Micro powder prepolymer formula and preparation method thereof

A prepolymer and micropowder technology, applied in chemical instruments and methods, other chemical processes, etc., can solve the problems of abrasive application limitations, long working hours, and affecting efficiency, and achieve high-speed grinding characteristics, high grinding rate, and durable and stable cutting force effect

Pending Publication Date: 2018-04-20
河北思瑞恩新材料科技有限公司
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AI-Extracted Technical Summary

Problems solved by technology

[0002] During the use of traditional abrasives, there is a contradiction between grinding efficiency and grinding effect. Large-grained abrasives have a high grinding rate but will cause large scratches on the surface of the workpiece to be processed. Small-grained abrasives can be processed better. Superficial, but it takes a long time to work and affects efficiency
How to make grinding achieve fast and good pro...
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Abstract

The invention discloses a micro powder prepolymer formula, which is prepared from the following ingredients including 30 to 70 percent of grinding materials, 0.1 to 3.5 percent of auxiliary agents, 8to 45 percent of filling materials and 25 to 65 percent of adhesive water solution. Small-particle micro powder can be combined through bonding agents to become a larger micro powder prepolymer. In the grinding process of the prepolymer, the large-area multi-point contact is realized; the big particle high-speed grinding characteristics are realized; high grinding speed is realized; in addition, the prepolymer can gradually release fine and crushed ground materials in the grinding process; the restoration and polishing effects are achieved; the durable and stable cutting force is realized; meanwhile, the fine grinding surface can also be obtained. In addition, the roasting process can be regulated to obtain a smooth surface and a rough surface; the prepolymers with different combination force can also be obtained; the prepolymer is applied to the preparation of grinding liquid, coating milling tools and concretion milling tools; the high-speed and high-flatness surface processing can be realized.

Application Domain

Other chemical processes

Technology Topic

PrepolymerHigh-speed grinding +11

Examples

  • Experimental program(4)

Example Embodiment

[0019] Example 1
[0020] A formula of micropowder prepolymer, the formula of said micropowder prepolymer is as follows:
[0021] Abrasive 60%
[0022] Additive 1.5%
[0023] Filler 8.5%
[0024] Adhesive aqueous solution 30%
[0025] The invention also provides a method for preparing the micropowder prepolymer, which includes the following steps:
[0026] S1. After mixing abrasives, additives, fillers and adhesive solutions in a certain proportion, disperse them evenly in a ball mill tank to obtain a slurry. The grinding ball is zirconia, the diameter is 5mm, the ball to material ratio is 2:1, and the speed is 80rpm, ball milling time is 24 h;
[0027] S2. The ball mill slurry is granulated. The slurry is centrifuged and spray-dried to obtain spherical granulated powder. The diameter of the granulated powder can be controlled at 55μm by adjusting the parameters of the dryer. The inlet temperature of the spray dryer is 180 ℃, and the outlet The temperature is 90 ℃, the feed rate is 0.2 L/min, and the atomizer rotation speed is 25000 rpm;
[0028] S3. The granulated powder is calcined in a muffle furnace. The calcining temperature is 300 ℃ and the holding time is 3 hours according to the selected abrasive and filler. After cooling to room temperature, the required powder prepolymer is obtained.

Example Embodiment

[0029] Example 2
[0030] A formula of micropowder prepolymer, the formula of said micropowder prepolymer is as follows:
[0031] Abrasive 55%
[0032] Additive 3.5%
[0033] Filling 16.5%
[0034] Adhesive aqueous solution 25%
[0035] The invention also provides a method for preparing the micropowder prepolymer, which includes the following steps:
[0036] S1. After mixing abrasives, additives, fillers, and adhesive solutions in a certain proportion, disperse them uniformly in a ball milling tank to obtain a slurry. The grinding ball is zirconia, the diameter is 12mm, the ball-to-battery ratio is 1:1, and the speed is 80 rpm, ball milling time is 48 h;
[0037] S2. The ball mill slurry is granulated. The slurry is spray-dried by centrifugal spray to obtain spherical granulated powder. The diameter of the granulated powder can be controlled at 28μm by adjusting the parameters of the dryer. The inlet temperature of the spray dryer is 230 ℃, and the outlet The temperature is 100 ℃, the feed rate is 0.5 L/min, and the atomizer rotation speed is 35000 rpm;
[0038] S3. The granulated powder is calcined in a muffle furnace. Depending on the selected abrasive and filler, the calcining temperature is 600 ℃, and the holding time is 4.5 hours. After cooling to room temperature, the required powder prepolymer is obtained.

Example Embodiment

[0039] Example 3
[0040] A formula of micropowder prepolymer, the formula of said micropowder prepolymer is as follows:
[0041] Abrasive 35%
[0042] Additive 0.5%
[0043] Filling 14.5%
[0044] Adhesive aqueous solution 50%
[0045] The invention also provides a method for preparing the micropowder prepolymer, which includes the following steps:
[0046] S1, after mixing abrasives, additives, fillers and adhesive solutions in a certain proportion, uniformly dispersed in a ball milling tank to obtain a slurry, the grinding ball is zirconia, the diameter is 12mm, and the ball-to-battery ratio is 1:0.5, Rotation speed is 110 rpm, ball milling time is 50 h;
[0047] S2. The ball mill slurry is granulated. The slurry is centrifuged and spray-dried to obtain spherical granulated powder. The diameter of the granulated powder can be controlled at 15μm by adjusting the parameters of the dryer. The inlet temperature of the spray dryer is 260 ℃, and the outlet The temperature is 130 ℃, the feed rate is 0.6 L/min, and the atomizer rotation speed is 40,000 rpm;
[0048] S3. The granulated powder is calcined in a muffle furnace. The calcining temperature is 700 ℃ and the holding time is 5.5h according to the selected abrasives and fillers. After cooling to room temperature, the required powder prepolymer is obtained.

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Description & Claims & Application Information

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