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Glass etching solution, preparation method of glass etching solution and method for preparing anti-glare glass with glass etching solution

An etching solution and anti-glare technology, which is applied in the field of vehicle-mounted anti-glare glass preparation, can solve problems such as interfering with the correct judgment of drivers and passengers, vehicle driving and personal safety hazards, and achieve homogenization of grain size and improvement of suspension capacity , The effect of slowing down the etching reaction speed

Active Publication Date: 2018-11-20
ZHENGZHOU HIHO OPTICAL TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] At present, the car display screens are all made of anti-glare glass with low fog and low roughness characteristics. Although it meets the requirements of normal use, in special environments such as strong sunlight, the driver and passengers will still be affected by the reflection of the screen, which will interfere with the driver and passengers. Correct judgment will bring great potential safety hazards to vehicle driving and personal safety

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] A kind of glass etchant, is made up of the raw material of following percentage by weight: citric acid 10%, acetic acid 10%, NH 4 F 25%, (NH 4 ) 2 SiF 6 5%, K 2 SiF 6 2.5%, (NH 4 ) 2 HPO 4 10%, viscosity modifier 1.0% (barium sulfate), surfactant 1.0% (sodium dodecylbenzenesulfonate), and the balance is pure water.

[0023] The method for preparing glass etching solution comprises the following steps:

[0024] At a stirring speed of 100 r / min,

[0025] Add acetic acid to water, mix well, then add citric acid, NH 4 F, (NH 4 ) 2 HPO 4 , after mixing, add (NH 4 ) 2 SiF 6 and K 2 SiF 6 , mix well, add a viscosity modifier and a surfactant, mix well, and age for 4 hours to obtain a glass etching solution.

[0026] The method for preparing anti-glare glass by using glass etching solution comprises the following steps:

[0027] Immerse the glass cleaned with pure water into the glass etching solution, let it stand for 90 seconds, polish it for 25 minutes, s...

Embodiment 2

[0030] A kind of glass etchant, is made up of the raw material of following percentage by weight: citric acid 7.5%, acetic acid 6.5%, NH 4 F 27%, (NH 4 ) 2 SiF 6 7.5%, K 2 SiF 6 1.5%, (NH 4 ) 2 HPO 4 7%, viscosity regulator 1.2% (propylene glycol alginate), surfactant 0.6% (sodium lauryl sulfate), and the balance is pure water.

[0031] The method for preparing glass etching solution comprises the following steps:

[0032] At a stirring speed of 50 r / min,

[0033] Add acetic acid to water, mix well, then add citric acid, NH 4 F, (NH 4 ) 2 HPO 4 , after mixing, add (NH 4 ) 2 SiF 6 and K 2 SiF 6 , mix well, add a viscosity modifier and a surfactant, mix well, and age for 12 hours to obtain a glass etching solution.

[0034] The method for preparing anti-glare glass by using glass etching solution comprises the following steps:

[0035] Immerse the glass cleaned with pure water into the glass etching solution, let it stand for 120 seconds, polish it for 30 m...

Embodiment 3

[0038] A kind of glass etchant, is made up of the raw material of following percentage by weight: citric acid 13%, acetic acid 10%, NH 4 F 21%, (NH 4 ) 2 SiF 6 9%, K2 SiF 6 2%, (NH 4 ) 2 HPO 4 10%, viscosity regulator 0.8% (polyanionic cellulose), surfactant 1.2% (sodium dodecylbenzenesulfonate), and the balance is pure water.

[0039] The method for preparing glass etchant and the method for preparing anti-glare glass with glass etchant refer to Example 1.

[0040] After testing, the anti-glare glass has a gloss of 128, a haze of 8.5%, and a roughness of 0.042 μm. 075μm。 The current car anti-glare glass has a haze of 0.6% and a roughness of 0.075μm.

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Abstract

The invention discloses a glass etching solution. The glass etching solution is prepared from raw materials in percentage by weight as follows: 5%-15% of citric acid, 5%-15% of acetic acid, 20%-30% ofNH4F, 5%-10% of (NH4)2SiF6, 1%-5% of K2SiF6, 5%-15% of (NH4)2HPO4, 0.5%-1.5% of a viscosity regulator, 0.5%-1.5% of a surfactant and the balance of water. Meanwhile, the invention provides a corresponding preparation method of the glass etching solution and a method for preparing anti-glare glass with the glass etching solution. The glass etching solution has good stability and durability, and the prepared anti-glare glass is in the gloss 100-130 range required by vehicle mounting display, has the haze up to 6%-17% and the roughness of 0.040-0.065 mu m and has the performance superior to existing anti-glare glass.

Description

technical field [0001] The invention relates to the technical field of preparation of vehicle-mounted anti-glare glass, in particular to a glass etching solution, a preparation method thereof, and a method for preparing anti-glare glass using the glass etching solution. Background technique [0002] With the development of modernization, automobiles are used as people's daily means of transportation, and the automobile industry has ushered in unprecedented development. Display screens are one of the important components of vehicle display systems and vehicle imaging system equipment, and automobiles have their own unique safety features. Therefore, the display screen glass must also have safe and reliable all-weather display characteristics. Whether it is a traditional fuel vehicle or a pure electric vehicle, transparent plastic panels and glass cover materials are basically abandoned in the vehicle display system and vehicle imaging system equipment, and more anti-glare gla...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C03C15/00C03C21/00
CPCC03C15/00C03C21/002
Inventor 熊国祥盛成明
Owner ZHENGZHOU HIHO OPTICAL TECH CO LTD
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