Temperature-resisting diaphragm for solar lithium battery and solar lithium battery
A lithium battery and solar energy technology, applied in lithium batteries, battery pack components, non-aqueous electrolyte batteries, etc., can solve the problems of aggravated heat accumulation, high risk, easy to melt, etc., and achieve good charge-discharge efficiency and dispersion. Good, low thermal shrinkage effect
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Embodiment 1
[0026] A temperature-resistant separator for solar lithium batteries comprises a polyolefin film and a cellulose film compounded on the polyolefin film, and the cellulose film is made of microcrystalline cellulose and porous silicon dioxide.
[0027] Wherein, the preparation method of described cellulose film comprises the steps:
[0028] A, adding 3 parts by weight of nanocellulose to 25 parts by weight of an aqueous ethanol solution with a volume concentration of 95% for ultrasonic dispersion to obtain a dispersion;
[0029] B. Add 33 parts by weight of ethyl orthosilicate to the dispersion, adjust the pH to 9.5 with ammonia water to hydrolyze the ethyl orthosilicate to obtain nanocellulose / silicon dioxide nanospheres;
[0030] C. Calcining the nanocellulose / silica nanospheres to remove the nanocellulose to obtain porous silica nanospheres;
[0031] D. At a temperature of 80°C, dissolve microcrystalline cellulose in 1-methyl 3-butylimidazolium chloride ionic liquid in a mas...
Embodiment 2
[0041] A temperature-resistant separator for solar lithium batteries comprises a polyolefin film and a cellulose film compounded on the polyolefin film, and the cellulose film is made of microcrystalline cellulose and porous silicon dioxide.
[0042] Wherein, the preparation method of described cellulose film comprises the steps:
[0043]A, adding 1 weight part of nanocellulose to 20 weight parts of ethanol aqueous solution with a volume concentration of 92% for ultrasonic dispersion to obtain a dispersion;
[0044] B. Add 28 parts by weight of ethyl orthosilicate to the dispersion, use ammonia water to adjust the pH to 9 to hydrolyze the ethyl orthosilicate to obtain nanocellulose / silicon dioxide nanospheres;
[0045] C. Calcining the nanocellulose / silica nanospheres to remove the nanocellulose to obtain porous silica nanospheres;
[0046] D. At a temperature of 70°C, dissolve microcrystalline cellulose in 1-methyl 3-butylimidazolium chloride ionic liquid in a mass ratio of ...
Embodiment 3
[0056] A temperature-resistant separator for solar lithium batteries comprises a polyolefin film and a cellulose film compounded on the polyolefin film, and the cellulose film is made of microcrystalline cellulose and porous silicon dioxide.
[0057] Wherein, the preparation method of described cellulose film comprises the steps:
[0058] A, adding 5 parts by weight of nanocellulose to 30 parts by weight of an aqueous ethanol solution with a volume concentration of 98% for ultrasonic dispersion to obtain a dispersion;
[0059] B. Add 38 parts by weight of ethyl orthosilicate to the dispersion, use ammonia to adjust the pH to 10 to hydrolyze the ethyl orthosilicate to obtain nanocellulose / silicon dioxide nanospheres;
[0060] C. Calcining the nanocellulose / silica nanospheres to remove the nanocellulose to obtain porous silica nanospheres;
[0061] D. At a temperature of 90°C, dissolve microcrystalline cellulose in 1-methyl 3-butylimidazolium chloride ionic liquid in a mass rat...
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