Preparation method of wild jujube effect-developing components for cigarette and application thereof in cigarette
A technology for sour jujube and cigarettes, which is applied to the field of preparation of effective components of sour jujube for cigarettes, can solve the problems of single spice extraction solvent, can not fully exert the function and effect of functional components, etc., and achieves rich tobacco aroma and obvious style characteristics. , enhance the effect of aroma quality
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0019] Embodiment 1, a kind of preparation method of effective component of wild jujube for tobacco, is characterized in that comprising the following steps:
[0020] (1) Take a certain amount of wild jujube and carry out supercritical CO 2 Extraction, extraction temperature 56°C, extraction pressure 30Mpa, separation kettle I pressure 10Mpa, separation kettle I temperature 45°C, separation kettle II pressure 4Mpa, separation kettle II temperature 20°C;
[0021] (2) Molecularly distill the jujube supercritical extract in step (1), the distillation temperature is 40°C, the distillation pressure is controlled at 200Pa, the feed rate is 1mL / min, and the scraper speed is 150r / min to obtain the jujube light component;
[0022] (3) Step (1) Jujube supercritical CO 2 The residue after extraction is reflux extracted, the extraction solvent is tap water, the material ratio is 1:4, the extraction time is 3 hours, and the heating temperature is 100°C. After extraction, it is cooled, fil...
Embodiment 2
[0025] Embodiment 2, a kind of preparation method of effective component of wild jujube for tobacco, is characterized in that comprising the following steps:
[0026] (1) Take a certain amount of wild jujube and carry out supercritical CO 2 Extraction, extraction temperature 56°C, extraction pressure 40Mpa, separation kettle I pressure 12Mpa, separation kettle I temperature 45°C, separation kettle II pressure 6Mpa, separation kettle II temperature 25°C;
[0027] (2) Molecularly distill the jujube supercritical extract in step (1), the distillation temperature is 40°C, the distillation pressure is controlled at 400Pa, the feed rate is 2mL / min, and the scraper speed is 150r / min to obtain the jujube light component;
[0028] (3) Step (1) Jujube supercritical CO 2 The residue after extraction is reflux extracted, the extraction solvent is tap water, the material ratio is 1:6, the extraction time is 4 hours, cooled after extraction, filtered, concentrated to a relative density of ...
Embodiment 3
[0031] Embodiment 3, a kind of preparation method of effective component of wild jujube for tobacco, is characterized in that comprising the following steps:
[0032] (1) Take a certain amount of wild jujube and carry out supercritical CO 2 Extraction, extraction temperature 58°C, extraction pressure 35Mpa, separation kettle I pressure 11Mpa, separation kettle I temperature 48°C, separation kettle II pressure 5Mpa, separation kettle II temperature 28°C;
[0033] (2) Molecularly distill the jujube supercritical extract in step (1), the distillation temperature is 50°C, the distillation pressure is controlled at 300Pa, the feed rate is 1.5mL / min, and the scraper speed is 200r / min, to obtain the jujube light component;
[0034] (3) Step (1) Jujube supercritical CO 2 The residue after extraction is heated and reflux extracted, the extraction solvent is tap water, the material ratio is 1:6, the extraction time is 4 hours, cooled after extraction, filtered, concentrated to a relati...
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com