Preparation method of high-purity fine-grained pure copper material for medicine-type cover
A high-purity, medicine-shaped mask technology, which is applied in the field of preparation of high-purity fine-grained pure copper materials for medicine-shaped masks, can solve problems such as uneven grain size and many impurity elements, and achieve stable material performance and high material yield. High efficiency, friction reduction effect
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Embodiment 1
[0031] A preparation method of a high-purity fine-grained pure copper material for a drug-type cover is carried out according to the following steps:
[0032] (1) Preparation of blanks: commercial T2 pure copper rods are used, the size specification is φ120mm, and the average grain size is about 250μm (such as figure 1 ), the content of impurity elements is shown in Table 1. Use sawing to cut the material to a length of 500mm to remove oxides and oil on the surface.
[0033] Table 1 Content of impurity elements in T2 copper rods
[0034] grade P Bi Sb As Fe Ni sn S 0 Pb Zn sum T2 60 40 30 20 50 200 20 40 380 120 40 1000
[0035] (2) Vacuum electron beam melting: use an electron beam melting furnace with a power of 900kw for secondary electron beam melting and purification, the copper crystallizer is φ250mm, and the vacuum degree of the melting chamber is ≥2×10 -3 Pa, the primary smelting speed is 100kg / h, the ingot spinning...
Embodiment 2
[0044] A preparation method of a high-purity fine-grained pure copper material for a drug-type cover is carried out according to the following steps:
[0045] (1) Preparation of the billet: commercial T3 pure copper rods are used, the size specification is φ90mm, and the average grain size is about 130μm (such as image 3 ), the content of impurity elements is shown in Table 3. Use sawing to cut the material to a length of 800mm to remove oxides and oil stains on the surface.
[0046] Table 3 The content of impurity elements in T3 copper rods (×10 -6 )
[0047]
[0048]
[0049] (2) Vacuum electron beam melting: use an electron beam melting furnace with a power of 900kw for secondary electron beam melting and purification, the copper crystallizer is φ250mm, and the vacuum degree of the melting chamber is ≥2×10 -3 Pa, the primary smelting speed is 80kg / h, the ingot rotating and drawing speed is 2mm / min; the secondary melting speed is 100kg / h, and the ingot rotating and...
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