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Preparation method of biological adsorbent for treating basic fuchsin in printing and dyeing wastewater

A biosorbent, printing and dyeing wastewater technology, applied in the direction of chemical instruments and methods, adsorption water/sewage treatment, other chemical processes, etc., can solve the problems of poor removal effect, secondary pollution, etc., to achieve the reuse of waste resources, realize The Effect of Economic Circular Development and Environmental Protection

Active Publication Date: 2019-05-17
YUNCHENG UNIVERISTY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0008] The purpose of the present invention is to solve the technical problem that existing adsorbents for treating printing and dyeing sewage have poor removal effect and easily produce secondary pollution, and provide a preparation method for biosorbents for treating basic fuchsin in printing and dyeing wastewater

Method used

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  • Preparation method of biological adsorbent for treating basic fuchsin in printing and dyeing wastewater
  • Preparation method of biological adsorbent for treating basic fuchsin in printing and dyeing wastewater
  • Preparation method of biological adsorbent for treating basic fuchsin in printing and dyeing wastewater

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Embodiment 1

[0026] A kind of preparation method of the biosorbent for treating basic fuchsin in the printing and dyeing wastewater in the present embodiment, its specific steps are as follows:

[0027] 1) Washing: After cleaning the poplar leaves, cut them into 4 cm pieces and soak them in distilled water for 20 minutes;

[0028] 2) Drying: Place the above-mentioned cleaned poplar leaves in a constant temperature drying oven at 70°C and 6.67×10 Pa to dry to constant weight;

[0029] 3) Soaking in hydrochloric acid: put the poplar leaves baked to constant weight into the hydrochloric acid solution of pH=1, and completely soak the poplar leaves for 2 hours;

[0030] 4) Ultrasonic hydrolysis: put the poplar leaves soaked in hydrochloric acid into an ultrasonic instrument for hydrolysis, the ultrasonic power is 200W, the temperature is 70°C, and the time is 10min;

[0031] 5) Salting out: Rinse the ultrasonically treated poplar leaves with distilled water for 3-5 times, then add the filtered...

Embodiment 2

[0071] A kind of preparation method of the biosorbent for treating basic fuchsin in the printing and dyeing wastewater in the present embodiment, its specific steps are as follows:

[0072] 1) Washing: After cleaning the poplar leaves, cut them into 5 cm pieces and soak them in distilled water for 40 minutes;

[0073] 2) Drying: Place the above-mentioned cleaned poplar leaves in a constant temperature drying oven at 80° C. and 6.67×10 Pa to dry to constant weight;

[0074] 3) Soaking in hydrochloric acid: put the poplar leaves baked to constant weight into a hydrochloric acid solution of pH=2, and soak the poplar leaves for 3 hours;

[0075] 4) Ultrasonic hydrolysis: put the poplar leaves soaked in hydrochloric acid into an ultrasonic instrument for hydrolysis, the ultrasonic power is 200W, the temperature is 70°C, and the time is 20min;

[0076] 5) Salting-out: Rinse the ultrasonically treated poplar leaves with distilled water for 3-5 times, then add the filtered poplar lea...

Embodiment 3

[0082] A kind of preparation method of the biosorbent for treating basic fuchsin in the printing and dyeing wastewater in the present embodiment, its specific steps are as follows:

[0083] 1) Washing: After cleaning the poplar leaves, cut them into 2 cm pieces and soak them in distilled water for 10 minutes;

[0084] 2) Drying: Place the above-mentioned cleaned poplar leaves in a constant temperature drying oven at 60°C and 6.67×10 Pa to dry to constant weight;

[0085] 3) Soaking in hydrochloric acid: put the poplar leaves baked to constant weight into a hydrochloric acid solution with pH=0.5, and soak the poplar leaves for 1 hour;

[0086] 4) Ultrasonic hydrolysis: Put the poplar leaves soaked in hydrochloric acid into an ultrasonic instrument for hydrolysis, the ultrasonic power is 200W, the temperature is 70°C, and the time is 5min;

[0087] 5) Salting out: Rinse the ultrasonically treated poplar leaves with distilled water for 3-5 times, then add the filtered poplar lea...

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Abstract

The invention relates to a preparation method of a biological adsorbent for treating basic fuchsin in printing and dyeing wastewater, belongs to a production method of an environment-friendly originalecological green biological adsorbent, and aims to solve the technical problems that an existing adsorbent for treating printing and dyeing wastewater has poor removal effect and is liable to producesecondary pollution. The technical scheme is characterized in that the preparation method of the biological adsorbent for treating basic fuchsin in the printing and dyeing wastewater comprises the following specific steps: 1) washing; 2) drying; 3) soaking in hydrochloric acid; 4) ultrasonic hydrolysis; 5) salting out; 6) soaking in hydrogen peroxide; 7) soaking in ethanol; 8) drying; 9) pulverizing. The preparation method has the advantages that waste resources are reused, adsorption effect is good, secondary pollution is unlikely to produce and the like.

Description

technical field [0001] The invention relates to a preparation method of a biosorbent for treating basic fuchsin in printing and dyeing wastewater, which belongs to an environment-friendly production method of original ecological green biosorbent. Background technique [0002] Printing and dyeing wastewater contains a large amount of dyes, pastes, inorganic salts, oils, acids and bases, and fiber impurities. These impurities pollute the water body mainly in three aspects. First, it reduces the transparency of the water body, making it difficult for plants in the water to perform photosynthesis. Second, it can reduce the amount of dissolved oxygen in the water, making it difficult for aerobic organisms in the water to survive. The last pollutants are highly toxic and can seriously impair the health of organisms that absorb them into their bodies. [0003] As a traditional landscaping tree species in the north, poplar has the characteristics of strong adaptability, strong resi...

Claims

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Application Information

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IPC IPC(8): B01J20/24B01J20/30C02F1/28
Inventor 李新陈莉
Owner YUNCHENG UNIVERISTY
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