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High-stability emulsion adhesive

A high-stability, adhesive technology, applied in the direction of adhesive types, ester copolymer adhesives, etc., can solve the problems of poor stability, precipitation, and reduced adhesive performance of emulsion adhesives, and achieves easy settling, The effect of prolonged storage time and good stability

Pending Publication Date: 2017-11-24
FOSHAN CITY YONGHENGDA NEW MATERIAL TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] However, artificially synthesized emulsion adhesives have poor stability, and if they are placed for a long time, precipitation will occur, resulting in a greatly reduced adhesive performance; however, if the adhesive just produced is transported to the user immediately, then Will result in greatly increased adhesive costs

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] High-stability emulsion binder, its raw material components include by mass parts:

[0025]

[0026] Its production method is:

[0027] Accurately weigh butyl acrylate, vinyl acetate, acrylonitrile, methacrylic acid, hydroxyethyl acrylate, azobisisobutyronitrile, p-octylphenol polyoxyethylene ether, sodium hydroxide and deionized water;

[0028] Add half the amount of deionized water, p-octylphenol polyoxyethylene ether, butyl acrylate, vinyl acetate, acrylonitrile, methacrylic acid, and hydroxyethyl acrylate into the reactor, and stir at a speed of 260r / min , stirred for 40 minutes to obtain a pre-emulsified mixture, set aside;

[0029] The pre-emulsified mixture is equally divided into 6 batches, and azobisisobutyronitrile is also equally divided into 6 batches;

[0030] In another reaction kettle, add the other half of the deionized water and half of the sodium hydroxide at the same time, add the first batch of pre-emulsified mixture to the reaction kettle, the ...

Embodiment 2

[0038] High-stability emulsion binder, its raw material components include by mass parts:

[0039]

[0040] Its production method is:

[0041] Accurately weigh the components of butyl acrylate, vinyl acetate, acrylonitrile, methacrylic acid, hydroxyethyl acrylate, benzoyl peroxide, emulsified silicone oil, ammonia water and deionized water;

[0042] Add half the amount of deionized water, emulsified silicone oil, butyl acrylate, vinyl acetate, acrylonitrile, methacrylic acid, and hydroxyethyl acrylate into the reaction kettle, and stir for 60 minutes at a stirring speed of 200r / min to obtain the prepared emulsified mixture, set aside;

[0043] Divide the pre-emulsified mixture into 6 equal parts, and divide the benzoyl peroxide into 6 equal parts;

[0044] In another reactor, add the other half of deionized water and half of the ammonia water at the same time, add the first batch of pre-emulsified mixture into the reactor, the stirring speed is 450r / min, and heat the reac...

Embodiment 3

[0052] High-stability emulsion binder, its raw material components include by mass parts:

[0053]

[0054] Its production method is:

[0055] Accurately weigh butyl acrylate, vinyl acetate, acrylonitrile, methacrylic acid, hydroxyethyl acrylate, cyclohexanone peroxide, emulsified silicone oil, sodium bicarbonate and deionized water;

[0056] Add deionized water, emulsified silicone oil, butyl acrylate, vinyl acetate, acrylonitrile, methacrylic acid, and hydroxyethyl acrylate into the reaction kettle, and stir for 45 minutes at a stirring speed of 245 r / min to obtain the prepared emulsified mixture, set aside;

[0057] The pre-emulsified mixture is equally divided into 6 batches, and cyclohexanone peroxide is also equally divided into 6 batches;

[0058] In another reaction kettle, add the other half of the deionized water and half of the sodium bicarbonate at the same time, add the first batch of pre-emulsified mixture to the reaction kettle, the stirring speed is 340r / m...

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Abstract

The invention discloses a high-stability emulsion adhesive, which is prepared from the following components in parts by mass: 34-42 parts of butyl acrylate, 16-24 parts of vinyl acetate, 24-48 parts of acrylonitrile, 11-20 parts of methacrylic acid, 40-48 parts of hydroxyethyl acrylate, 1-3 parts of an initiator, 2-6 parts of an emulsifier, 4-9 parts of a pH modifier and 150-180 parts of water. The invention provides the high-stability emulsion adhesive. The emulsion adhesive has good stability and dispersibility, and is not easy to settle, and the storage time of the emulsion adhesive can be greatly prolonged.

Description

technical field [0001] The invention relates to the technical field of adhesives, in particular to a high-stability emulsion adhesive. Background technique [0002] Adhesive, also known as adhesive, referred to as glue (bonding agent, adhesive), is a non-metallic medium material that makes an object closely connected with another object. The adhesive only occupies a very thin layer of volume between the two adherend surfaces, but after the adhesive is used to complete the bonding construction, the obtained adhesive joints can meet various requirements of actual needs in terms of mechanical properties and physical and chemical properties. It can effectively bond materials together. [0003] In recent decades, humans have invented "synthetic binders" made of polymer chemistry and petrochemicals, which have a wide variety and strong adhesion. Production has also grown by leaps and bounds. [0004] However, artificially synthesized emulsion adhesives have poor stability, and ...

Claims

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Application Information

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IPC IPC(8): C09J133/14C08F220/28C08F220/18C08F218/08C08F220/06C08F2/30C08F220/46
CPCC08F2/30C08F220/28C08F220/281C09J133/14C08F220/1804C08F218/08C08F220/46C08F220/06
Inventor 陈见玲
Owner FOSHAN CITY YONGHENGDA NEW MATERIAL TECH CO LTD