Heat-generating phase-change core-sheath fiber and preparation method thereof
A skin-core fiber and phase change technology, which is applied in fiber processing, fiber chemical characteristics, rayon manufacturing, etc., can solve the problems of no mention of fiber temperature regulation and temperature control function, poor heat absorption efficiency, etc., to improve comfort and The effect of ambient temperature adaptability
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Embodiment 1
[0026] Embodiment 1: A method for preparing a heat-generating phase-change sheath-core fiber, comprising the following steps:
[0027] (1) Preparation of inorganic exothermic particle modified polymer fiber-forming polymer
[0028] It is prepared by mixing 99.9 kg of PET with 0.1 kg of zirconium carbide powder with a mesh size of 1000, drying them, and blending and granulating with twin-screws at 275°C.
[0029] (2) Preparation of the temperature-regulating material for the core layer:
[0030] With 0.1 kilogram of n-decane (alkane low molecular weight phase change material), 0.1 kilogram of NiFe 2 o 4 , 99.8 kilograms of PET were mixed uniformly and dried to prepare a core layer temperature-regulating material (or a core layer phase change material).
[0031] (3) Preparation of exothermic phase change sheath-core fiber:
[0032] Put 100 kg of the prepared inorganic heating particle modified polymer fiber-forming polymer and 100 kg of the core layer temperature-regulating ...
Embodiment 2
[0033] Embodiment 2: A method for preparing a heat-generating phase-change sheath-core fiber, comprising the following steps:
[0034] (1) Preparation of inorganic exothermic particle modified polymer fiber-forming polymer
[0035] 90 kg of PBT and 10 kg of 2000-mesh far-infrared ceramic powder were uniformly mixed and dried. Under the condition of 245° C., the fiber-forming polymer was prepared by twin-screw blending and granulation to obtain the inorganic heating particle modified polymer.
[0036] (2) Preparation of the temperature-regulating material for the core layer:
[0037] With 1 kilogram of n-eicosane (alkane low molecular weight phase change material), 1 kilogram of Fe 3 o 4 , 98 kilograms of PBT were mixed uniformly and dried to prepare the temperature-regulating material for the core layer.
[0038] (3) Preparation of exothermic phase change sheath-core fiber:
[0039] Put 60 kg of the prepared inorganic heat-generating particle-modified polymer fiber-forming...
Embodiment 3
[0040] Embodiment 3: A method for preparing a heat-generating phase-change sheath-core fiber, comprising the following steps:
[0041] (1) Preparation of inorganic exothermic particle modified polymer fiber-forming polymer
[0042] 80 kg of PA66 and 20 kg of silicon carbide powder with a mesh size of 3000 were mixed uniformly and dried. Under the condition of 250°C, they were blended and granulated by twin-screw to prepare inorganic exothermic particle modified polymer fiber-forming polymer (exothermic Powder modified polymer fiber-forming polymer).
[0043] (2) Preparation of the temperature-regulating material for the core layer:
[0044] With 10 kilograms of n-tetradecane (alkane low molecular weight phase change material), 2 kilograms of Fe 3 o 4, 88 kilograms of PTT were mixed uniformly and dried to prepare a core layer temperature-regulating material (or a core layer phase change material).
[0045] (3) Preparation of exothermic phase change sheath-core fiber:
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