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Combustion dynamic parameter-based asphalt component thermal stability evaluation method

A thermal stability and evaluation method technology, which is applied in chemical analysis by combustion, scientific instruments, and analytical materials, etc., can solve the problems of difficult simulation of heating rate, poor reliability of asphalt, and difficulty in objectively evaluating the thermal stability of asphalt. The effect of economic and social benefits

Inactive Publication Date: 2018-12-21
NANJING FORESTRY UNIV
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Problems solved by technology

[0012] In view of the fact that the current asphalt four-component thermal stability evaluation method is based on a single heating rate, it is difficult to simulate the variability of the heating rate during an actual fire, the reliability of the calculated combustion kinetic parameters of each component of asphalt is poor, and it is difficult to objectively evaluate the thermal stability of each component of asphalt. The inability to deeply evaluate the combustion dynamics of asphalt from the component level

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Embodiment Construction

[0015] The present invention provides a four-component asphalt thermal stability evaluation method based on combustion kinetic parameters at multiple heating rates, and the specific implementation steps are as follows:

[0016] (1) Separate the four components of saturates, aromatics, colloids and asphaltenes from asphalt, record the content of each component, and conduct industrial analysis and elemental analysis of each component to understand the volatile content of each component , ash, fixed carbon, moisture content, and C, H, N, S element content;

[0017] (2) The thermogravimetric-differential thermal synchronous analyzer is used to carry out thermal analysis tests on each component in an air atmosphere, and three different heating rates of 5°C / min, 10°C / min and 15°C / min are raised from room temperature to 800°C, obtain the TG-DTG curves of each component at different heating rates;

[0018] (3) According to the DTG curves of asphalt components at different heating rat...

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Abstract

The invention relates to a novel method for evaluating asphalt four-component combustion dynamics based on a plurality of heating rates, belongs to the technical field of asphalt materials, and solvesthe problems that the temperature rise rate variability is difficult to simulate in actual fire disaster on the basis of a single heating rate, the reliability in calculation of the combustion dynamics parameters is poor, the thermal stability of all the components of the asphalt is difficult to objectively evaluate, and the asphalt combustion dynamics characteristic cannot be deeply evaluated. The method comprises the following steps of firstly, separating four components from asphalt, and carrying out industrial and element analysis respectively; carrying out thermo-gravimetric analysis inthe air, raising the temperature to 800 DEG C from the room temperature at three temperature rising rates, and obtaining a TG-DTG curve; dividing different combustion stages, and calculating dynamic parameters of different combustion stages by adopting a differential method and an integral method, and carrying out mutual checking; and finally, observing the microscopic morphology of the surface ofthe combustion residue, testing element components and contents, comparing the dynamic parameters of different combustion stages of the asphalt components, evaluating the four-component thermal stability of the asphalt, and disclosing the asphalt combustion characteristic from the component level.

Description

technical field [0001] The invention relates to a four-component asphalt thermal stability evaluation method based on combustion kinetic parameters at multiple heating rates, and belongs to the technical field of asphalt materials. Background technique [0002] Thermal analysis is a technique for measuring the relationship between the physical properties of a substance and the temperature at a programmed temperature. It is mainly used to study physical changes of materials, such as crystal transformation, melting, sublimation, etc., and chemical changes, such as dehydration, decomposition, redox, etc. Thermal analysis provides not only thermodynamic parameters, but also combustion kinetic parameters. Therefore, thermal analysis is of great significance in material research and selection, as well as theoretical research in thermodynamics and kinetics. [0003] Thermal analysis refers to the method of analyzing the relationship between thermodynamic parameters or physical pa...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N25/22G01N23/2251G01N31/12
CPCG01N23/2251G01N25/22G01N31/12
Inventor 夏文静许涛王斯文王宏畅
Owner NANJING FORESTRY UNIV
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