Novel sesquiterpenes compound and preparation method and application thereof
A compound and solvate technology, applied in the field of novel sesquiterpene compounds and their preparation, can solve the problems of irreversibility and progressive aggravation, and achieve the effects of good application prospect, protection of nerve cells and novel structure
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Embodiment 1
[0059] The preparation of embodiment 1 compound of the present invention
[0060] (1) Experimental materials:
[0061] ① Medicinal materials
[0062] Dendrobium nobile was purchased from Sichuan Wanan Dendrobium Industry Development Co., Ltd. (Chengdu), and was identified as the fresh stems and leaves of Dendrobium nobile Lindl. by Professor Zhang Tingmo of Chengdu University of Traditional Chinese Medicine.
[0063] ②Reagents and fillers
[0064] Automatic polarimeter (Shanghai Yili Scientific Instrument Co., Ltd.)
[0065] Perkin-Elmer spectrum one FT-IR infrared spectrometer (KBr tablet)
[0066] Chirascan CD spectrometer (Applied Photophysics, UK)
[0067] Bruker-600 nuclear magnetic resonance instrument (Germany Bruker company)
[0068] Waters Synapt G2 Tof-HDMS mass spectrometer (Waters, USA)
[0069] RE-52A rotary evaporator (Shanghai Yarong Instrument Biochemical Factory)
[0070] Silica G (Qingdao Ocean Chemical Factory)
[0071] GF254 Silica Gel Preparation...
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