Inorganic powder surface treatment method, chemical plating activating agent, polymer product and surface selective metalizing method of polymer product
A surface treatment agent and surface treatment technology, applied in the direction of liquid chemical plating, metal material coating process, coating, etc., can solve the problem of affecting the compatibility of SBID powder and non-metallic materials, and affecting the impact strength of polymer products , easy to introduce impurity ions and other problems, to achieve the effect of eliminating impurity ions, improving impact strength and avoiding agglomeration
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preparation example 1-9
[0096] It is used to illustrate the surface treatment method of the inorganic powder of the present invention.
preparation example 1
[0098] 2.5kg of boric acid (in B 2 o 3 1.4kg) and 200L absolute ethanol are placed in the evaporator 10 for dissolution; Cu 3 (PO 4 ) 2 Powder (purchased from Xilong Chemical Co., Ltd., green) takes 50 kg and pours it into the tank body 11 of the evaporation tank 10, raises the tank body 11 to combine with the sealing cover 13 to form a sealed evaporation tank 10, and starts stirring 20 (stirring speed is 150r / min), ultrasonic oscillator (oscillating frequency is 28KHZ, power 1000W), condenser 31, so that the mixed system in the evaporation tank 10 is subjected to the effect of mechanical stirring and ultrasonic oscillation at the same time, and simultaneously sends water to the evaporation tank 10 The hot water of 95°C is introduced into the thermal insulation jacket to make the temperature in the evaporation tank 10 reach the range of 83-93°C, and the anhydrous ethanol in the evaporation tank 10 is heated and evaporated, condensed in the condenser 31 and recovered to the ...
preparation example 2
[0100] The surface treatment method of inorganic powder: with reference to Example 1, the difference is that
[0101] (1) 13.32kg of boric acid (in B 2 o 3 7.5kg) and 200L absolute ethanol are placed in the evaporator 10 for dissolution; Cu 3 (PO 4 ) 2 Powder (purchased from Xilong Chemical Co., Ltd., green) gets 50kg and pours it into the tank body 11 of the evaporation tank 10;
[0102] (2) The stirring speed of the agitator 20 is 200r / min, the oscillation frequency of the ultrasonic oscillator is 28kHz, and the power is 1000W, and the hot water of 95°C is passed into the thermal insulation jacket of the evaporator 10 to make the temperature in the evaporator 10 Reach the range of 83-93°C;
[0103] The resulting surface-treated (boron-coated) Cu 3 (PO 4 ) 2 Powder (particle size D 50 4.2 μm, D 90 9.5 μm), this product is recorded as P2.
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