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33results about How to "Long bubble time" patented technology

Composite fiber reinforced foam concrete and preparation method thereof

The invention relates to composite fiber reinforced foam concrete and a preparation method thereof. The foam concrete comprises the following components in parts by weight: 0-400 parts of fly ash, 100-900 parts of cement, 500-1000 parts of sands, 300-600 parts of water, 0.4-1 part of organic fiber, 1-3 parts of plant fiber, 0.2-15 parts of early strength agent, 3-20 parts of foaming agent, 0.5-4 parts of water reducing agent and 0.5-2 parts of water retention agent. The preparation method of the foam concrete comprises the following steps of: generating foams by using the foaming agent, adding the foams to fully stirred cement mortar containing composite fibers and the like and keeping stirring so that the foams are dispersed in the mortar uniformly, measuring the volume weight and carrying out casting forming or coating forming and carrying out standard curing for 28 days. In the invention, industrial and agricultural wastes, such as fly ash, plant fiber and the like, are used, shrinkage crack of the foam concrete is inhibited obviously, and the composite fiber reinforced foam concrete has low price; and the foam concrete has simple formula, good workability, long foam stabilizing time, light weight and low coefficient of thermal conductivity and is suitable for exterior wall thermal insulation, roof thermal insulation and non-load-bearing wall manufacturing.
Owner:TONGJI UNIV

Sasanqua saponin concrete air entraining agent and preparation method thereof

The invention provides a sasanqua saponin concrete air entraining agent and a preparation method thereof. The air entraining agent is characterized by containing sasanqua saponin therein. The preparation method is characterized by extracting sasanqua as a raw material at normal temperature by hydrophilic solvent water solution, and filtering; removing large-molecule impurities from the filtrate by membrane separation under pressure, removing small-molecule impurities by membrane separation, concentrating to be concentrate with Baume degree of not lower than 10Be (60 DEG C), and spray-drying to form solid formulation; or adding a modifying agent to prepare the air entraining agent in liquid formulation. The idea is novel, the raw materials are abundant, the production efficiency is high, the energy consumption in the production is low, the production cost is low, the preparation method is simple in process, green and environment-friendly and is convenient to implement; when the air entraining agent is used in concrete engineering, the dosage of the air entraining agent is low, the air production rate is high, the aperture of the entrained air bubbles is small and the distance among the entrained air bubbles is small, and the air holes of the concrete are more even, more compact and non-communicated, therefore, the sasanqua saponin concrete air entraining agent is valuable for popularizing.
Owner:FUZHOU UNIV

Camellia saponin type oilfield foaming agent and preparation method and application thereof

The invention relates to a camellia saponin type oilfield foaming agent and a preparation method and application thereof. The oilfield foaming agent comprises the following components in part by mass: 100 parts of camellia saponin based on the solid content, 1 to 10 parts of cocoanut oil diethanol amide, 1 to 10 parts of amine ether alkyl glucoside, 1 to 10 parts of dodecyl betaine, and 0.5 to 2 parts of lauryl dimethy amine oxide, wherein the camellia saponin is natural plant source camellia saponin or structure-modified camellia saponin. The camellia saponin type oilfield foaming agent is used as an oilfield foaming agent in oil recovery, has the characteristics of acid, alkali and salt resistance, temperature resistance, high foam expansion ratio, long stable foam time and the like, can meet oil extraction requirements under different geological and weather conditions, cannot pollute an oilfield soil layer employing the foaming agent, can prevent a chemically synthesized foaming agent from harming the oilfield stratum, and has remarkable environmental protection characteristic.
Owner:青田中野天然植物科技有限公司

Structural modification type cameclia oleifera saponin and preparation method and application thereof

The invention discloses structural modification type cameclia oleifera saponin, which is prepared by the following method: stirring cameclia oleifera saponin and normal butanol at room temperature and carrying out an esterification reaction under the action of 4-dmethylamino pyridine as a catalyst and N-dicyclohexylcarbodiimide as a dehydrating agent; tracking and detecting to complete reaction; adding fatty alcohol and stirring at room temperature and reacting for 2-5 hours; heating to 70-100DEG C; controlling the reaction pressure to be 0.005-0.015MPa; stirring and carrying out an ester exchange reaction, tracking and detecting to complete reaction; filtering reaction liquid; washing filtrate B; drying and then filtering an organic layer to obtain filtrate C; carrying out reduced pressure distillation to recover the normal butanol; and obtaining a remainder which is the structural modification type cameclia oleifera saponin. The structural modification type cameclia oleifera saponinhas the characteristics of high foaming multiplying power, long foam stabilizing time and the like and can be used as a matrix raw material of an oil filed foaming agent; and the oil filed foaming agent synthesized by matching and optimizing has the performances of resisting acid, alkali, temperature and salt and capability of meeting the oil extracting requirements under different conditions.
Owner:江西新中野茶业科技有限公司

Environment-friendly compound concrete foaming agent and preparation method thereof

The invention discloses an environment-friendly compound concrete foaming agent and a preparation method thereof. The environment-friendly compound concrete foaming agent comprises the following components: sodium alpha-olefin sulfonate, alkyl glycoside, methyl ester sulfonate, cocamidopropyl betaine, tea saponin, arabic gum, hydroxypropyl methyl cellulose, gelatin, polyanionic cellulose, polyvinyl alcohol and sodium bentonite. The environment-friendly compound concrete foaming agent disclosed by the invention is alkalescent, achieves the pH value of 7-9, has the advantages of high foaming power, large foam expansion, fine uniform and tough foam, durability, stability, long foam stabilizing time, small bleeding amount, small deposition amount, good hard water resistance and suitability for water with various rigidities.
Owner:深圳市中天元实业有限公司

Multifunctional liquid foam used for underground coal mine and using method thereof

The invention belongs to the technical field of coal mine safety, and patricianly relates to multifunctional liquid foam used for an underground coal mine and a using method of the multifunctional liquid foam. The multifunctional liquid foam used for the underground coal mine comprises, by mass, 0.5-10% of crystal whisker stopping agents, 0.5-30% of quaternary ammonium salt cationic surface active agents, 0.5-30% of non-ionic surface active agents and 0-10% of additives, the balance of water. The multifunctional liquid foam preparation method and using method are simple, bring convenience for use and manual operation, and are strong in applicability because of being suitable for mines rich in acid gases like sulfuretted hydrogen and sulfur dioxide, tunnels with large coal spontaneous combustion tendency, mine working faces and the like and particularly suitable for mine goaves.
Owner:LIAONING TECHNICAL UNIVERSITY

Oil-proof sustained-release solid foaming drainage agent used for gas wells, and preparation method and applications thereof

The invention discloses an oil-proof sustained-release solid foaming drainage agent used for gas wells, and a preparation method and applications thereof. The oil-proof sustained-release solid foaming drainage agent is mainly used for solving problems of conventional solid foaming drainage agents that high local concentration and waste are caused because of high dissolving speed, and preferable application is different to realize when gas well output water is high in gas condensate content, high in mineralization degree, and high in temperature. The dissolving time of the oil-proof sustained-release solid foaming drainage agent at 90 DEG C formation water condition is longer than 72h, and agent effect lasting time is long; the oil-proof sustained-release solid foaming drainage agent is capable of resisting gas condensate of 50% or higher, temperature of 120 DEG C or higher, and mineralization degree of 250000ppm; the foaming power is equal to or larger than 140mm; foam stabilizing time is long; and compatibility with agents such as methyl alcohol, corrosion inhibitors, and scale inhibitors is high. The preparation method is simple; no environment pollution is caused; no chemical reaction of products with gas and liquid ingredients is caused; equipment or pipeline corrosion is not caused; the prominent problems of gas wells are solved; and the oil-proof sustained-release solid foaming drainage agent is suitable for a plurality of water-producing gas wells.
Owner:四川锦盛油田技术服务有限公司

Anti-collapse and anti-leakage drilling washing fluid used during drilling and field production method thereof

The invention discloses an anti-collapse and anti-leakage drilling washing fluid used during drilling and a field production method thereof, belongs to the technical field of geological core drilling technology, and aims to solve the problem that drilling washing fluid is poor in wall protecting effect under the stratum conditions of strong breaking and continuous leakage. The drilling washing fluid is characterized in that 30-50kg of bentonite, 2-4kg of soda ash, 2-5kg of tackifier, 20-50kg of fluid loss agent, 5-15kg of flow pattern regulator, 30-80kg of bridging agent, 20-50kg of blocking agent, 10-30kg of inhibitor and 1-3L of foaming agent are added to each cubic meter of water. The anti-collapse and anti-leakage drilling washing fluid has the advantages that the drilling washing fluid is good in collapse preventing effect, fast in leakage blocking, high in leakage blocking strength, wide in adaptive crack width range, and widely applicable to the drilling of water-sensitive and loose and broken stratums, low-pressure leakage layers and fracture hole developed stratums.
Owner:INST OF EXPLORATION TECH OF CHINESE ACAD OF GEOLOGICAL SCI

Preparation method and application of lauramide concrete foaming agent

The invention discloses a preparation method and an application of a lauramide concrete foaming agent. The method is characterized in that: lauric acid and hydroxyethylethylene diamine with a molar ratio of 1.0:1.0-1.5 are added into a reaction vessel, a solvent toluene is added, and the mixture is subject to a reaction for 2 to 5 hours under a temperature of 140 to 160 DEG C; the mixture is cooled, and a crude product of a yellow solid is obtained; the crude product is washed by using anhydrous acetone, and is dried, such that a white powdery solid is obtained, wherein the solid is an intermediate; the intermediate, chloroacetic acid and sodium hydroxide are formulated according to a molar ratio of 1:1.0-1.3:2.0-2.6; chloroacetic acid and sodium hydroxide are dissolved in water, such that a sodium monochloroacetate solution with a mass percent concentration of 10 to 20% is prepared; the intermediate is heated to 80 to 90 DEG C until melted, the sodium monochloroacetate solution is dropped into the intermediate, and the mixture is then subject to a reaction for 3 to 5 hours with maintained temperature; the mixture is cooled and filtered, insoluble substances are discarded, and the filtrate is the lauramide concrete foaming agent with excellent foaming performance.
Owner:SOUTHWEAT UNIV OF SCI & TECH

Ultralight building material and its producing method

The invention relates to an ultra-light building material which consists of driers, extravasation materials, foaming agents and water and is characterized in that the driers consist of cement which is 10 to 15 percent of the total weight of the driers and semi-hydrated gypsum which is 85 to 90 percent of the total weight of the driers; the extravasation materials consist of an efficient water reducing agent which is 1 to 3 thousandth of the total weight of the driers, a retarder for plaster which is 2 to 4 thousandth of the total weight of the driers, polyvinyl propyl ethernamine which is 0.5 to 1.0 thousandth of the total weight of the driers and anti-cracking fiber which is 1.0 to 1.5 thousandth of the total weight of the driers; the foaming agents is 5 to 6 percent of the total weight of the driers; the weight ratio of the driers to water is 1:0.6 to 1:0.65. The invention also discloses a manufacturing method of the material. The building material is characterized by good mixture workability, easy foam adding and stabilizing and high foaming efficiency.
Owner:GANSU BUILDING MATERIALS DESIGN & RES INST CO LTD

Concrete and air entraining agent used at high-cold and high-altitude areas, and preparation method thereof

The invention provides a concrete and an air entraining agent which are used at high-cold and high-altitude areas, and a preparation method thereof. 100% of the air entraining agent is prepared from,by weight, 92 to 95% of a triterpenoid saponin solution, 1.8 to 2.8% of modified polybutadiene resin, 0.7 to 0.95% of modified polyacrylamide, 2.5 to 4.25% of sodium carbonate. Compared with conventional used triterpenoid saponin air entraining agents, water soluble resin modified polybutadiene resin and water soluble ion polymer modified polyacrylamide are added; the triterpenoid saponin possesses carbohydrate chains, is high in hydrophilic performance, and is capable of combining with modified polyacrylamide, so that bubble wall strength is increased, foaming is stabilized, bubble diameter is reduced, bubble film viscosity and strength are increased, and after bubble formation, the liquid film possesses enough continuity and elasticity.
Owner:CHANGAN UNIV

Preparation method for high-temperature lightweight tough mullite aggregate

The invention relates to a preparation method for a high-temperature lightweight tough mullite aggregate. According to the technical scheme, the preparation method comprises the following steps: mixing 40-65 parts of mullite powder, 5-25 parts of 94.5% silica powder, 20-55 parts of soft clay and 0.3-0.5 part of water reducer in parts by weight with water while stirring at a stirring rate of 500 rad / min, thereby fully mixing main materials and forming into a uniform slurry; adding 10-40 parts of foaming agent and 0.1-0.6 part of foam stabilizer into the uniform slurry. According to the invention, a manner of one-step foaming is combined with a unique stirring process, for fully and uniformly distributing the foaming agent into the slurry and lastly forming a foam slurry; the production process is simple and practicable; volume density of aggregate body is 0.5kg / m3-0.6kg / m3; volume density of sintered aggregate is 0.3kg / m3-0.4kg / m3.
Owner:RUITAI MATERIALS TECHNOLOGY CO LTD

Method for preparing expanded asphalt

The invention discloses a method for preparing expanded asphalt, and belongs to the technical field of materials for paving pavements. The method comprises the following steps: performing a heat insulation reaction on a functional assistant, a sodium silicate solution, water and crushed asphalt at a lower temperature, rising the temperature, performing heat insulation foaming, lowering the temperature to room temperature, adding isocyanate, and continuously performing stirring and reacting to obtain the expanded asphalt, wherein the functional assistant is obtained by mixing a self-made emulsified dispersion, polyethyleneimine and a crosslinking agent, and carbon dioxide is continuously introduced into the system in the mixing process; and the emulsified dispersion is formed by octenyl succinic acid modified starch, enzymatically hydrolyzed chitosan, water and linoleic acid. The expanded asphalt prepared in the invention has the characteristics of excellent mechanical properties, prolonged foam stabilizing time and effectively improved bonding strength.
Owner:周荣

A kind of environment-friendly composite concrete foaming agent and preparation method thereof

The invention discloses an environment-friendly compound concrete foaming agent and a preparation method thereof. The environment-friendly compound concrete foaming agent comprises the following components: sodium alpha-olefin sulfonate, alkyl glycoside, methyl ester sulfonate, cocamidopropyl betaine, tea saponin, arabic gum, hydroxypropyl methyl cellulose, gelatin, polyanionic cellulose, polyvinyl alcohol and sodium bentonite. The environment-friendly compound concrete foaming agent disclosed by the invention is alkalescent, achieves the pH value of 7-9, has the advantages of high foaming power, large foam expansion, fine uniform and tough foam, durability, stability, long foam stabilizing time, small bleeding amount, small deposition amount, good hard water resistance and suitability for water with various rigidities.
Owner:深圳市中天元实业有限公司

A kind of anti-oil slow-release solid foam drainage agent for gas well, its preparation method and application

The invention discloses an oil-proof sustained-release solid foaming drainage agent used for gas wells, and a preparation method and applications thereof. The oil-proof sustained-release solid foaming drainage agent is mainly used for solving problems of conventional solid foaming drainage agents that high local concentration and waste are caused because of high dissolving speed, and preferable application is different to realize when gas well output water is high in gas condensate content, high in mineralization degree, and high in temperature. The dissolving time of the oil-proof sustained-release solid foaming drainage agent at 90 DEG C formation water condition is longer than 72h, and agent effect lasting time is long; the oil-proof sustained-release solid foaming drainage agent is capable of resisting gas condensate of 50% or higher, temperature of 120 DEG C or higher, and mineralization degree of 250000ppm; the foaming power is equal to or larger than 140mm; foam stabilizing time is long; and compatibility with agents such as methyl alcohol, corrosion inhibitors, and scale inhibitors is high. The preparation method is simple; no environment pollution is caused; no chemical reaction of products with gas and liquid ingredients is caused; equipment or pipeline corrosion is not caused; the prominent problems of gas wells are solved; and the oil-proof sustained-release solid foaming drainage agent is suitable for a plurality of water-producing gas wells.
Owner:四川锦盛油田技术服务有限公司

Camellia saponin type oilfield foaming agent and preparation method and application thereof

The invention relates to a camellia saponin type oilfield foaming agent and a preparation method and application thereof. The oilfield foaming agent comprises the following components in part by mass: 100 parts of camellia saponin based on the solid content, 1 to 10 parts of cocoanut oil diethanol amide, 1 to 10 parts of amine ether alkyl glucoside, 1 to 10 parts of dodecyl betaine, and 0.5 to 2 parts of lauryl dimethy amine oxide, wherein the camellia saponin is natural plant source camellia saponin or structure-modified camellia saponin. The camellia saponin type oilfield foaming agent is used as an oilfield foaming agent in oil recovery, has the characteristics of acid, alkali and salt resistance, temperature resistance, high foam expansion ratio, long stable foam time and the like, can meet oil extraction requirements under different geological and weather conditions, cannot pollute an oilfield soil layer employing the foaming agent, can prevent a chemically synthesized foaming agent from harming the oilfield stratum, and has remarkable environmental protection characteristic.
Owner:青田中野天然植物科技有限公司

Method for preparing novel composite concrete air entraining agent

The invention discloses a method for preparing a novel composite concrete air entraining agent. The novel composite concrete air entraining agent is prepared from 5%-15% of dodecyl dimethylamine, 5%-15% of sodium ethoxylated alkyl sulfate, 5%-10% of sodium abietate, 5%-15% of coconut oil diethanolamide and the balance water. According to the method, the materials with different components for airentraining, bubble stabilizing, plastification and the like are compounded to be used for perfecting the application performance of concrete, the novel composite concrete air entraining agent is liquid, can be dissolved in water, and can be diluted into the liquid with the concentration of 1.5%-2.0% in a stirring station to be automatically metered and added. The novel composite concrete air entraining agent can be used when a finished additive is compounded, the compounding performance of the product and other concrete additives is good, the amount of admixture is small, the compounding effect is superior to that of a deltonin air entraining agent, the surface tension of a solution can be effectively reduced, and sealed and independent bubbles are generated. The advantages of being high in foaming rate, small in bubble diameter and bubble stabilizing time are achieved, and the work performance of the concrete and the concrete flowing slump loss resistant performance can be obviously improved.
Owner:湖南加美乐素新材料股份有限公司

Anti-freezing green vegetation concrete and preparation method thereof

The invention relates to the field of concrete, and particularly discloses anti-freezing green vegetation concrete and a preparation method thereof.The anti-freezing green vegetation concrete is prepared from, by weight, 200-300 parts of cement, 60-80 parts of kieselguhr, 300-380 parts of aggregate, 60-100 parts of soil, 10-20 parts of composite fibers, 1-2.5 parts of air entraining agent, 4-10 parts of water reducing agent and 120-160 parts of water; the air entraining agent is prepared from the following components in parts by weight: 20 to 35 parts of rosin powder, 8 to 14 parts of nekal, 12 to 16 parts of melamine, 5 to 15 parts of sulfuric acid, 10 to 20 parts of sodium hydroxide and 12 to 18 parts of polyethylene glycol. The anti-freezing green vegetation concrete disclosed by the invention has relatively good anti-freezing performance.
Owner:杭州汉特建材有限公司

Preparation method for compound type foaming agent

The invention discloses a preparation method for a compound type foaming agent, relates to a preparation method for an additive for a building, in particular to a preparation method for a foaming agent added into concrete. The compound type foaming agent is compounded from an initial product, N,N'-dinitrosopentamethylamine (DPT), diglycol and lauryl alcohol. The compound type foaming agent is prepared on the basis of the original foaming agent, substances with excellent foaming properties are added into the foaming agent, and other additives are added to achieve the effects of increasing foams, stabilizing foams and regulating. The compound type foaming agent prepared by the preparation method is verified in practical production, and has the outstanding characteristics of being great in foaming amount, small in foam loss, small in strength effect and the like. The preparation method is simple to operate, is easy to control and is relatively high in yield.
Owner:云南森博混凝土外加剂有限公司

A kind of multifunctional liquid foam used in underground coal mine and its application method

The invention belongs to the technical field of coal mine safety, and patricianly relates to multifunctional liquid foam used for an underground coal mine and a using method of the multifunctional liquid foam. The multifunctional liquid foam used for the underground coal mine comprises, by mass, 0.5-10% of crystal whisker stopping agents, 0.5-30% of quaternary ammonium salt cationic surface active agents, 0.5-30% of non-ionic surface active agents and 0-10% of additives, the balance of water. The multifunctional liquid foam preparation method and using method are simple, bring convenience for use and manual operation, and are strong in applicability because of being suitable for mines rich in acid gases like sulfuretted hydrogen and sulfur dioxide, tunnels with large coal spontaneous combustion tendency, mine working faces and the like and particularly suitable for mine goaves.
Owner:LIAONING TECHNICAL UNIVERSITY

A kind of preparation method of temperature-resistant and salt-resistant foam discharge agent

The invention discloses a preparation method of a temperature-resistant and salt-resistant foam discharge agent, which comprises the following steps: adding sodium fatty acid methyl ester sulfonate into a three-necked flask, heating and melting; introducing nitrogen gas to discharge oxygen, and then adding N,N-2 Methyl-1,3-propylenediamine; then condensed and refluxed, stirred evenly and reacted to obtain a solid; the obtained solid was recrystallized with sodium chloride solution, filtered, and dried to obtain the foam discharge agent. The synthetic foam release agent of the present invention has low raw material price, convenient source, simple synthesis operation, easy control, and high yield. Compared with the conventional foam release agent, the dosage is less, the foaming foam is rapid, the foaming volume is large, the foam is delicate and The bubble stabilization time is long, which saves resources and reduces costs.
Owner:SOUTHWEST PETROLEUM UNIV +1

A kind of anti-collapse and anti-leakage drilling flushing fluid while drilling and on-site preparation method thereof

The invention discloses an anti-collapse and anti-leakage drilling washing fluid used during drilling and a field production method thereof, belongs to the technical field of geological core drilling technology, and aims to solve the problem that drilling washing fluid is poor in wall protecting effect under the stratum conditions of strong breaking and continuous leakage. The drilling washing fluid is characterized in that 30-50kg of bentonite, 2-4kg of soda ash, 2-5kg of tackifier, 20-50kg of fluid loss agent, 5-15kg of flow pattern regulator, 30-80kg of bridging agent, 20-50kg of blocking agent, 10-30kg of inhibitor and 1-3L of foaming agent are added to each cubic meter of water. The anti-collapse and anti-leakage drilling washing fluid has the advantages that the drilling washing fluid is good in collapse preventing effect, fast in leakage blocking, high in leakage blocking strength, wide in adaptive crack width range, and widely applicable to the drilling of water-sensitive and loose and broken stratums, low-pressure leakage layers and fracture hole developed stratums.
Owner:INST OF EXPLORATION TECH OF CHINESE ACAD OF GEOLOGICAL SCI

Structural modification type cameclia oleifera saponin and preparation method and application thereof

The invention discloses structural modification type cameclia oleifera saponin, which is prepared by the following method: stirring cameclia oleifera saponin and normal butanol at room temperature and carrying out an esterification reaction under the action of 4-dmethylamino pyridine as a catalyst and N-dicyclohexylcarbodiimide as a dehydrating agent; tracking and detecting to complete reaction; adding fatty alcohol and stirring at room temperature and reacting for 2-5 hours; heating to 70-100DEG C; controlling the reaction pressure to be 0.005-0.015MPa; stirring and carrying out an ester exchange reaction, tracking and detecting to complete reaction; filtering reaction liquid; washing filtrate B; drying and then filtering an organic layer to obtain filtrate C; carrying out reduced pressure distillation to recover the normal butanol; and obtaining a remainder which is the structural modification type cameclia oleifera saponin. The structural modification type cameclia oleifera saponinhas the characteristics of high foaming multiplying power, long foam stabilizing time and the like and can be used as a matrix raw material of an oil filed foaming agent; and the oil filed foaming agent synthesized by matching and optimizing has the performances of resisting acid, alkali, temperature and salt and capability of meeting the oil extracting requirements under different conditions.
Owner:江西新中野茶业科技有限公司

Ultralight building material and its producing method

The invention relates to an ultra-light building material which consists of driers, extravasation materials, foaming agents and water and is characterized in that the driers consist of cement which is 10 to 15 percent of the total weight of the driers and semi-hydrated gypsum which is 85 to 90 percent of the total weight of the driers; the extravasation materials consist of an efficient water reducing agent which is 1 to 3 thousandth of the total weight of the driers, a retarder for plaster which is 2 to 4 thousandth of the total weight of the driers, polyvinyl propyl ethernamine which is 0.5to 1.0 thousandth of the total weight of the driers and anti-cracking fiber which is 1.0 to 1.5 thousandth of the total weight of the driers; the foaming agents is 5 to 6 percent of the total weight of the driers; the weight ratio of the driers to water is 1:0.6 to 1:0.65. The invention also discloses a manufacturing method of the material. The building material is characterized by good mixture workability, easy foam adding and stabilizing and high foaming efficiency.
Owner:GANSU BUILDING MATERIALS DESIGN & RES INST CO LTD

A kind of thermal damage isolation material for deep-heat shaft and its preparation method

The invention discloses a thermal damage isolation material for deep-heat shafts and a preparation method thereof, and belongs to the fields of heat damage control of mine surrounding rocks and building thermal environment. It includes the following components in parts by weight, modified fly ash 0-300, cement 100-800, medium coarse sand 500-900, water 300-600, organic fiber 10-15, early strength agent 5-15, compound With foaming agent 3-15, additive 5-10. The present invention selects the modified fly ash that has been physically activated and chemically excited, so that more active pozzolans in the fly ash can participate in the hydration reaction, effectively saving the amount of high-grade cement, and improving the workability of the mixture. Reduce heat of hydration and thermal expansion, improve compression resistance and impermeability; the present invention uses organic fibers and additives to enhance flexural strength and deformability, and can effectively inhibit shrinkage and cracking; the thermal conductivity is determined to be 0.08-0.18 W / (m·K), has excellent thermal damage barrier ability; the invention has simple formula, long foam stabilization time and low thermal conductivity, and is suitable for thermal insulation of underground tunnels, external walls and non-load-bearing walls.
Owner:HENAN POLYTECHNIC UNIV

A colloidal foam fire extinguishing agent suitable for high-level fire sources and concealed fire sources in coal mines

The invention provides a colloidal foam fire extinguishing agent suitable for high-level fire sources and concealed fire sources in coal mines, and belongs to the technical field of fire extinguishing agents. The colloidal foam fire extinguishing agent suitable for high-level fire sources and concealed fire sources in coal mines provided by the present invention includes the following components in mass percentages: 1-4% of refractory soil, 20-30% of foaming agent, 3-7% of cooked rubber powder, Fly ash 1-10%, the rest water. The colloidal foam fire extinguishing agent provided by the present invention has a foam stabilization time of more than 100 hours, which can effectively avoid the phenomenon of "flowing along the channel" and the phenomenon of slurry deterioration on the working surface; Cracks accumulate and cover a wide area, which can effectively extinguish fire sources at high positions and hidden places with cracks. It is suitable for controlling fire sources in complex underground coal mines. When foam encounters high-temperature coal bodies in application, it can absorb the heat of coal bodies, and aggregates are adsorbed on them. In the coal body or cracks, a layer of water colloid is formed to absorb heat, cool down and isolate oxygen.
Owner:徐州铭博矿山科技有限公司

Colloid foam extinguishing agent suitable for high-position fire source and concealed fire source of coal mine

The invention provides a colloid foam extinguishing agent suitable for a high-position fire source and a concealed fire source of coal mine, and belongs to the technical field of extinguishing agents.The colloid foam extinguishing agent suitable for the high-position fire source and the concealed fire source of the coal mine comprises the following components in percentage by mass: 1-4% of refractory soil, 20-30% of a foaming agent, 3-7% of cooked rubber powder, 1-10% of fly ash and the balance of water. According to the invention, the colloid foam extinguishing agent provided by the invention has the advantages that the foam stabilizing time is more than 100 h, and the channeling phenomenon and the phenomenon that the working surface is deteriorated due to slurry collapse can be effectively avoided; and the colloid foam extinguishing agent provided by the invention can be accumulated towards cracks in a high space, so that the foam extinguishing agent is wide in coverage, can effectively extinguish a fire source at a high position and a crack concealing place, is suitable for governing the fire source under complex conditions of an underground coal mine, and can absorb heat of acoal body after foam encounters the high-temperature coal body in application, so that aggregates are adsorbed in the coal body or cracks to form a layer of moisture colloid so as to achieve the effects of heat absorption, cooling and oxygen isolation.
Owner:徐州铭博矿山科技有限公司

High-quality foam fracturing fluid and preparation method and application thereof

The invention discloses a high-quality foam fracturing fluid and a preparation method and application thereof, and the high-quality foam fracturing fluid is prepared from the following raw material components in parts by mass: 0.217 to 1.694 parts of a stabilizer, 0.394 to 3.388 parts of a compounding agent, 1.183 to 6.776 parts of a foaming agent, 0.986 to 6.098 parts of a foam stabilizer and 98.6 to 169.4 parts of water, the high-quality foam fracturing fluid with the density of 0.683 g / cm < 3 >-0.879 g / cm < 3 > can be prepared by mixing and stirring the raw material components. The high-quality foam fracturing fluid overcomes the defects that an existing low-density foam fracturing fluid is short in foam stabilizing time, low in foaming rate, uneven in foaming size, not resistant to high temperature and the like, the preparation process is simple, construction is easy, and the high-quality foam fracturing fluid is suitable for yield increasing transformation of low-pressure low-permeability, leakage and water-sensitive stratums.
Owner:BETTER OILFIELD TECH

A kind of camellia saponin concrete air-entraining agent and preparation method thereof

The invention provides a camellia saponin concrete air-entraining agent and a preparation method thereof. The air-entraining agent is characterized in that it contains Camellia oleifera saponin; the preparation method is characterized in that: taking Camellia oleifera as a raw material, adopting a hydrophilic solvent aqueous solution, extracting and filtering under conditions above normal temperature; after the filtrate is separated by membrane under pressure to remove macromolecular impurities, Remembrane separation to remove small molecular impurities, and concentrated into a concentrated solution with a Baumé degree of not less than 10 Be (60 ° C), spray-dried into a solid dosage form; or by adding modifiers to make an air-entraining agent for liquid dosage forms. The invention has novel concept, abundant raw materials, high production efficiency, low production energy consumption, low production cost, simple preparation method, green environmental protection, convenient implementation, small amount of air-entraining agent, large gas production, and introduced bubble pore size during concrete engineering application. Small, small spacing, concrete pores are more uniform, dense, non-connected, and have greater promotion.
Owner:FUZHOU UNIV

Preparation method and application of lauramide concrete foaming agent

The invention discloses a preparation method and an application of a lauramide concrete foaming agent. The method is characterized in that: lauric acid and hydroxyethylethylene diamine with a molar ratio of 1.0:1.0-1.5 are added into a reaction vessel, a solvent toluene is added, and the mixture is subject to a reaction for 2 to 5 hours under a temperature of 140 to 160 DEG C; the mixture is cooled, and a crude product of a yellow solid is obtained; the crude product is washed by using anhydrous acetone, and is dried, such that a white powdery solid is obtained, wherein the solid is an intermediate; the intermediate, chloroacetic acid and sodium hydroxide are formulated according to a molar ratio of 1:1.0-1.3:2.0-2.6; chloroacetic acid and sodium hydroxide are dissolved in water, such that a sodium monochloroacetate solution with a mass percent concentration of 10 to 20% is prepared; the intermediate is heated to 80 to 90 DEG C until melted, the sodium monochloroacetate solution is dropped into the intermediate, and the mixture is then subject to a reaction for 3 to 5 hours with maintained temperature; the mixture is cooled and filtered, insoluble substances are discarded, and the filtrate is the lauramide concrete foaming agent with excellent foaming performance.
Owner:SOUTHWEAT UNIV OF SCI & TECH
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