A kind of modified succinyl chitosan hydrogel and its preparation method and application
A technology of succinyl chitosan water and succinyl chitosan, which is applied in the field of modified succinyl chitosan hydrogel and its preparation, can solve problems such as insufficient functional properties such as antibacterial and insufficient safety of cross-linking systems, and achieve excellent results. Functional properties, flexible and controllable performance, and the effect of good swelling performance
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Embodiment 1
[0030] Such as figure 1 Shown, a kind of preparation method of modified succinyl chitosan hydrogel is specifically as follows:
[0031] (1) Take 0.80g of succinochitosan and dissolve it in distilled water, and stir it with magnetic force to make it dissolve completely. Another certain amount of 2.0 generation polyamide-amine dendrimers was taken, and the pH was adjusted to 7 with dilute hydrochloric acid to obtain a polyamide-amine dendrimer solution. The two solutions were mixed according to the mass ratio of 2.0-generation polyamidoamine dendrimers to succinyl chitosan at 1:9, and magnetically stirred for 30 minutes until they were evenly mixed. The concentration of succinyl chitosan in the resulting mixed solution is 40g L -1 .
[0032] (2) Add crosslinking agents 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide hydrochloride and N-hydroxysuccinimide to the above mixed solution and stir evenly. Wherein, the molar ratio of 1-ethyl-3-(3-dimethylaminopropyl) carbodiimide hydr...
Embodiment 2
[0036] A kind of preparation method of modified succinyl chitosan hydrogel is specifically as follows:
[0037] (1) Take 0.80g of succinochitosan and dissolve it in distilled water, and stir it with magnetic force to make it dissolve completely. Another certain amount of 2.0 generation polyamide-amine dendrimers was taken, and the pH was adjusted to 7 with dilute hydrochloric acid to obtain a polyamide-amine dendrimer solution. The two solutions were mixed according to the mass ratio of 2.0 generation polyamidoamine dendrimers to succinyl chitosan 5:5, and magnetically stirred for 30 minutes until the mixture was uniform. The concentration of succinyl chitosan in the resulting mixed solution is 40g L -1 .
[0038] (2) Add crosslinking agents 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide hydrochloride and N-hydroxysuccinimide to the above mixed solution and stir evenly. Wherein, the molar ratio of 1-ethyl-3-(3-dimethylaminopropyl) carbodiimide hydrochloride to succinyl chito...
Embodiment 3
[0042] A kind of preparation method of modified succinyl chitosan hydrogel is specifically as follows:
[0043] (1) Take 0.80g of succinochitosan and dissolve it in distilled water, and stir it with magnetic force to make it dissolve completely. Another certain amount of 2.0 generation polyamide-amine dendrimers was taken, and the pH was adjusted to 7 with dilute hydrochloric acid to obtain a polyamide-amine dendrimer solution. The two solutions were mixed according to the mass ratio of 2.0 generation polyamidoamine dendrimers to succinyl chitosan 5:5, and magnetically stirred for 30 minutes until the mixture was uniform. The concentration of succinyl chitosan in the resulting mixed solution is 40g L -1 .
[0044] (2) Add crosslinking agents 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide hydrochloride and N-hydroxysuccinimide to the above mixed solution and stir evenly. Wherein, the molar ratio of 1-ethyl-3-(3-dimethylaminopropyl) carbodiimide hydrochloride to succinyl chito...
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