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Hydrophilic color fixing agent for cotton fabric and preparation method thereof

A technology of cotton fiber fabric and hydrophilic type, which is applied in the field of hydrophilic color fixing agent and its preparation, can solve the problems of not affecting the hygroscopicity and the color fixing effect, and achieve the improvement of wet treatment fastness and color fixing effect Good, good color fixing effect

Inactive Publication Date: 2018-03-13
杭州瑞江实业有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

These two types of hydrophilic color-fixing agents cannot solve the contradiction between the color-fixing effect and the hygroscopicity.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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  • Hydrophilic color fixing agent for cotton fabric and preparation method thereof
  • Hydrophilic color fixing agent for cotton fabric and preparation method thereof
  • Hydrophilic color fixing agent for cotton fabric and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0035] A hydrophilic color fixing agent for cotton fiber fabrics, which is polymerized by the following components by mass: 10 parts of 2-vinylpyridine (2VP), 20 parts of hydroxyethylethylenediamine (AEEA), aminoethyl 50 parts of piperazine (AEP), 5 parts of methyl methacrylate, 10 parts of ethanol, 0.8 parts of azobis(2-amidinopropane) dihydrochloride, and 10 parts of hydrochloric acid.

[0036] A kind of preparation method of hydrophilic type color fixing agent for cotton fiber fabric, adopts following steps:

[0037] A. Take the raw materials according to the above ratio for subsequent use, and purify the vinylpyridine compound;

[0038] B. Mix the amine compound, acrylic compound, and solvent evenly at room temperature, heat to 25°C and keep it for 30 minutes, add vinylpyridine compound, mix well, continue to heat up to 50°C, keep the temperature for 30 minutes, and start to drop slowly to trigger agent, the initiator dropping time is 2.0h, the temperature rises to 80°C, ...

Embodiment 2

[0042] A hydrophilic color fixing agent for cotton fiber fabrics, which is polymerized by the following components by mass: 10 parts of 2-vinylpyridine (2VP), 20 parts of hydroxyethylethylenediamine (AEEA), aminoethyl 30 parts of piperazine (AEP), 20 parts of tetraethylenepentamine (TEPA), 5 parts of methyl methacrylate, 10 parts of dimethyl sulfoxide, 1.0 part of ammonium persulfate and 10 parts of hydrochloric acid.

[0043] A kind of preparation method of hydrophilic type color fixing agent for cotton fiber fabric, adopts following steps:

[0044] A. Take the raw materials according to the above ratio for subsequent use, and purify the vinylpyridine compound;

[0045] B. Mix the amine compound, acrylic compound and solvent evenly at room temperature, heat to 40°C and keep it for 30 minutes, add the vinylpyridine compound, mix it evenly, continue to heat up to 75°C, keep the temperature for 60 minutes, start to slowly drop the trigger agent; the dripping time of the initiat...

Embodiment 3

[0049] A hydrophilic color fixing agent for cotton fiber fabrics, which is polymerized from the following components by mass: 5 parts of 2-vinylpyridine (2VP), 5 parts of 4-vinylpyridine (4VP), aminoethyl 50 parts of piperazine (AEP), 20 parts of tetraethylenepentamine (TEPA), 5 parts of methyl methacrylate, 5 parts of ethanol, 5 parts of dimethyl sulfoxide, 1.0 part of ammonium persulfate and 10 parts of hydrochloric acid.

[0050] A kind of preparation method of hydrophilic type color fixing agent for cotton fiber fabric, adopts following steps:

[0051] A. Take the raw materials according to the above ratio for subsequent use, and purify the vinylpyridine compound;

[0052] B. Mix the amine compound, acrylic compound, and solvent evenly at room temperature, heat to 30°C and keep it for 30 minutes, add the vinylpyridine compound, mix it evenly, continue to heat up to 50°C, keep the temperature for 60 minutes, and start to slowly drop the trigger agent; the dripping time of ...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Abstract

The invention relates to a hydrophilic color fixing agent for cotton fabric. The hydrophilic color fixing agent for the cotton fabric is characterized by being prepared by polymerizing the following components: 5-30 parts of a vinyl pyridine compound, 30-90 parts of an amine compound, 5-40 parts of an acrylic compound, 5-50 parts of a solvent, 0.02-3 parts of an initiator and 5-30 parts of neutralizing acid. The hydrophilic color fixing agent for the cotton fabric has the beneficial effects as follows: the hydrophilic color fixing agent for the cotton fabric does not affect the hydrophilicityand the hand feel of the fabric itself and can achieve a good color fixing effect.

Description

technical field [0001] The invention relates to a hydrophilic color-fixing agent for cotton fiber fabrics and a preparation method thereof. The hydrophilic color-fixing agent does not affect the hydrophilicity and hand feeling of the fabric itself, and at the same time can achieve the color fastness of traditional color-fixing agents Spend. technical background [0002] Cotton fiber fabrics have good hygroscopicity, warmth retention and soft hand properties and play an important role in fabric fibers. Cotton fiber dyeing mainly includes reduction, direct vulcanization and reactive dyes, etc. Among them, reactive dyes have achieved rapid development because of their broad color spectrum, economy, and environmental protection. The color-fixing agents for reactive dye cotton on the market have mainly experienced dicyandiamide formaldehyde resin-type color-fixing agents, polyamine-type resin-type color-fixing agents, polycation-type color-fixing agents, reactive resin color-fix...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Application Information

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IPC IPC(8): D06P1/52D06P3/60
CPCD06P1/5242D06P1/525D06P3/60
Inventor 张春梅
Owner 杭州瑞江实业有限公司
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