36V and below low-voltage driven PTC electrothermal film and preparation method thereof
An electrothermal film and low-voltage technology, which is applied in the field of electrothermal material preparation, can solve problems such as potential safety hazards, electric leakage, electric shock, and easy formation of air bubbles, and achieve the effects of improving safety performance, prolonging service life, and improving stability
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[0032] The PTC electrothermal film preparation method driven by 36V low voltage of the present invention comprises the following steps:
[0033] 1. Preparation of graphene microchip-filled PTC conductive particles: Weigh 1.5-5 parts of graphene microchips, 63.5-97 parts of polyethylene resin, 1.5-31.5 parts of polymethyl methacrylate, and place in a high-speed mixer Stir at medium and high speed for 20-25 minutes to obtain the graphene microflake composition; use an extruder to melt and extrude, water-cool at room temperature, and then granulate through a cutting machine to obtain graphene microflake-filled PTC conductive particles;
[0034] 2. Preparation of heating layer 2: Use a casting film forming machine to cast the conductive particles prepared in step 1 at 120-150°C to form a film, and wind up to obtain a graphene microchip-filled PTC heating element 5 with a thickness of 30-150°C. 60 μm, and then two conductive copper strips 4 are hot-compressed in parallel at 120-150...
Embodiment 1
[0040] 1. Preparation of graphene microflake-filled PTC conductive particles: Weigh 0.2kg of graphene microflakes, 7kg of low-density polyethylene resin, 1kg of polymethyl methacrylate, and stir in a high-speed mixer for 20 minutes to obtain a mixture;
[0041] The extruder melts the mixture and extrudes and spins it, and after it is cooled in water, it is pelletized by a cutting machine to obtain graphene microflake-filled PTC conductive particles;
[0042]2. Preparation of heating layer 2: using a casting film forming machine, the conductive particles prepared in step 1 were cast into a film at 130°C, and rolled to obtain a graphene microchip-filled PTC heating element 5 with a thickness of 60 μm, and then in The prepared graphene microchip-filled PTC heating element 5 is parallel hot-pressed at 130°C on both sides and combined with two conductive copper strips 4 to obtain the heating layer 2;
[0043] 3. Composite insulating layer: thermally compound the upper insulating la...
Embodiment 2
[0046] 1. Prepare graphene microchip-filled PTC conductive particles: weigh 0.3kg of graphene microchip, 7kg of low-density polyethylene resin, 1kg of polymethyl methacrylate, and stir in a high-speed mixer for 20 minutes to obtain a mixture;
[0047] The extruder melts the mixture and extrudes and spins it, and after it is cooled in water, it is pelletized by a cutting machine to obtain graphene microflake-filled PTC conductive particles;
[0048] 2. Preparation of heating layer 2: Use a casting film forming machine to cast the conductive particles prepared in step 1 at 150°C to form a film, and wind up to obtain a graphene microchip-filled PTC heating element 5 with a thickness of 50 μm, and then in The prepared graphene microchip-filled PTC heating element 5 is parallel hot-pressed at 130°C on both sides and combined with two conductive copper strips 4 to obtain the heating layer 2;
[0049] 3. Composite insulating layer: thermally compound the upper insulating layer 1 and ...
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