Preparation method for high-temperature lightweight tough mullite aggregate
A technology for mullite and high temperature, applied in applications, household utensils, ceramic products, etc., to avoid brittle fracture, reduce the introduction of impurity elements, and improve thermal insulation performance
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Embodiment 1
[0031] In parts by weight, 45 parts of mullite powder, 15 parts of microsilica powder with a mass fraction of 94.0%, 40 parts of soft clay, and 0.2 parts of water reducer are mixed with water, and the stirring speed is 500r / min. Mix well to form a homogeneous slurry.
[0032] Add 10 parts of TR-WLFP and 0.3 parts of foam stabilizer to the homogeneous slurry. The stirring steps are as follows: Step 1: The stirring speed is 700r / min, and the stirring time is 8 minutes;
[0033] The second step: the stirring speed is 400r / min, and the stirring time is 3min;
[0034] After the foaming slurry is prepared, the stirring speed is controlled at 200 r / min, 10 parts of chopped refractory fibers and 15 parts by mass of silica sol are added, and stirring is continued for 3 minutes. The prepared fiber composite foam slurry was poured into a mold, placed in a drying oven at 70°C for 8 hours, and then the temperature of the oven was increased to 110°C. After being dried for 12 hours, it was ...
Embodiment 2
[0036] In parts by weight, 45 parts of mullite powder, 15 parts of microsilica powder with a mass fraction of 94.0%, 40 parts of soft clay, and 0.2 parts of water reducer are mixed with water, and the stirring speed is 500r / min. Mix well to form a homogeneous slurry.
[0037] Add 20 parts of TR-WLFP and 0.2 parts of foam stabilizer to the homogeneous slurry. The stirring steps are as follows: Step 1: The stirring speed is 700r / min, and the stirring time is 8 minutes;
[0038] The second step: the stirring speed is 400r / min, and the stirring time is 3min;
[0039] After the foaming slurry is prepared, the stirring speed is controlled at 200 rad / min, 10 parts of chopped refractory fibers and 15 parts by mass of aluminum sol are added, and stirring is continued for 3 minutes. The prepared fiber composite foam slurry was poured into a mold, placed in a drying oven at 70°C for 8 hours, and then the temperature of the oven was increased to 110°C. After being dried for 12 hours, it ...
Embodiment 3
[0041] In parts by weight, 45 parts of mullite powder, 15 parts of microsilica powder with a mass fraction of 94.0%, 40 parts of soft clay, and 0.2 parts of water reducer are mixed with water, and the stirring speed is 500r / min. Mix well to form a homogeneous slurry.
[0042] Add 25 parts of TR-WLFP and 0.2 parts of foam stabilizer to the homogeneous slurry. The stirring steps are as follows: the first step: the stirring speed is 700r / min, and the stirring time is 8min;
[0043] The second step: the stirring speed is 400r / min, and the stirring time is 3min;
[0044] After the foaming slurry is prepared, control the stirring speed at 200 rad / min, add 10 parts of chopped refractory fiber, 10 parts by mass of aluminum sol and 5 parts by mass of silica sol, and continue stirring for 3 minutes. The prepared fiber composite foam slurry was poured into a mold, placed in a drying oven at 70°C for 8 hours, and then the temperature of the oven was increased to 110°C. After being dried ...
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