Method for preparing LiNi<1/3>Co<1/3>Mn<1/3>O<2> ternary cathode material
A positive electrode material and concentration technology, applied in the field of electrochemical power supply, can solve the problems of increasing the difficulty and cost of ternary material production, and achieve the effects of easy production operation, simple synthesis process, and reduced production cost
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[0015] Example 1
[0016] 1.7515 g NiSO 4 ·6H 2 O, 1.8731 g CoSO 4 ·7H 2 O, 1.1266 g MnSO 4 ·H 2 O was sequentially dissolved in 40 mL of deionized water at a molar ratio of 1:1:1, stirred for 30 minutes to completely dissolve, and 1.6109 g of NaOH was added to 80 mL of deionized water. Then, add the mixed solution containing nickel ions, cobalt ions, and manganese ions dropwise to the NaOH solution, and add 15 mL with a concentration of 3.35 mol L -1 Ammonia water as a complexing agent, with 400 r min -1 Stir at a rotating speed of 50-55°C for 12 hours to obtain a black suspension. After standing for 6-8 hours, it is filtered, washed several times, and dried in an oven at 90°C for 9 hours to obtain a precursor. Add 0.7265 g Li to the precursor (1.8 g) 2 CO 3 , After ball milling with absolute ethanol for 6 hours, dry and sinter at 450 ℃ for 5 hours, then sinter at 900 ℃ for 12 hours, cool and sieving to obtain LiNi 1 / 3 Co 1 / 3 Mn 1 / 3 O 2 Ternary cathode material. LiNi 1 / 3 Co 1 / 3...
Example Embodiment
[0017] Example 2
[0018] 1.7515 g NiSO 4 ·6H 2 O, 1.8731 g CoSO 4 ·7H 2 O, 1.1266 g MnSO 4 ·H 2 O was sequentially dissolved in 80 mL of deionized water at a molar ratio of 1:1:1, stirred for 30 minutes to completely dissolve, and 1.6109 g of NaOH was added to 80 mL of deionized water. Then, slowly drop the mixed solution containing nickel ions, cobalt ions, and manganese ions into the NaOH solution, and add 15 mL with a concentration of 3.35 mol L -1 As the complexing agent, the ammonia water was stirred at a speed of 400 r min-1, and the reaction was kept at 50-55℃ for 12 hours to obtain a black suspension. After standing for 6-8 hours, it was filtered and washed several times. Dry in an oven at ℃ for 9 hours to obtain a precursor. Add 0.7265 g Li to the precursor (1.8 g) 2 CO 3 , After 6 hours of ball milling with absolute ethanol as the medium, dry, sinter at 450 ℃ for 5 hours, then sinter at 900 ℃ for 12 hours, cool and sieving to obtain LiNi 1 / 3 Co 1 / 3 Mn 1 / 3 O 2 Ternary c...
Example Embodiment
[0019] Example 3
[0020] 1.7515 g NiSO 4 ·6H 2 O, 1.8731 g CoSO 4 ·7H 2 O, 1.1266 g MnSO 4 ·H 2 O was dissolved in 200 mL of deionized water with a molar ratio of 1:1:1, and stirred for 30 minutes to completely dissolve it. At the same time, 1.6109 g of NaOH was added to 80 mL of deionized water. Then, slowly drop the mixed solution containing nickel ions, cobalt ions, and manganese ions into the NaOH solution, and add 15 mL with a concentration of 3.35 mol L -1 As the complexing agent, the ammonia water was stirred at a speed of 400 r min-1, and the reaction was kept at 50-55 ℃ for 12 hours to obtain a black suspension. After standing for 6-8 hours, it was filtered and washed several times. Dry in an oven at ℃ for 9 hours to obtain a precursor. Add 0.7265 g Li to the precursor (1.8 g) 2 CO 3 , After ball milling with absolute ethanol for 6 hours, dry, sinter at 450 ℃ for 5 hours, then sinter at 900 ℃ for 12 hours, cool and sieving to obtain LiNi 1 / 3 Co 1 / 3 Mn 1 / 3 O 2 Ternary ca...
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