Preparation method of chitosan leather mildew-proof novel material

A new material, chitosan technology, applied in botany equipment and methods, chemicals for biological control, animal repellents, etc., can solve problems such as adverse human health, achieve strong bactericidal effect and long duration , evenly dispersed effect

Inactive Publication Date: 2018-03-16
孝感市锐思新材科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] Most of the existing leather antifungal agent products use organic substances with antibacterial effect or heavy metal silver as effective antibacterial ingredients, and many leather products stick to the human body for a long time, which is not good for human health

Method used

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  • Preparation method of chitosan leather mildew-proof novel material

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0020] In the reaction kettle, add 100Kg of carboxymethylcellulose, 2Kg of ethylene bis(oxyethylene) dicaproate, 2Kg of 1,3-adamantanediol diacrylate, 0.3Kg of yttrium disilicate, N-sulfonic acid 0.2Kg of acid butylpyridine p-toluenesulfonate ionic liquid, 0.2Kg of calcium lignosulfonate, 200Kg of ethanol, 0.3Kg of benzoyl peroxide, 2Kg of gelatin, heated to 85°C, and stirred at a speed of 250rpm for 3h to obtain Chitosan leather anti-mildew new material.

Embodiment 2

[0022] In the reaction kettle, add 100Kg of carboxymethylcellulose, 1Kg of ethylene bis(oxyethylene) dicaproate, 1Kg of 1,3-adamantanediol diacrylate, 0.1Kg of yttrium disilicate, N-sulfonic acid 0.1Kg of acid butylpyridine p-toluenesulfonate ionic liquid, 0.1Kg of calcium lignosulfonate, 150Kg of ethanol, 0.1Kg of benzoyl peroxide, and 1Kg of gelatin, heated to 80°C, and stirred at a speed of 200rpm for 2h to obtain Chitosan leather anti-mildew new material.

Embodiment 3

[0024] In the reaction kettle, add 100Kg of carboxymethylcellulose, 3Kg of ethylene bis(oxyethylene) dicaproate, 3Kg of 1,3-adamantanediol diacrylate, 0.5Kg of yttrium disilicate, N-sulfonic acid Acid butylpyridine p-toluenesulfonate ionic liquid 0.3Kg, calcium lignosulfonate 0.3Kg, ethanol 250Kg, benzoyl peroxide 0.5Kg, gelatin 5Kg, heat up to 90°C, stir at 300rpm for 4h, and obtain Chitosan leather anti-mildew new material.

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Abstract

The invention relates to a preparation method of a chitosan leather mildew-proof novel material. The preparation method of the chitosan leather mildew-proof novel material comprises the following steps: adding the following components in a reaction kettle in parts by weight: carboxymethyl chitosan, ethylene bis(oxy-ethylene) adipic esters, 1,3-adamantane glycol diacrylate, yttrium mesosilicate, N-butylpyridine sulfonate p-toluene sulfonate ionic liquid, calcium lignosulphonate, ethanol, benzoyl peroxide and gelatin; and heating and stirring to obtain the chitosan leather mildew-proof novel material.

Description

technical field [0001] The invention relates to a preparation method of an antifungal agent, in particular to a preparation method of a chitosan leather antifungal new material. Background technique [0002] With the improvement of people's living standards, the amount of leather is increasing. However, the raw hides used in tanning production are rich in nutrients such as protein and fat, and are very vulnerable to the invasion of microorganisms during preservation. Although the processed leather has increased resistance to microorganisms, mildew will still occur, especially in the leather production process, a large amount of fatliquor produced with natural oils is introduced, and they are also breeding grounds for microorganisms to multiply. In addition, the porosity and polar structure of the leather structure make it easy to absorb moisture and the leather is acidic. All of the above reasons constitute the basic conditions for mildew. White, blue, yellow and black co...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A01N43/40A01N43/16A01P1/00
CPCA01N43/16A01N43/40
Inventor 王艺霖王新
Owner 孝感市锐思新材科技有限公司
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