Synthesis method of cyclobutanol nitro-substituted naphthol compound
A synthesis method and compound technology, applied in the preparation of nitro compounds, organic chemistry, etc., can solve the problems of a large number of by-products, low product yield, expensive reagents, etc., and achieve simple operation, high atom economy, and wide application range. Effect
Inactive Publication Date: 2019-02-22
HENAN NORMAL UNIV
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Abstract
The invention discloses a synthesis method of a cyclobutanol nitro-substituted naphthol compound and belongs to the technical field of organic synthesis. The synthesis method of the cyclobutanol nitro-substituted naphthol compound is characterized by comprising the following steps of: dissolving orthoalkynyl substituted phenyl allenyl ketone compound and tert-butyl nitrite in a solvent, and heating in an air atmosphere for a temperature rise reaction to form the cyclobutanol nitro-substituted naphthol compound. The method has the advantages of easiness and simplicity in operation, mild conditions, wide substrate application scope and the like and is suitable for industrial production.
Application Domain
Nitro compound preparation
Technology Topic
Air atmosphereSolvent +5
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