Micro powder prepolymer formula and preparation method thereof
A prepolymer and micropowder technology, applied in chemical instruments and methods, other chemical processes, etc., can solve the problems of abrasive application limitations, long working hours, and affecting efficiency, and achieve high-speed grinding characteristics, high grinding rate, and durable and stable cutting force effect
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[0019] Example 1
[0020] A formula of micropowder prepolymer, the formula of said micropowder prepolymer is as follows:
[0021] Abrasive 60%
[0022] Additive 1.5%
[0023] Filler 8.5%
[0024] Adhesive aqueous solution 30%
[0025] The invention also provides a method for preparing the micropowder prepolymer, which includes the following steps:
[0026] S1. After mixing abrasives, additives, fillers and adhesive solutions in a certain proportion, disperse them evenly in a ball mill tank to obtain a slurry. The grinding ball is zirconia, the diameter is 5mm, the ball to material ratio is 2:1, and the speed is 80rpm, ball milling time is 24 h;
[0027] S2. The ball mill slurry is granulated. The slurry is centrifuged and spray-dried to obtain spherical granulated powder. The diameter of the granulated powder can be controlled at 55μm by adjusting the parameters of the dryer. The inlet temperature of the spray dryer is 180 ℃, and the outlet The temperature is 90 ℃, the feed rate is 0.2 L...
Example Embodiment
[0029] Example 2
[0030] A formula of micropowder prepolymer, the formula of said micropowder prepolymer is as follows:
[0031] Abrasive 55%
[0032] Additive 3.5%
[0033] Filling 16.5%
[0034] Adhesive aqueous solution 25%
[0035] The invention also provides a method for preparing the micropowder prepolymer, which includes the following steps:
[0036] S1. After mixing abrasives, additives, fillers, and adhesive solutions in a certain proportion, disperse them uniformly in a ball milling tank to obtain a slurry. The grinding ball is zirconia, the diameter is 12mm, the ball-to-battery ratio is 1:1, and the speed is 80 rpm, ball milling time is 48 h;
[0037] S2. The ball mill slurry is granulated. The slurry is spray-dried by centrifugal spray to obtain spherical granulated powder. The diameter of the granulated powder can be controlled at 28μm by adjusting the parameters of the dryer. The inlet temperature of the spray dryer is 230 ℃, and the outlet The temperature is 100 ℃, the fe...
Example Embodiment
[0039] Example 3
[0040] A formula of micropowder prepolymer, the formula of said micropowder prepolymer is as follows:
[0041] Abrasive 35%
[0042] Additive 0.5%
[0043] Filling 14.5%
[0044] Adhesive aqueous solution 50%
[0045] The invention also provides a method for preparing the micropowder prepolymer, which includes the following steps:
[0046] S1, after mixing abrasives, additives, fillers and adhesive solutions in a certain proportion, uniformly dispersed in a ball milling tank to obtain a slurry, the grinding ball is zirconia, the diameter is 12mm, and the ball-to-battery ratio is 1:0.5, Rotation speed is 110 rpm, ball milling time is 50 h;
[0047] S2. The ball mill slurry is granulated. The slurry is centrifuged and spray-dried to obtain spherical granulated powder. The diameter of the granulated powder can be controlled at 15μm by adjusting the parameters of the dryer. The inlet temperature of the spray dryer is 260 ℃, and the outlet The temperature is 130 ℃, the feed...
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