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nb based on layer-by-layer stacking 3 Al superconducting precursor wire preparation method

A precursor and wire technology, which is applied in the field of preparation of multi-core Nb3Al superconducting precursor wires, can solve the problems of uneven deformation, difficult adjustment, and low tube filling rate, and achieve uniform tightness and convenient displacement and deformation. , avoid the effect of precision requirements

Active Publication Date: 2020-05-19
SOUTHWEST JIAOTONG UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The compound after winding is prone to problems such as large size deviation, low tube filling rate, and uneven lamination between layers.
In addition, the foils of each layer of the composite after winding are extruded, entangled, and pulled to form constraints, which are difficult to adjust in the later stage, which leads to uneven deformation of each component in subsequent processing. During the process, it is easy to have defects such as wire breakage and component segregation in the wire, which will eventually affect the performance of the superconducting wire.
As a result, it is difficult to process, the consistency of the product is poor, and the pass rate is low

Method used

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  • nb based on layer-by-layer stacking  <sub>3</sub> Al superconducting precursor wire preparation method
  • nb based on layer-by-layer stacking  <sub>3</sub> Al superconducting precursor wire preparation method
  • nb based on layer-by-layer stacking  <sub>3</sub> Al superconducting precursor wire preparation method

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0030] figure 1 , figure 2 It shows that a specific embodiment of the present invention is a layer-by-layer stacked Nb 3 A method for preparing an Al superconducting precursor wire, the steps of which are:

[0031] A. Preparation of Nb-Al composite sheath

[0032] Remove the upper cover 1 of the tubular Nb box 2, stack Nb foils 3 and Al foils 4 alternately in the rectangular groove of the tubular Nb box 2 from bottom to top, then cover the upper cover 1 of the tubular Nb box 2; finally put the tubular The Nb box 2 is set in the Cu tube, and the two ends of the Cu tube are welded and sealed by vacuum electron beams to obtain the Nb-Al composite sheath;

[0033] The thickness of the Nb foil 3 is 0.03mm, the thickness of the Al foil 4 is 0.01mm, and the purity of the Nb foil 3 and the Al foil 4 are both better than 99.9%.

[0034] The number of layers of the Nb foil 3 or Al foil 4 is 100, and the wall thickness of the Nb box 2 is 1mm.

[0035] The ratio of the volume of the...

Embodiment 2

[0042] A layer-by-layer stacking of Nb 3 The preparation method of Al superconducting precursor wire rod, its steps are:

[0043] A. Preparation of Nb-Al composite sheath

[0044] Remove the upper cover 1 of the tubular Nb box 2, stack Nb foils 3 and Al foils 4 alternately in the rectangular groove of the tubular Nb box 2 from bottom to top, then cover the upper cover 1 of the tubular Nb box 2; finally put the tubular The Nb box 2 is set in the Cu tube, and the two ends of the Cu tube are welded and sealed by vacuum electron beams to obtain the Nb-Al composite sheath;

[0045] The thickness of the Nb foil 3 is 0.13mm, the thickness of the Al foil 4 is 0.05mm, and the purity of the Nb foil 3 and the Al foil 4 are both better than 99.9%.

[0046] The number of layers of the Nb foil 3 or Al foil 4 is 125, and the wall thickness of the Nb box 2 is 5 mm.

[0047] The ratio of the volume of the rectangular slot of the Nb box 2 to the volume of the whole Nb box 2 is 2.5:4.

[004...

Embodiment 3

[0054] A layer-by-layer stacking of Nb 3 The preparation method of Al superconducting precursor wire rod, its steps are:

[0055] A. Preparation of Nb-Al composite sheath

[0056] Remove the upper cover 1 of the tubular Nb box 2, stack Nb foils 3 and Al foils 4 alternately in the rectangular groove of the tubular Nb box 2 from bottom to top, then cover the upper cover 1 of the tubular Nb box 2; finally put the tubular The Nb box 2 is set in the Cu tube, and the two ends of the Cu tube are welded and sealed by vacuum electron beams to obtain the Nb-Al composite sheath;

[0057] The thickness of the Nb foil 3 is 0.3mm, the thickness of the Al foil 4 is 0.1mm, and the purity of the Nb foil 3 and the Al foil 4 are both higher than 99.9%.

[0058] The number of layers of the Nb foil 3 or Al foil 4 is 150, and the wall thickness of the Nb box 2 is 10 mm.

[0059] The ratio of the volume of the rectangular slot of the Nb box 2 to the volume of the whole Nb box 2 is 3:4.

[0060] ...

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Abstract

A Nb based on layer-by-layer stacking 3 The preparation method of Al superconducting precursor wire mainly includes: A. Preparation of Nb-Al composite sheath: Nb foil and Al foil are alternately stacked in the rectangular groove of the tubular Nb box from bottom to top, and the upper cover is covered , in the Cu tube, welded and sealed; B. Preparation of Nb-Al single mandrel: the Nb-Al composite sheath is hydrostatically extruded, repeatedly drawn, and then corroded to remove the copper to obtain the Nb-Al single mandrel. Mandrel; C, Nb 3 Preparation of Al superconducting precursor wires: multiple Nb‑Al single mandrels are packed closely into Cu or Cu alloy sheaths, and multi-cores are obtained by electron beam sealing welding, hydrostatic extrusion, and repeated drawing. Wire rod; then corrode to remove copper. The method is simple to operate, the assembly filling rate of the foil material is high, and the compactness of each layer of foil material is uniform. The final superconducting wire prepared by it has good performance, strong consistency and high qualified rate. It is especially suitable for the preparation of long superconducting wires.

Description

technical field [0001] The invention belongs to the technical field of preparation methods of low-temperature superconducting materials, and in particular relates to a multi-core Nb 3 Preparation method of Al superconducting precursor wire. Background technique [0002] Nb 3 Al is the current superconducting transition temperature (T c ), critical current density (J c ) and upper critical field (H c2 ) and other low-temperature superconducting materials with the best comprehensive practical performance. it with Nb 3 Compared with Sn, the superconducting transition temperature reaches 19.3K, and it also belongs to the A15 structure intermetallic compound and grain boundary pinned superconductor; and has a higher upper critical field and better high-field critical current density characteristics; especially important, It is better than Nb 3 Sn has more excellent stress-strain tolerance characteristics. Therefore Nb 3 Al superconducting wires are considered to have gre...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): H01B12/10H01B13/00
CPCH01B12/10H01B13/00H01B13/0006Y02E40/60
Inventor 孙霞光羊新胜潘熙锋赵勇
Owner SOUTHWEST JIAOTONG UNIV
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