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A kind of preparation method of tannic acid modified leaf-adhesive pesticide

A technology of tannic acid and pesticides, applied in botany equipment and methods, chemicals for biological control, fungicides, etc., can solve problems such as poor adhesion on leaves, reduce contact angle, and enhance adhesion on leaves , the effect of material enhancement

Active Publication Date: 2021-07-20
INST OF ENVIRONMENT & SUSTAINABLE DEV IN AGRI CHINESE ACADEMY OF AGRI SCI
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] The purpose of the present invention is to provide a method for preparing tannic acid-modified foliage-adhesive pesticides for the defects of poor adhesion of existing commercially available water-dispersible granule pesticides on crop leaves

Method used

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  • A kind of preparation method of tannic acid modified leaf-adhesive pesticide
  • A kind of preparation method of tannic acid modified leaf-adhesive pesticide
  • A kind of preparation method of tannic acid modified leaf-adhesive pesticide

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0034] Example 1: Preparation of foliage-adhesive pesticides

[0035] Specific steps are as follows:

[0036] (1) Azoxystrobin water-dispersible granule pesticide primary liquid preparation

[0037] Weigh 0.1 g of 50% azoxystrobin water-dispersible granule pesticide, dissolve it in 100 mL of deionized water, and stir evenly with a magnetic stirrer to obtain solution A;

[0038] (2) Preparation of tannic acid and ferric chloride solution

[0039] Weigh 1g of tannic acid and dissolve it in 20mL deionized water to configure a 1:20 mass ratio tannic acid solution to obtain solution B; weigh 0.25g of FeCl 3 ˙6H 2 O was dissolved in 20mL deionized water to prepare a 1:80 mass ratio ferric chloride solution to obtain solution C;

[0040] (3) Preparation of leaf-adhesive pesticides

[0041] Solution A was magnetically stirred at 600rpm, and slowly added dropwise 1mL solution B to solution A according to the volume ratio of 100:1; the solution system was magnetically stirred for 5...

Embodiment 2

[0042] Example 2: Preparation of foliage-adhesive pesticides

[0043] (1) Abamectin water dispersible granule pesticide primary liquid preparation

[0044] Weigh 0.1 g of abamectin water-dispersible granule pesticide with a mass fraction of 10% and dissolve it in 100 mL of deionized water, and stir evenly with a magnetic stirrer to obtain solution A;

[0045] (2) Preparation of tannic acid and ferric chloride solution

[0046] Weigh 1g of tannic acid and dissolve it in 20mL deionized water to configure a 1:20 mass ratio tannic acid solution to obtain solution B; weigh 0.25g of FeCl 3 ˙6H 2 O was dissolved in 20mL deionized water to prepare a 1:80 mass ratio ferric chloride solution to obtain solution C;

[0047] (3) Preparation of leaf-adhesive pesticides

[0048] Solution A was magnetically stirred at 600rpm, and slowly added dropwise 1mL solution B to solution A according to the volume ratio of 100:1; the solution system was magnetically stirred for 5 minutes, and slowly...

Embodiment 3

[0049] Example 3: Preparation of foliage-adhesive pesticides

[0050] (1) Preparation of initial liquid of emamectin benzoate water dispersible granule pesticide

[0051] Weigh 0.1 g of emamectin benzoate water-dispersible granule pesticide with a mass ratio of 5% and dissolve it in 50 mL of deionized water, and stir evenly with a magnetic stirrer to obtain solution A;

[0052] (2) Preparation of tannic acid and ferric chloride solution

[0053] Weigh 1g of tannic acid and dissolve it in 20mL deionized water to configure a 1:20 mass ratio tannic acid solution to obtain solution B; weigh 0.25g of FeCl 3 ˙6H 2O was dissolved in 20mL deionized water to prepare a 1:80 mass ratio ferric chloride solution to obtain solution C;

[0054] (3) Preparation of leaf-adhesive pesticides

[0055] Solution A was stirred magnetically at 600rpm, and slowly added 0.5mL solution B to solution A according to the volume ratio of 100:1; the solution system was magnetically stirred for 5 minutes,...

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Abstract

The invention discloses a preparation method of a tannic acid-modified leaf-adhesive pesticide, which belongs to the field of preparation of pesticide formulations. The method is to weigh a certain amount of pesticide and dissolve it in deionized water, stir it evenly to obtain solution A; prepare tannic acid solution B, prepare ferric chloride to obtain solution C; Add 1 mL of solution B dropwise; the solution system was magnetically stirred for 5 minutes, and 1 mL of solution C was slowly added dropwise to the above system in the same volume ratio of 100:1. When solution C was dropped in, the color of the solution quickly turned into sea blue. After the system reacted for 5 minutes, the solution was centrifuged at 6000 rpm for 10 minutes to obtain the leaf-adhesive pesticide. The invention uses environment-friendly materials to modify the surface of the water-dispersible granule pesticide particles to improve its adhesion to the crop leaf surface, thereby increasing the effective utilization rate of the pesticide. contribute.

Description

【Technical field】 [0001] The invention relates to a preparation method for modifying tannic acid to enhance the adhesion of pesticide leaves, in particular to a method for improving the anti-photolysis stability of pesticides on the basis of the original water-dispersible granule and nano-suspension formulation pesticide production, and enhancing the anti-photolysis stability of pesticides on plants. The invention relates to a method for leaf surface adhesion, which belongs to the field of preparation of pesticide formulations. 【Background technique】 [0002] Pesticides are also called agrochemicals or agricultural growth regulators. With the development of biotechnology, the emergence of insect-resistant varieties can reduce the use of pesticides to a limited extent. However, the total population of our country is still showing an increasing trend. Under the condition of no increase in the total cultivated land area, pesticides still play an irreplaceable role in today's a...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A01N25/22A01N25/24A01N43/90A01N43/54A01N43/56A01P7/04A01P3/00
CPCA01N25/22A01N25/24A01N43/54A01N43/56A01N43/90
Inventor 曾章华智亨崔海信
Owner INST OF ENVIRONMENT & SUSTAINABLE DEV IN AGRI CHINESE ACADEMY OF AGRI SCI
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