Preparation method of wild jujube effect-developing components for cigarette and application thereof in cigarette

A technology for sour jujube and cigarettes, which is applied to the field of preparation of effective components of sour jujube for cigarettes, can solve the problems of single spice extraction solvent, can not fully exert the function and effect of functional components, etc., and achieves rich tobacco aroma and obvious style characteristics. , enhance the effect of aroma quality

Active Publication Date: 2019-01-01
HUBEI CHINA TOBACCO IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] At present, the development of wild jujube extract still adopts the traditional method of solvent extraction, which has many shortcomings: First, the extraction technology: the spice extraction solvent is single, usually alcohol extraction or water extraction is used, and various components in the spice are extracted at the same time, which cannot be fully utilized. The functions and effects of various non-functional components; second, separation technology: the separation of different components is the key technology to obtain high-efficiency components, but the separation of chemical components with different properties needs to start with selective extraction, and then through chromatographic technology , adsorption technology, centrifugation and other technologies can selectively separate the target components; third, functional identification: there are synergistic, inhibitory and other interactions among the different components in the wild jujube extract, and functional evaluation requires step-by-step separation, or group separation methods to find out step by step. target product

Method used

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  • Preparation method of wild jujube effect-developing components for cigarette and application thereof in cigarette
  • Preparation method of wild jujube effect-developing components for cigarette and application thereof in cigarette
  • Preparation method of wild jujube effect-developing components for cigarette and application thereof in cigarette

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0019] Embodiment 1, a kind of preparation method of effective component of wild jujube for tobacco, is characterized in that comprising the following steps:

[0020] (1) Take a certain amount of wild jujube and carry out supercritical CO 2 Extraction, extraction temperature 56°C, extraction pressure 30Mpa, separation kettle I pressure 10Mpa, separation kettle I temperature 45°C, separation kettle II pressure 4Mpa, separation kettle II temperature 20°C;

[0021] (2) Molecularly distill the jujube supercritical extract in step (1), the distillation temperature is 40°C, the distillation pressure is controlled at 200Pa, the feed rate is 1mL / min, and the scraper speed is 150r / min to obtain the jujube light component;

[0022] (3) Step (1) Jujube supercritical CO 2 The residue after extraction is reflux extracted, the extraction solvent is tap water, the material ratio is 1:4, the extraction time is 3 hours, and the heating temperature is 100°C. After extraction, it is cooled, fil...

Embodiment 2

[0025] Embodiment 2, a kind of preparation method of effective component of wild jujube for tobacco, is characterized in that comprising the following steps:

[0026] (1) Take a certain amount of wild jujube and carry out supercritical CO 2 Extraction, extraction temperature 56°C, extraction pressure 40Mpa, separation kettle I pressure 12Mpa, separation kettle I temperature 45°C, separation kettle II pressure 6Mpa, separation kettle II temperature 25°C;

[0027] (2) Molecularly distill the jujube supercritical extract in step (1), the distillation temperature is 40°C, the distillation pressure is controlled at 400Pa, the feed rate is 2mL / min, and the scraper speed is 150r / min to obtain the jujube light component;

[0028] (3) Step (1) Jujube supercritical CO 2 The residue after extraction is reflux extracted, the extraction solvent is tap water, the material ratio is 1:6, the extraction time is 4 hours, cooled after extraction, filtered, concentrated to a relative density of ...

Embodiment 3

[0031] Embodiment 3, a kind of preparation method of effective component of wild jujube for tobacco, is characterized in that comprising the following steps:

[0032] (1) Take a certain amount of wild jujube and carry out supercritical CO 2 Extraction, extraction temperature 58°C, extraction pressure 35Mpa, separation kettle I pressure 11Mpa, separation kettle I temperature 48°C, separation kettle II pressure 5Mpa, separation kettle II temperature 28°C;

[0033] (2) Molecularly distill the jujube supercritical extract in step (1), the distillation temperature is 50°C, the distillation pressure is controlled at 300Pa, the feed rate is 1.5mL / min, and the scraper speed is 200r / min, to obtain the jujube light component;

[0034] (3) Step (1) Jujube supercritical CO 2 The residue after extraction is heated and reflux extracted, the extraction solvent is tap water, the material ratio is 1:6, the extraction time is 4 hours, cooled after extraction, filtered, concentrated to a relati...

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Abstract

The invention provides a preparation method of wild jujube effect-developing components for a cigarette and application thereof in the cigarette. The preparation method of the wild jujube effect-developing components comprises the following steps: (1) supercritical CO2 extracting; (2) extracting of the wild jujube aroma-causing components by molecule distillation; (3) extracting of wild jujube polysaccharide by water-extracting and sectional alcohol settling; (4) compounding of the wild jujube aroma-causing components and the polysaccharide. The preparation method has the advantages that by adopting the types of gradual separating, sectional enriching and ratio compounding, and combining with supercritical extracting, molecule distillation and sectional alcohol settling techniques, the wild jujube effect-developing components for the cigarette, such as the aroma-causing components and the polysaccharide, are extracted, separated and compounded, so as to complete the refining development and comprehensive utilization of the wild jujube; a kind of wild jujube effect-developing component for cigarette with better cigarette application effect than the traditional wild jujube extract isdeveloped; the aroma of the cigarette is improved and enriched, the flavor feature is obvious, the smoke gas is fine, and the elegant feel is good.

Description

technical field [0001] The invention relates to the preparation of spices for tobacco, in particular to a preparation method of effective components of wild jujube for tobacco and its application in cigarettes. Background technique [0002] Zizyphus jujube is the ripe fruit of jujube jujube in the Rhamnaceae family. Spices such as jujube tincture and extract of wild jujube prepared from jujube have the functions of giving cigarettes a characteristic sour aroma and reducing the irritation of cigarettes, which play an important role in improving the quality of cigarettes. [0003] At present, the traditional method of solvent extraction is still used in the development of wild jujube extract, and there are many shortcomings: First, the extraction technology: the spice extraction solvent is single, usually alcohol extraction or water extraction is used, and various components in the spice are extracted at the same time, which cannot be fully utilized. The functions and effects ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11B9/02A24B3/12
CPCA24B3/12C11B9/025
Inventor 庞登红程书锋程志坤陈胜彭建
Owner HUBEI CHINA TOBACCO IND
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