Tire sidewall rubber and preparation method thereof
A technology for sidewall rubber and tires, which is applied in special tires, tire parts, rolling resistance optimization, etc. It can solve problems such as mixing formula and method to be studied, and achieve compatibility and co-vulcanization characteristics improvement, fatigue resistance performance Improved and excellent fatigue resistance
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[0051] The present invention also provides a kind of preparation method of above-mentioned tire sidewall rubber, comprises the following steps:
[0052] A) mixing natural rubber, TBIR-BR masterbatch, zinc oxide, stearic acid, anti-aging agent, filler and process oil in banburying to obtain one stage of masterbatch;
[0053] B) mixing said one-stage masterbatch, accelerator and sulfur banburying to obtain two-stage masterbatch;
[0054] C) The second-stage masterbatch is opened for kneading, and the obtained final mix is placed at a temperature of 21-25° C. and a humidity of 30-80% for 4-168 hours;
[0055] D) vulcanizing the final rubber mix after standing at a temperature of 140-180° C. and a pressure of 10-35 MPa to obtain tire sidewall rubber.
[0056] In the preparation method, the components and proportions of the raw materials are the same as above, and will not be repeated here.
[0057] In an embodiment of the present invention, the TBIR-BR masterbatch is prepared ...
Embodiment 1
[0081] Preparation of TBIR-BR masterbatch:
[0082] The trans-butadiene rubber TBIR-0963 and butadiene rubber BR 9000 were banburyed and blended according to the mass ratio of 50:10. The blending input coefficient is 0.75, and the mixing time is 3 minutes.
[0083] Prepare tire sidewall compound:
[0084] First mix natural rubber and TBIR-BR masterbatch for 1min, then add zinc oxide, stearic acid, anti-aging agent (3 parts by weight of anti-aging agent 4020, 1.5 parts by weight of anti-aging agent RD and 1.5 parts by weight of paraffin), carbon black N330, carbon black dispersant and environmental protection aromatic hydrocarbon oil VIVATEC 500 banbury mixing 4min; The temperature of twice banbury blending is 70 ℃, the rotating speed is 70rpm, and the feeding coefficient is 0.75. The glue temperature is 155°C, and a section of masterbatch is obtained;
[0085] Put one stage of masterbatch into the banbury mixer, add accelerator NS and sulfur powder for banbury mixing to obt...
Embodiment 2
[0090] Preparation of TBIR-BR masterbatch:
[0091] Trans-butadiene rubber TBIR-2063 and butadiene rubber BR 9000 were banburyed and blended according to the mass ratio of 50:10. The blending input coefficient is 0.75, and the mixing time is 3 minutes.
[0092] Prepare tire sidewall compound:
[0093] First mix natural rubber and TBIR-BR masterbatch for 1min, then add zinc oxide, stearic acid, anti-aging agent (3 parts by weight of anti-aging agent 4020, 1.5 parts by weight of anti-aging agent RD and 1.5 parts by weight of paraffin), carbon black N330, carbon black dispersant and naphthenic oil banbury mixing 5min; The temperature of twice banbury blending is 70 ℃, and the rotating speed is 70rpm, and the feeding coefficient is 0.75, and the debinding temperature after described banbury blending at 155°C to obtain a section of masterbatch;
[0094] Put one stage of masterbatch into the banbury mixer, add accelerator NS and sulfur powder for banbury mixing to obtain the seco...
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