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Aerogel plastic film and preparation method thereof

A plastic film and aerogel technology, applied in the field of aerogel plastic film and its preparation, can solve the problems of complex process, high technical and capital requirements, difficulty in large-scale production, etc. The effect of omitting chemical equipment

Inactive Publication Date: 2017-12-08
湖北硅金凝节能减排科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The disadvantage of this method is that the process is complex, and special equipment such as reactors and supercritical reactors are required to complete a series of reactions from airgel precursors to aerogels, requiring a large enough production space, technology and capital requirements High barriers to entry and difficulty in large-scale production
Due to the complexity of the gelation process, there are many shortcomings in the in-situ composite between airgel and other reinforcing materials. It is necessary to develop a new preparation method for airgel composites.

Method used

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  • Aerogel plastic film and preparation method thereof

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Effect test

preparation example Construction

[0023] Such as figure 1 Shown, a kind of preparation method of airgel plastic film, it comprises the steps:

[0024] S1. Preparation of airgel powder slurry: fully mix airgel powder, interface agent, functional additive and water to obtain airgel powder slurry;

[0025] S2. Mixture preparation: put the airgel powder slurry and the resin material into the mixing equipment and mix evenly to obtain the mixture;

[0026] S3. Film forming: the mixture is made into a film through a forming process, which is the airgel plastic film.

Embodiment 1

[0028] An airgel plastic film, which is prepared by the following method:

[0029] S1. Preparation of airgel powder slurry: fully mix 50g of airgel powder with a particle size of 5-20μm, 10g of silane coupling agent, 10g of functional additive zinc oxide powder and 930g of ethanol to obtain airgel Powder slurry;

[0030] S2. Mixture preparation: 1000g of airgel powder slurry, 500g of polyacrylic resin powder and 500g of water-based polyurethane resin are put into a tank mixer and mixed evenly to obtain a mixture;

[0031] S3. Forming the film: spraying the mixture onto the hard and smooth surface of the template, drying to form a film, and obtaining the airgel plastic film. Its thickness is about 0.1-0.5mm, and the content of airgel powder in it is about 5wt%.

[0032] According to the performance test, the thermal conductivity of the above-mentioned airgel plastic film at room temperature is about 0.04W / (m·k).

Embodiment 2

[0034] An airgel plastic film, which is prepared by the following method:

[0035] S1. Preparation of airgel powder slurry: fully mix 150g of airgel powder with a particle size of 20-40μm, 20g of silane coupling agent, 5g of functional additive zinc oxide powder and 875g of ethanol to obtain airgel Powder slurry;

[0036] S2. Mixture preparation: put 1000g of airgel powder slurry and 1500g of polyvinyl alcohol resin powder into a trough mixer and mix evenly to obtain a mixture;

[0037] S3. Forming the film: roll coating the mixed material on the hard and smooth surface of the template, and drying it to form a film to obtain the airgel plastic film. Its thickness is about 1-2mm, and the content of airgel powder in it is about 10wt%.

[0038] According to the performance test, the normal temperature thermal conductivity of the above-mentioned airgel plastic film is about 0.035W / (m·k).

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Abstract

The invention relates to a method for preparing an aerogel plastic film. The method comprises the following steps: S1, preparing aerogel powder slurry, namely sufficiently mixing aerogel powder, an interfacial agent, a functional additive and a solvent to obtain the aerogel powder slurry; S2, preparing a mixture, namely uniformly mixing the aerogel powder slurry and a resin material into mixing equipment to obtain the mixture; and S3, molding the film, namely preparing the film from the mixture by a molding process, which is the aerogel plastic film. The aerogel plastic film has the beneficial effects that, different from conventional in-situ compounding, a step for gelling a reinforcing material with aerogel precursor does not exist, the process is simple without a great number of chemical equipment or site limitation, can conveniently realize large-scale production. The method can be used for preparing the aerogel plastic film, which is a novel product mode to meet the requirement of the prior art for ultrathin aerogel materials.

Description

technical field [0001] The invention belongs to the field of gel materials, and in particular relates to an airgel plastic film and a preparation method thereof. Background technique [0002] Airgel is a low-density material with a nano-porous structure. Due to its extremely low density and light weight, airgel is usually called solid smoke; at the same time, more than 95% of airgel is air, so It also has a very good thermal insulation effect. For example, the electrical conductivity of silicon aerogel can be as low as 0.013W / (m·k) at room temperature. Therefore, aerogel is considered to be a thermal insulation material with outstanding performance. However, the strength of pure airgel is poor, and it is difficult to act as a bulk material for thermal insulation engineering or other fields. The usual way to solve the above problems is to combine airgel with fiber reinforced materials to form composite materials to enhance the strength of airgel materials and meet the requir...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08J5/18C08L33/00C08L75/04C08L29/04C08L77/00C08K7/24C08K3/22
CPCC08J5/18C08J2329/04C08J2333/00C08J2375/04C08J2433/00C08J2475/04C08K3/22C08K7/24C08K2003/2296C08K2201/003C08K2201/006C08K2201/011C08L33/00C08L75/04C08L2203/16C08L29/04C08L77/00
Inventor 王天赋彭战军
Owner 湖北硅金凝节能减排科技有限公司
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