Non-phosphorus antisludging agent containing tracer polymer and preparation method of non-phosphorus antisludging agent

A phosphorus-free scale inhibitor and polymer technology, which is applied in chemical instruments and methods, scale removal and water softening, water/sludge/sewage treatment, etc. The release effect is reduced, the stability of the tracer is poor, etc., and the effects of easy monitoring and dosage, significant social benefits, economic promotion value, and low cost are achieved.

Inactive Publication Date: 2019-05-17
URUMQI KEFAZHAN FINE CHEM
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, for water with high alkalinity and high hardness, the scale inhibition ability and slow release effect are significantly reduced, and the stability to zinc salts is weak
In the daily use of chemicals, the concentration of chemicals is monitored by adding tracers, but the tracers added in traditional phosphorus-free antiscalants have poor stability and cannot correctly reflect the concentration of chemicals in water quality

Method used

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  • Non-phosphorus antisludging agent containing tracer polymer and preparation method of non-phosphorus antisludging agent
  • Non-phosphorus antisludging agent containing tracer polymer and preparation method of non-phosphorus antisludging agent

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0009] Embodiment 1. A phosphorus-free scale inhibitor containing a tracer polymer, which is formulated in parts by weight from the following raw materials: (1) 15 parts of AA / AHPSE; (2) 2.2 parts of zinc chloride; (3) 3.8 parts of polyaspartic acid; (4) 1 part of sulfuric acid; (5) 1 part of triethanolamine; (6) 3 parts of polyepoxysuccinic acid; (7) 4 parts of sodium gluconate; 5 parts of hydrogen oxide; (9) 1.5 parts of tracer PTSA; (10) the balance of pure water.

[0010] Preparation method: use a pump to batch the claims (1), (2), (3), (5), and (7) sequentially; pump the raw materials (6), (8) (10) into the reaction kettle for Stir and heat, stir for about 1 hour, heat the temperature to 60°C-80°C, then pump the prepared (1), (2), (3), (5), and (7) into the reaction kettle, the temperature Keep it between 60°C-65°C, stir for 2-3 hours, adjust the pH value of the solution through (4), control the pH between 6.5-8.5, and keep stirring for 30 minutes; finally add the raw ma...

Embodiment 2

[0011] Embodiment 2, a phosphorus-free scale inhibitor containing a tracer polymer, which is prepared from the following raw materials in parts by weight: (1) 10 parts of AA / AHPSE; (2) 1 part of zinc chloride; (3) 3 parts of polyaspartic acid; (4) 3 parts of sulfuric acid; (5) 2.5 parts of triethanolamine; (6) 5 parts of polyepoxysuccinic acid; (7) 5 parts of sodium gluconate; 10 parts of hydrogen oxide; (9) 1 part of tracer PTSA; (10) the balance of pure water.

[0012] The preparation method is the same as in Example 1.

Embodiment 3

[0013] Embodiment 3, the phosphorus-free antiscalant that contains tracer polymer, this antiscalant is formulated by weight parts by following raw material: (1) AA / AHPSE 25 parts; (2) Zinc chloride 3 parts; (3) 6 parts of polyaspartic acid; (4) 1 part of sulfuric acid; (5) 2 parts of triethanolamine; (6) 2 parts of polyepoxysuccinic acid; (7) 2 parts of sodium gluconate; 8 parts of hydrogen oxide; (9) 3 parts of tracer PTSA; (10) the balance of pure water.

[0014] The preparation method is the same as in Example 1.

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Abstract

The invention belongs to the technical field of water treatment, and particularly discloses a non-phosphorus antisludging agent containing tracer polymer and a preparation method of the non-phosphorusantisludging agent. The antisludging agent is prepared from the following raw materials: (1) AA/AHPSE; (2) zinc chloride; (3) polyaspartic acid; (4) organic amine; (5) triethanolamine; (6) polyepoxysuccinic acid; (7) sodium gluconate; (8) hydrogen peroxide; (9) a tracer agent PTSA; and (10) the balance of pure water. The prepared non-phosphorus antisludging agent containing tracer polymer is a water treatment antisludging agent having the good effect, low cost, high antisludging capability, and capable of being monitoring adding and usage conveniently, and has oustanding social benefits andeconomic popularization value.

Description

technical field [0001] The invention belongs to the technical field of water treatment, and specifically discloses a phosphorus-free scale inhibitor containing a tracer polymer and a preparation method thereof. Background technique [0002] At present, most of the traditional phosphorus-free scale inhibitors sold in the market are AA / AMPS (acrylic acid / 2-acrylamide-2-methylpropanesulfonic acid). Traditional phosphorus-free scale inhibitors have acceptable scale inhibition ability for water with general alkalinity and hardness. However, for water with high alkalinity and high hardness, the scale inhibition ability and slow release effect are obviously reduced, and the stability of zinc salt is weak. In the daily use of chemicals, the concentration of chemicals is monitored by adding tracers, but the tracers added in traditional phosphorus-free antiscalants have poor stability and cannot correctly reflect the concentration of chemicals in water quality. Therefore, the resear...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C02F5/12
Inventor 何晶基杨桂萍
Owner URUMQI KEFAZHAN FINE CHEM
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