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Preparation method of ice blast base oil with natural pungent and sweet note

A technology of base oil and fragrance, which is applied in the field of preparation of popcorn base oil, can solve the problems of affecting the molding of popcorn, weak aroma of synthetic essence, unstable state of popcorn, etc., and achieves the solution of thin aroma, rich aroma and compatibility good effect

Inactive Publication Date: 2019-03-15
HUBEI CHINA TOBACCO IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the aroma of synthetic flavors is relatively thin, and its chemical properties are active, so it is easy to react with base oil and wall materials, which leads to an unstable state during the online molding process of popping beads, thus affecting the molding of popping beads

Method used

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  • Preparation method of ice blast base oil with natural pungent and sweet note

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0014] Example 1 provides a method for preparing quick-bead base oil with natural pungent and sweet flavor, and the specific steps are as follows:

[0015] (1) Take 100g of the raw material parsnip and 200g of cassia twig, add 10 times the weight of the mixed raw material with tap water, soak at room temperature for 8, then heat to 65°C under normal pressure for reflux extraction for 2h, collect the distillate with a condenser, and separate the oil and water Obtain volatile oil, and then dissolve the volatile oil into polyglycerol fatty acid ester 3000 times its weight;

[0016] (2) Add 0.1‰ of Tween 60 by weight to the mixture obtained in step (1), filter to remove impurities and insolubles. The filtrate is sonicated for 0.5h at a temperature of 30℃ and a frequency of 30kHz. After standing for 2 hours, the quick-bead base oil with natural pungent and sweet fragrance is obtained.

Embodiment 2

[0017] Example 2 provides a method for preparing quick-bead base oil with natural pungent and sweet flavor. The specific steps are as follows:

[0018] (1) Take 200g of the raw materials of parsnips and 100g of cassia twigs, add 8 times the weight of the mixed raw materials in tap water, soak at room temperature for 12, heat to 60℃ under normal pressure and reflux for extraction for 5 hours, collect the distillate with a condenser, and separate the oil and water Obtain the volatile oil, and then dissolve the volatile oil into 5000 times the polyglycerol fatty acid ester;

[0019] (2) Add 0.3‰ of Tween 60 by weight to the mixture obtained in step (1), filter to remove impurities and insolubles, and the filtrate is sonicated for 1h at a temperature of 40°C and a frequency of 35kHz, and then left to stand after the ultrasonic is finished. 4 hours, it is the said base oil for pop pearls with natural sweet fragrance.

Embodiment 3

[0020] Example 3 provides a method for preparing quick-bead base oil with natural pungent and sweet flavor, and the specific steps are as follows:

[0021] (1) Take 200g of raw materials, fenfeng, 200g of cassia twigs, add 6 times the weight of the mixed raw materials with tap water, soak at room temperature for 8, then heat to 55°C under normal pressure for reflux extraction for 4 hours, collect the distillate with a condenser, and separate the oil and water Obtain the volatile oil, and then dissolve the volatile oil into the polyglycerol fatty acid ester 10,000 times its weight;

[0022] (2) Add 0.1‰ of Tween 60 by weight to the mixture obtained in step (1), filter to remove impurities and insolubles. The filtrate is sonicated for 1.5h at a temperature of 50°C and a frequency of 25kHz. Leave it for 24 hours, and it will be the said quick-bead base oil with natural pungent and sweet fragrance.

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Abstract

The invention provides a preparation method of ice blast base oil with natural pungent and sweet note. The preparation method of the ice blast base oil comprises the following specific preparation steps: mixing raw materials of radix saposhnikoviae and ramulus cinnamomi and adding tap water, soaking at room temperature for 8 to 24 hours, heating, refluxing and extracting at normal pressure for 1 to 5 hours, collecting distillate by using a condenser, carrying out oil and water separation to obtain volatile oil, then dissolving the volatile oil into polyglycerol fatty acid ester of which the weight is 1000 to 10000 times that of the volatile oil, adding Tween 60 of which the weight accounts for 0.1 to 1 per mill that of the mixture into the mixture, filtering to remove impurities and insolubles, collecting filtrate, and carrying out ultrasonic treatment at 20 to 60 DEG C or below to obtain the ice blast base oil with the natural pungent and sweet note. The ice blast base oil disclosed by the invention can bring obvious pungent and sweet note, strong aroma, as well as comfortable and nature property by using extremely-low dosage of the radix saposhnikoviae and the ramulus cinnamomi in cigarette ice blast; in addition, the prepared ice blast base oil has good compatibility with a wall material, so that the problems of thin aroma and unstable molding caused by the addition of synthetic spices into the ice blast base oil can be well solved.

Description

Technical field [0001] The invention relates to the field of tobacco flavors and fragrances, and in particular to a method for preparing quick pearl base oil with natural pungent and sweet flavor. Background technique [0002] Blasting pearls is a special process for adding fragrance to cigarette auxiliary materials, and is a major innovation in the tobacco industry. The method of popping pearls to add fragrance improves the safety of cigarette products and greatly enriches the categories of fragrance raw materials. In recent years, major tobacco companies have increased their investment in the research and development of blasted pearls, and launched a large number of their own distinctive pearl-blasted cigarette products. As a brand-new way of flavoring, cigarette blasting has become an innovation in cigarettes in recent years. Important direction. [0003] The flavor used for the base oil of the pearls is basically a synthetic fragrance, which plays an important role in enhancin...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11B9/02A24B15/30A24B3/12
CPCC11B9/02A24B3/12A24B15/30A24B15/302C11B9/022C11B9/027
Inventor 蹇顺华陈胜苗丽坤孙炜炜谭烨
Owner HUBEI CHINA TOBACCO IND
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