KDP crystalloid long-seed crystal single-cone growth method

A growth method and crystal growth technology, applied in crystal growth, single crystal growth, single crystal growth, etc., can solve the problems of difficult growth, large growth solution disturbance, large growth stress, etc., and achieve high optical quality, high cutting efficiency, The effect of high optical uniformity

Active Publication Date: 2019-07-26
SHANGHAI INST OF OPTICS & FINE MECHANICS CHINESE ACAD OF SCI
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In the crystal carrier provided by the invention, the upper and lower horizontal plates are of plate structure, which greatly disturbs the growth solution during the crystal growth and rotation process, resulting in a decline in crystal quality; the invention fixes the seed crystal on the lower surface or lower surface of the upper horizontal plate. The center of the upper surface of the horizontal plate, but it is only rotated during the crystal growth without stirring effect, which will cause uneven crystal growth; and when the crystal grows to touch another horizontal plate, the collision contact between the crystal and the horizontal plate will occur , resulting in the growth of miscellaneous crystals
The invention patent with application number CN201710987729.6 and application publication number CN107805844A introduces a method for limiting the growth of KDP-like crystals with long seed crystals. During the growth process of this invention, the growth stress of the seed crystal will be relatively large because the seed crystal grows both up and down. Causes growth difficulties, and the height of the seed crystal that needs to be provided is large, which increases the growth pressure

Method used

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  • KDP crystalloid long-seed crystal single-cone growth method
  • KDP crystalloid long-seed crystal single-cone growth method
  • KDP crystalloid long-seed crystal single-cone growth method

Examples

Experimental program
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Effect test

Embodiment 1

[0025] Embodiment 1: KDP crystal long seed crystal single cone growth

[0026] KDP crystal long seed crystal single cone growth, including the following steps:

[0027] 1) Make the growth tank 1 used for crystal growth, the top of the growth tank 1 is equipped with a motor 5, the lower end of the rotating shaft 4 of the motor 5 is connected to the connecting rod 6 of the crystal carrier 3;

[0028] 2) making the crystal carrier 3 used for crystal growth: the crystal carrier 3 includes an upper beam 7, a lower tray 12, a connecting rod 6, supporting side bars 8, 9 and two leaf-shaped stirring paddles 10, 11, the The upper beam 7 is a slat with smooth edges and corners, the connecting rod 6 is a hollow round rod fixed in the middle of the upper beam 7, the lower tray 12 is a circular plate, and the supporting side bars 8, 9 The lower ends are welded to both ends of the same diameter of the lower tray 12, the upper ends of the support side bars 8,9 are welded to the two ends of ...

Embodiment 2

[0036] Embodiment 2: DKDP crystal long seed crystal single cone growth of 30% deuteration rate

[0037] 30% deuteration rate DKDP crystal long seed crystal single cone growth, including the following steps:

[0038] 1) Make the growth tank 1 used for crystal growth, the top of the growth tank 1 is equipped with a motor 5, the lower end of the rotating shaft 4 of the motor 5 is connected to the connecting rod 6 of the crystal carrier 3;

[0039]2) making the crystal carrier 3 used for crystal growth: the crystal carrier 3 includes an upper beam 7, a lower tray 12, a connecting rod 6, supporting side bars 8, 9 and two leaf-shaped stirring paddles 10, 11, the The upper beam 7 is a slat with smooth edges and corners, the connecting rod 6 is a hollow round rod fixed in the middle of the upper beam 7, the lower tray 12 is a circular plate, and the supporting side bars 8, 9 The lower ends are welded to both ends of the same diameter of the lower tray 12, the upper ends of the suppor...

Embodiment 3

[0047] Embodiment 3: DKDP crystal long seed crystal single cone growth of 70% deuteration rate

[0048] 70% deuteration rate DKDP crystal long seed crystal single cone growth, including the following steps:

[0049] 1) Make the growth tank 1 used for crystal growth, the top of the growth tank 1 is equipped with a motor 5, the lower end of the rotating shaft 4 of the motor 5 is connected to the connecting rod 6 of the crystal carrier 3;

[0050] 2) making the crystal carrier 3 used for crystal growth: the crystal carrier 3 includes an upper beam 7, a lower tray 12, a connecting rod 6, supporting side bars 8, 9 and two leaf-shaped stirring paddles 10, 11, the The upper beam 7 is a slat with smooth edges and corners, the connecting rod 6 is a hollow round rod fixed in the middle of the upper beam 7, the lower tray 12 is a circular plate, and the supporting side bars 8, 9 The lower ends are welded to both ends of the same diameter of the lower tray 12, the upper ends of the suppo...

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Abstract

The invention discloses a KDP crystalloid long-seed crystal single-cone growth method. According to the growth method, the lower end of a long-seed crystal is limited by a lower tray, the upper end ofthe long-seed crystal freely and conically grows, four cylindrical surfaces in the two directions of (100) and (010) can grow, the problem of growth stress is omitted in the growth process of the crystal, all cut out optical elements have high optical quality, four cylindrical surfaces with highly similar growing environments simultaneously grow in the growth process, mixing is implemented by a leaf-shaped mixing propellers in the growth process of the crystal, so that the cut out optical elements have high optical homogeneity, a cutting angle of a KDP crystal triple frequency element is unique, the grown crystal has high cutting efficiency when cutting the triple frequency element, and the area of the cut maximum triple frequency element can be known according to the horizontal size of the grown crystal in advance.

Description

technical field [0001] The invention relates to KDP-like crystals, in particular to a method for growing KDP-like crystals with long seed crystals and single cones, aiming at rapidly growing KDP-like crystals with high cutting efficiency and low growth stress. Background technique [0002] Potassium dihydrogen phosphate / dideuterium potassium phosphate (KDP / DKDP) crystal material is widely used in the production of frequency doubling and electro-optical devices due to its large nonlinear optical coefficient, wide transmission band, and excellent optical uniformity. Laser inertial confinement fusion (ICF) devices in various countries require a large number of high-quality, large-diameter KDP crystals; among them, KDP crystals are used as optical switches and frequency-doubling components, and DKDP crystals are used as frequency-tripling components. However, the KDP-like crystals grown by the prior art mainly have defects such as poor crystal quality and low aspect ratio, and f...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C30B7/08C30B29/14
CPCC30B7/08C30B29/14G02F1/3551G02F1/354G02F1/37
Inventor 王斌齐红基邵建达陈端阳王虎王晓亮
Owner SHANGHAI INST OF OPTICS & FINE MECHANICS CHINESE ACAD OF SCI
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