Grain refinement in IN706 using laves phase precipitation
A technology of precipitates and intermediate products, applied in the field of grain refinement using Laves phase precipitation in IN706, which can solve the problems of rough grain size, reduction, low cycle fatigue life, etc.
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[0037] In one aspect, the invention provides a method of making an article comprising deforming an ingot of a nickel-based superalloy to form an intermediate article in which a substantially uniform dispersion of Laves phase precipitates is formed , wherein the Laves phase precipitates are present in the intermediate article at a concentration of at least about 0.05% by volume, and wherein the precipitates have an average diameter of less than 1 micron.
[0038] In one example, the Laves phase precipitate can be present in the intermediate article at a concentration of at least about 0.075% by volume. In another example, the Laves phase precipitate can be present in the intermediate article at a concentration of at least about 0.1% by volume.
[0039] In yet another example, forming a substantially uniform dispersion of Laves phase precipitates can include maintaining the temperature range to which the intermediate article is exposed, eg, between 700°C and 1000°C for at least ...
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