Reinforced product comprising a self-adhesive composite reinforcement containing a block copolymer
A technology of block copolymers and products, which can be used in the reinforcement layer of pneumatic tires, vehicle parts, transportation and packaging, etc., and can solve the problems of increasing the cost of rubber matrix, increasing the sensitivity of oxidation and aging, etc.
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no. 1 approach
[0118] According to the first embodiment, the block copolymer used according to the invention has the following formula:
[0119] PA-(R-Pol) n -R-Pol-R-PA
[0120] Wherein n is between 0 and 100, especially 0 to 10, preferably 0 or 1,
[0121] PA stands for polyamide block,
[0122] R represents an alkylene block,
[0123] Pol stands for polyolefin block.
no. 2 approach
[0124] According to the second embodiment, the block copolymer used according to the invention has the following formula:
[0125] PA-(R-Pol-PA) n -R-Pol-R-PA
[0126] Wherein n is between 0 and 100, especially 0 to 10, preferably 0 or 1,
[0127] PA, R and Pol are as defined above.
[0128] According to the third embodiment, the block copolymer used according to the invention has the following formula:
[0129] PA-(R-Pol-R-PA) n -R-Pol-R-PA
[0130] Wherein n is between 0 and 100, especially 0 to 10, preferably 0 or 1,
[0131] PA, R and Pol are as defined above.
[0132] Block content
[0133] Preferably, the block copolymer present in the coating composition according to the present invention contains between 0.1% and 25% by weight, preferably between 1% and 15% by weight, based on the total weight of the block copolymer The alkylene block content.
[0134] Advantageously, the block copolymer used according to the invention comprises an alkylene block content between 0.1% and 25% by wei...
Embodiment
[0370] I. Synthesis of block copolymer
[0371] Synthesis of copolymer: PA 1 according to the invention
[0372] The polybutadiene and the fatty acid dimer were mixed at a molar ratio of 1 / 2 (polybutadiene / fatty acid dimer).
[0373] The resulting mixture is then mixed with the polyamide as described below.
[0374] ·Preparation of PA11 diamine with a number average molecular weight of 5000g / mol:
[0375] 5000 g of 11-aminoundecanoic acid, 116.2 g of hexamethylene diamine and 750 g of deionized water were introduced into a 12-liter autoclave equipped with an anchor stirrer. The medium is inerted with nitrogen and then heated to a material temperature of 210°C with stirring. Then the pressure is 20 bar. The medium was then heated to a material temperature of 230°C while maintaining a pressure of 20 bar. When this temperature is reached, the pressure is returned to atmospheric pressure by reducing the pressure and flushing under nitrogen for 90 minutes.
[0376] The product thus obta...
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Abstract
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