Long-period energy-saving melamine production system

A technology of melamine and production system, applied in the direction of sustainable manufacturing/processing, chemical industry, climate sustainability, etc., which can solve the problems of danger and environmental hazards, large fluctuations in product quality, and restrictions on the long-term stable operation level of melamine production, etc. To achieve the effect of realizing intrinsic safety and environmental protection, ensuring long-term stable operation, and optimizing energy conversion scheme

Inactive Publication Date: 2019-02-22
SHANXI YANGMEI FENGXI FERTILIZER IND GRPCO
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0002] Melamine production processes mainly include Ouzhi high pressure method, DSM low pressure method, and BASF atmospheric pressure gas phase extraction cooling method. Ouzhi high pressure method and DSM low pressure method are stable in operation and good in product quality, but have huge investment and high energy consumption; BASF atmospheric pressure method The gas-phase extraction cooling process and China's improved pressurized gas-phase extraction cooling process have small investment, short process and low energy consumption, but the operation cycle is short, and the product quality fluctuates greatly due to the impact of stopping feeding.
[0003] At present, the domestic production of melamine mainly adopts the BASF atmospheric pressure gas-phase extraction cooling process. In this process, there is fouling of the hot gas cooler tube bundle, periodic switching of standby equipment, and inspection and maintenance of fouling equipment; poor filtration accuracy and efficiency of hot gas filters affect product quality. The surface of the filter bag is clogged and the standby equipment is periodically switched; the melamine wall on the top of the crystallizer 5 causes landslides, affects product quality, and in severe cases leads to problems such as paralysis of the discharging equipment
[0004] In the existing process, the hot gas cooler uses raw oil as the heat exchange medium. The physical and chemical properties of raw oil are toxic, volatile, flammable and explosive, and there are dangers and environmental protection risks in use.
[0005] The above problems have seriously restricted the long-term stable operation level of melamine production. The operation cycle is basically 1-3 months. During the inspection and maintenance process, a large number of work such as unblocking, replacement, and cleaning will be caused. The consumption of auxiliary materials is large, and the labor intensity of workers Large, producing a lot of ground melamine and solid waste

Method used

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Embodiment Construction

[0022] The following clearly and completely describes the technical solutions in the embodiments of the present invention. Obviously, the described embodiments are only some of the embodiments of the present invention, but not all of them. Based on the embodiments of the present invention, all other embodiments obtained by persons of ordinary skill in the art without making creative efforts belong to the protection scope of the present invention.

[0023] like figure 1 As shown, a long-cycle energy-saving melamine production system includes reactor 1, hot gas heat exchanger 2, hot gas separator 3, crystallizer 5, finished product cyclone separator 6, tail gas heat exchanger 8 and tail gas separation 9, the reactor 1 is connected to the instant melting pot 12, and the hot gas separator 3 and the tail gas separator 9 are respectively connected to the slag tank 4. The reactor 1 is connected with the tail gas separator 9 through the carrier gas compressor 11 , the finished produc...

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Abstract

The invention belongs to the technical field of melamine production and in particular relates to a long-period energy-saving melamine production system. The melamine production system comprises a reactor, a hot gas exchanger, a hot gas separator, a crystallizer, a finished cyclone separator, a tail gas exchanger and a tail gas separator connected in sequence, wherein the reactor is connected witha quick melting kettle; and the hot gas separator and the tail gas separator are respectively connected with slag pots. Compared with other processes, the melamine production system disclosed by the invention has the advantages that a liquid urine washing system is removed, standby equipment of a hot gas cooler and a filter is reduced, and investment is less; long-period stable operation is realized, and the period can reach one year or longer; a liquid urine pump, an air-cooling fan and other equipment are reduced, and due to simplified process procedures and an optimized energy conversion scheme, the process energy consumption is low; the energy consumption of ammonia back-flushing is greatly reduced, and the production cost is reduced; the tail gas is clean, equipment corrosion and wallscales can be reduced, and the influence of entrainments on later sections during tail gas utilization can be reduced; and diphenyl ether is not used in the hot gas cooling system, and production ofsolid wastes such as filter bags and the like is reduced.

Description

technical field [0001] The invention belongs to the technical field of melamine production, and in particular relates to a long-period energy-saving melamine production system. Background technique [0002] Melamine production processes mainly include Ouzhi high pressure method, DSM low pressure method, and BASF atmospheric pressure gas phase extraction cooling method. Ouzhi high pressure method and DSM low pressure method are stable in operation and good in product quality, but have huge investment and high energy consumption; BASF atmospheric pressure method The gas-phase extraction cooling process and China's improved pressurized gas-phase extraction cooling process have small investment, short process and low energy consumption, but the operation cycle is short, and the product quality fluctuates greatly due to the impact of stopping feeding. [0003] At present, the domestic production of melamine mainly adopts the BASF atmospheric pressure gas-phase extraction cooling ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C07D251/56
CPCC07D251/56Y02P20/10
Inventor 王敏赵哲军郑保平周伟峰王晓辉
Owner SHANXI YANGMEI FENGXI FERTILIZER IND GRPCO
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