A kind of umami tetradetrapeptide and its Maillard reaction product and application
A Maillard reaction and product technology, applied in the field of food additives, can solve problems that are not recognized by Western scholars.
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Embodiment 1
[0034] The synthetic method of polypeptide RGENESDEQGAIVT comprises the following steps:
[0035] Swell and wash 1 g of dichloro resin, remove the Fmoc protecting group, add amino acid for condensation reaction, repeat the deprotection-condensation process until all amino acids are connected. Cleave the resin to obtain the crude peptide RGENESDEQGAIVT, then purify it by reverse-phase high-performance liquid chromatography, and freeze-dry to obtain the umami tetradecapeptide.
[0036] The umami taste and umami-increasing threshold of umami tetradecapeptide are shown in Table 1.
[0037] The application effect of umami fourteen peptides in condiments is shown in Table 2.
Embodiment 2
[0039] The preparation method of the Maillard reaction product of polypeptide RGENESDEQGAIVT comprises the following steps:
[0040] Mix 3g of umami tetradecapeptide (RGENESDEQGAIVT), 1g of glucose and 6g of deionized water, adjust the pH of the system to 6.5 with 0.1mol / L sodium hydroxide solution, react at 110°C for 60min, finish the reaction and cool down to room temperature, freeze-dry , to obtain the umami fourteen peptide Maillard reaction product 1.
[0041] The umami taste and umami-increasing threshold of umami tetradetrapeptide Maillard reaction product 1 are shown in Table 1.
[0042] The application effect of the umami tetradetrapeptide Maillard reaction product 1 in condiments is shown in Table 2.
Embodiment 3
[0044] The preparation method of the Maillard reaction product of polypeptide RGENESDEQGAIVT comprises the following steps:
[0045] Mix 5.5g of umami fourteen peptide (RGENESDEQGAIVT), 0.5g of glucose and 4g of deionized water, adjust the pH of the system to 5.0 with 0.1mol / L sodium hydroxide solution and 0.1mol / L HCL solution, and react at 80°C for 20min After finishing the reaction, the temperature was lowered to normal temperature, freeze-dried, and the umami fourteen peptide Maillard reaction product 2 was obtained.
[0046] The umami taste and umami-increasing threshold of umami tetradetrapeptide Maillard reaction product 2 are shown in Table 1.
[0047] The application effect of the umami tetradetrapeptide Maillard reaction product 2 in condiments is shown in Table 2.
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