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Fermentation defoaming agent and preparation method thereof

A defoamer and emulsifier technology, applied in the field of fermentation defoamer and its preparation, can solve the problems of affecting the operation of fermentation industry, weak defoaming ability, difficult to ensure performance at the same time, to ensure fermentation production efficiency and product conversion rate , good defoaming performance and antifoaming performance, easy to realize the effect of industrial production

Inactive Publication Date: 2018-12-18
万洪玲
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

A large amount of foam will be produced during the fermentation process. These stable foams will not only reduce the fermentation efficiency but also lead to a decrease in the conversion rate, which seriously affects the operation of the fermentation industry. At present, defoaming is mainly carried out by adding defoamers
[0003] At present, the defoamers used for fermentation mainly include silicone defoamers and polyether defoamers. Silicone defoamers defoam quickly but have insufficient foam suppression performance. Polyether defoamers have better foam suppression performance, but defoamer The ability is weak. At present, the defoaming performance and antifoaming performance are mainly improved by polyether modification of silicone. Although the performance has been improved, its adaptability is relatively poor, and it is difficult in carbon source fermentation and nitrogen source fermentation. At the same time, its performance is guaranteed, so it needs to be further improved to meet the production needs

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0026] A fermentation defoamer, comprising the following raw materials in parts by weight: 40 parts of castor oil, 26 parts of epoxy-terminated silicone oil, 18 parts of polyethylene glycol, 8 parts of polyetheramine, 12 parts of isopropanol, hydrophobic white carbon 2 parts black, 4 parts emulsifier;

[0027] The viscosity of the epoxy-terminated silicone oil is 1000cSt;

[0028] The polyethylene glycol molecular weight is 2500;

[0029] The polyetheramine molecular weight is 1500;

[0030] The emulsifier is composed of S-60 and glyceryl monostearate in a weight ratio of 1:2.

[0031] A preparation method of fermentation defoamer, comprising the following steps:

[0032] (1) Weigh castor oil and polyethylene glycol by weight, add them to the reaction vessel and stir, and add 0.1% antimony oxide by weight of castor oil, vacuumize, heat up to 200°C for reaction, control the reaction temperature to 240°C, and react The time is 4h;

[0033] (2) Add polyetheramine and isoprop...

Embodiment 2

[0037] A fermentation defoamer, comprising the following raw materials in parts by weight: 42 parts of castor oil, 28 parts of epoxy-terminated silicone oil, 19 parts of polyethylene glycol, 9 parts of polyetheramine, 13 parts of isopropanol, hydrophobic white carbon 3 parts black, 5 parts emulsifier;

[0038] The viscosity of the epoxy-terminated silicone oil is 1200cSt;

[0039] The polyethylene glycol molecular weight is 2700;

[0040] The polyetheramine molecular weight is 1700;

[0041] The emulsifier is composed of S-60 and glyceryl monostearate in a weight ratio of 1:2.5.

[0042] A preparation method of fermentation defoamer, comprising the following steps:

[0043] (1) Weigh castor oil and polyethylene glycol by weight, add them to the reaction vessel and stir, and add 0.1% antimony oxide by weight of castor oil, vacuumize, heat up to 205°C for reaction, control the reaction temperature to 245°C, and react The time is 4.5h;

[0044] (2) Add polyetheramine and iso...

Embodiment 3

[0048] A fermentation defoamer, comprising the following raw materials in parts by weight: 45 parts of castor oil, 30 parts of epoxy-terminated silicone oil, 20 parts of polyethylene glycol, 10 parts of polyetheramine, 14 parts of isopropanol, hydrophobic white carbon 4 parts black, 6 parts emulsifier;

[0049] The viscosity of the epoxy-terminated silicone oil is 1500cSt;

[0050] The polyethylene glycol molecular weight is 3000;

[0051] The polyetheramine molecular weight is 2000;

[0052] The emulsifier is composed of S-60 and glyceryl monostearate in a weight ratio of 1:3.

[0053] A preparation method of fermentation defoamer, comprising the following steps:

[0054] (1) Weigh castor oil and polyethylene glycol by weight, add them to the reaction vessel and stir, and add 0.1% antimony oxide by weight of castor oil, vacuumize, heat up to 210°C for reaction, control the reaction temperature to 250°C, and react The time is 5h;

[0055] (2) Add polyetheramine and isopro...

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PUM

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Abstract

The invention discloses a fermentation defoaming agent and a preparation method thereof. The fermentation antifoaming agent is prepared from the following raw materials in parts by weight: 40 to 50 parts of castor oil, 26 to 34 parts of epoxy-terminated silicone oil, 18 to 22 parts of polyethylene glycol, 8 to 12 parts of polyetheramine, 12 to 16 parts of isopropanol, 2 to 6 parts of hydrophobic white carbon black, and 4 to 8 parts of an emulsifier; the fermentation defoaming agent is prepared by adopting the castor oil, the epoxy-terminated silicone oil, the polyethylene glycol, the polyetheramine, the isopropanol, the hydrophobic white carbon black and the emulsifier as raw materials through the preparation method, and the prepared defoaming agent has good defoaming performance and antifoaming performance in fermentation by modifying the silicone oil with polyether modification and castor oil modification at the same time, the use amount of the defoaming agent is reduced, the cost islowered, the influence on the quality of fermentation products is reduced, and the fermentation production efficiency and product conversion rate are ensured; the preparation process is simple, can easily achieve industrialized production, and is worth popularizing.

Description

technical field [0001] The invention relates to a food additive, in particular to a fermentation defoamer and a preparation method thereof. Background technique [0002] Food additives are synthetic or natural substances added to food to improve food color, aroma, taste and other qualities, as well as to meet the needs of antisepsis and processing technology. At present, there are 23 categories and more than 2,000 varieties of food additives in my country, including acidity regulators, anticaking agents, defoamers, antioxidants, bleaching agents, and leavening agents. A large number of foams will be produced during the fermentation process. These stable foams will not only reduce the fermentation efficiency but also lead to a decrease in the conversion rate, seriously affecting the operation of the fermentation industry. At present, defoaming is mainly carried out by adding defoamers. [0003] At present, the defoamers used for fermentation mainly include silicone defoamers...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01D19/04
CPCB01D19/0413
Inventor 万洪玲
Owner 万洪玲