sodium carbonate and 80 parts of water were made into highly alkaline aqueous solution. Under standard test conditions, the pH value of the highly alkaline aqueous solution was measured to be 11.3.

[0046] (2) Suspension dispersion: at normal temperature and pressure, mix 89.7 parts of the above-mentioned highly alkaline aqueous solution, 10 parts of hydroxypropyl methylcellulose ether with a viscosity of 100000mPa.s, and 0.3 part of xanthan gum to obtain High concentration non-ionic cellulose ether suspension dispersion.

[0047] With reference to GB / T10247-2008, under the standard test e...

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Abstract

The invention relates to a high-concentration non-ionic cellulose ether suspension dispersion liquid and a preparation method thereof. The dispersion liquid contains non-ionic cellulose ether and a high-alkalinity water solution, wherein the non-ionic cellulose ether is dispersed in the high-alkalinity water solution in a suspending mode instead of a dissolution mode. Compared with the prior art, a terminal product is produced by directly using the cellulose ether. When the mixing amount of the cellulose ether is required to be increased, the water consumption is not required to be passively and simultaneously increased. In addition, when a liquid compound additive is produced by using the cellulose ether, the water demand of the compound additive can be remarkably decreased, and the transportation cost of the compound additive is reduced. The prepared dispersion liquid is moderate in viscosity, has good liquidity, can be pumped, can also uniformly disperse a cellulose ether solution and is dispersed after long-time stable storage, and the thickening and water retention performance of the liquid is also same as the property of direct dissolution in water.

Description

technical field [0001] The invention relates to the technical field of cellulose ether suspension dispersion liquid, in particular to a high-concentration nonionic cellulose ether suspension dispersion liquid, and also relates to a preparation method of a high-concentration nonionic cellulose ether suspension dispersion liquid. Background technique [0002] Cellulose ethers, especially water-soluble non-ionic cellulose ethers, such as MC, HEC, HEMC, HPC, HPMC, etc., have a wide range of applications as thickening and water-retaining additives in food, medicine, chemical, petroleum, building materials and other industries. It is compared to "industrial monosodium glutamate". Cellulose ether can be used alone or compounded with other functional materials to become a composite additive with multiple properties. [0003] The initial form of cellulose ether products is powder, but its thickening and water-retaining performance in the end product needs to be in the form of an aqu...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08J3/03C08L1/28
CPCC08J3/03C08J2301/28
Inventor 蒋金明陈均侨
Owner GUANGDONG LADOS NEW MATERIAL CO LTD
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