Silicon-based polymer filling material for coal mines, and preparation method thereof
A silicon-based polymer and filling material technology, which is applied in the field of coal mine filling materials, can solve problems such as difficulty in meeting long-term plugging of leaks, flammable and toxic fumes, and difficulty in wall connection to the top, and achieves adjustable foaming ratio, The effect of adjustable curing time and low cost
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Embodiment 1
[0031] A method for preparing a silicon-based polymer filling material for coal mines is prepared by mixing components A and B at a mass ratio of 1.2:1.
[0032] Component A is made by mixing 90kg of sodium water glass with a Baume degree of 48, 2kg of AK-8805, 3kg of TX-10, 0.08kg of 1,6-hexanediol, and 0.25kg of dimethylcyclohexylamine.
[0033] Component B is made by mixing 50kg polymethylene polyphenyl polyisocyanate, 10kgTHPO and 20kgDOP.
[0034] Stir and mix the prepared component A and component B at a weight ratio of 1.5:1 to obtain the silicon-based polymer filling material for coal mines.
[0035] The prepared silicon-based polymer filling material for coal mines is naturally foamed at normal temperature and pressure, the expansion ratio is 15 times, the highest heat storage temperature is 78°C, and it is flame retardant according to the UL94 standard combustion test.
Embodiment 2
[0037] A method for preparing a silicon-based polymer filling material for coal mines is prepared by mixing components A and B at a mass ratio of 1.3:1.
[0038] Component A is made by mixing 95kg of sodium water glass with a Baume degree of 53, 4kg of AK-8805, 3kg of OP-10, 0.1kg of 1,4-butanediol, and 0.25kg of N,N-dimethylbenzylamine.
[0039] Component B is made by mixing 45kg polymethylene polyphenyl polyisocyanate, 8kg TCPP, and 20kg chlorinated paraffin-52.
[0040] Stir and mix the above components A and B at a weight ratio of 1.4:1 to obtain the silicon-based polymer filling material for coal mines.
[0041] The prepared silicon-based polymer filling material for coal mines is naturally foamed at normal temperature and pressure, the expansion ratio is 6 times, the highest heat storage temperature is 83°C, and it is flame retardant according to the UL94 standard combustion test.
Embodiment 3
[0043] A method for preparing a silicon-based polymer filling material for coal mines is prepared by mixing components A and B at a mass ratio of 1.4:1.
[0044] Component A is made by mixing 85kg of sodium water glass with a Baume degree of 45, 4.5kg of AK-8805, 5kg of TX-10, 0.12kg of 1,4-butanediol, and 0.25kg of N,N-dimethylbenzylamine.
[0045] Component B is made by mixing 45kg polymethylene polyphenyl polyisocyanate, 8kgDMMP and 25kgDOP.
[0046] Stir and mix the above-mentioned component A and component B at a weight ratio of 1.5:1 to obtain a silicon-based polymer filling material for coal mines.
[0047] The prepared silicon-based polymer filling material for coal mines is naturally foamed at normal temperature and pressure, the expansion ratio is 20 times, the highest heat storage temperature is 76°C, and it is flame retardant according to the UL94 standard combustion test.
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