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Low-pressure leakage layer blocking agent and preparation method thereof

A plugging agent and leakage technology, which is applied in the direction of chemical instruments and methods, drilling compositions, etc., can solve problems such as leakage, serious formation deficit, and poor anti-scourability of slurry, so as to prevent formation leakage and improve plugging The effect of missed success rate

Active Publication Date: 2019-02-12
CNPC BOHAI DRILLING ENG +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] With the continuous deepening of exploration and development of various oilfields, the formation deficit is becoming more and more serious. When drilling into low-pressure layers, leakage occurs frequently, especially when severe leakage occurs in the target layer, the drilling fluid plugging is often ineffective
The density of ordinary acid-soluble cement is difficult to reduce to 1.65g / cm 3 Below, it is easy to cause leakage, and the slurry has poor erosion resistance, so it is difficult to ensure the sealing weight

Method used

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  • Low-pressure leakage layer blocking agent and preparation method thereof
  • Low-pressure leakage layer blocking agent and preparation method thereof

Examples

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Effect test

Embodiment 1

[0018] Weigh sodium bentonite and 1000-1500 mesh blast furnace slag at a weight ratio of 1:9 and mix to obtain 50 parts by weight of cementitious material, 50 parts by weight of limestone powder of 200-500 mesh, 8 parts by weight of sepiolite fiber of 1-2 mm, 0.1 part by weight of a stabilizer formed by mixing azodicarbonamide and p-toluenesulfonylhydrazide at a weight ratio of 1:3 and 1 part by weight of sodium carboxymethylcellulose, and mix it uniformly to obtain a uniformly mixed Solid mixture; take water glass and sodium hydroxide and mix to obtain 10 parts by weight of activator according to the weight ratio of 1:1.5, and add 139 parts of water, stir until completely dissolved, pour into the slurry cup of the corrugated mixer, and start Corrugated agitator motor and maintain a speed of 4000r / min±200r / min, slowly pour the uniformly mixed solid mixture into the mixing cup, stir evenly, and finally cover the lid of the mixing cup, and set the temperature at 12000r / min±500r / m...

Embodiment 2

[0020] Weigh sodium bentonite and 1000-1500 mesh blast furnace slag at a weight ratio of 1:7 to prepare 60 parts by weight of cementitious material, 50 parts by weight of 200-500 mesh limestone powder, and 7 parts by weight of sepiolite fiber of 1-2 mm , 0.1 parts by weight of a stabilizer and 1.5 parts by weight of sodium carboxymethylcellulose mixed by azodicarbonamide and p-toluenesulfonyl hydrazide in a weight ratio of 1:3, and mix it uniformly to obtain a uniform mixture The solid mixture of 1:1.5 by weight takes water glass and sodium hydroxide and mixes the activator that makes 8.5 parts by weight, and adds 125 parts of water, stirs to after dissolving completely, pours in the slurry cup of corrugated stirrer, Start the motor of the corrugated mixer and maintain the speed of 4000r / min±200r / min, slowly pour the evenly mixed solid mixture into the mixing cup, stir evenly, and finally cover the lid of the mixing cup, and set it at 12000r / min±500r Stirring was continued for...

Embodiment 3

[0022] Weigh sodium bentonite and 1000-1500 mesh blast furnace slag at a weight ratio of 1:7 to prepare 75 parts by weight of cementitious material, 60 parts by weight of 200-500 mesh limestone powder, and 5 parts by weight of sepiolite fiber of 1-2 mm , 0.2 parts by weight of a stabilizer mixed with azodicarbonamide and p-toluenesulfonylhydrazide in a weight ratio of 1:3 and 1 part by weight of sodium carboxymethyl cellulose, and mix it uniformly to obtain a uniform mixture The solid mixture of 1:1.3 by weight takes water glass and sodium hydroxide and mixes the activator that makes 9 parts by weight, and adds 135 parts of water, after stirring to fully dissolving, pour in the slurry cup of corrugated stirrer, Start the motor of the corrugated mixer and maintain the speed of 4000r / min±200r / min, slowly pour the evenly mixed solid mixture into the mixing cup, stir evenly, and finally cover the lid of the mixing cup, and set it at 12000r / min±500r Stirring was continued for 35 s ...

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Abstract

The invention discloses a low-pressure leakage layer blocking agent and a preparation method thereof. The blocking agent is prepared by the following steps: dissolving 8.5 to 10 parts of an activatingagent in water for high-speed stirring and dissolving; weighing 50 to 75 parts of a binding material, 50 to 60 parts of a particle bridging material, 5 to 8 parts of a lightening material, 0.1 to 0.2part of a stabilizer and 1 to 1.5 parts of a slurry modifier; uniformly mixing and pouring the mixture into a slurry cup for uniformly stirring; covering the slurry cup with a cup cover; continuallystirring the mixture at the stirring speed of 12000+ / -500 r / min for 35 seconds, wherein the binding material is a mixture of sodium bentonite and blast furnace slag in the weight ratio of 1 to (7 to 9), the particle bridging material is limestone flour, and the lightening material is sepiolite fiber with the particle size of 1 to 2mm. The low-pressure leakage layer blocking agent is 1.2 to 1.4 g / cm<3> in density, and has the advantages of low density, high thixotropy, minimum inflation and high acid dissociation. By adopting the low-pressure leakage layer blocking agent, the problem of leakagedue to difficulty in lowering the density of ordinary acid-dissolved cement below 1.65 g / cm<3> is solved, so that plugging slurry is effectively prevented from pressing the stratum to cause leakage,and the plugging success rate is improved.

Description

technical field [0001] The invention relates to the technical field of leak plugging, in particular to a low pressure leak zone plugging agent and a preparation method thereof. Background technique [0002] With the continuous deepening of exploration and development of various oilfields, the formation deficit is becoming more and more serious. When drilling into low-pressure layers, leakage occurs frequently, especially when severe leakage occurs in the target layer, drilling fluid plugging often cannot be effective. The density of ordinary acid-soluble cement is difficult to reduce to 1.65g / cm 3 Below, it is easy to cause leakage, and the anti-scouring ability of the slurry is poor, so it is difficult to ensure the sealing weight. Contents of the invention [0003] The object of the present invention is to provide a low-pressure leakage layer plugging agent for sealing and temporarily sealing the malignant leakage of the target layer or the malignant leakage of the non-...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09K8/42C09K8/467
CPCC09K8/426C09K8/467C09K2208/08C09K2208/18
Inventor 李秀妹王野王绮杨豫杭张国山曹洪昌郭明红刘泸萍马骏任强李立华赵秋羽张丽华谈占广李海彪肖飞
Owner CNPC BOHAI DRILLING ENG
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