High polymer material for modifying explosive, and preparation method thereof, and method for modifying explosive

A technology of polymer materials and explosives, which can be used in non-explosive/non-thermal components, explosives, offensive equipment, etc., and can solve the problem of low stability of polymer materials

Inactive Publication Date: 2019-11-29
XIAN UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] Another object of the present invention is to provide a method for preparing a polymer material for explosive modificati

Method used

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  • High polymer material for modifying explosive, and preparation method thereof, and method for modifying explosive
  • High polymer material for modifying explosive, and preparation method thereof, and method for modifying explosive
  • High polymer material for modifying explosive, and preparation method thereof, and method for modifying explosive

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0056] A kind of preparation method of the polymer material that is used for explosive modification, concretely carries out according to the following steps:

[0057] Step 1, weigh 95 parts of N-vinylpyrrolidone according to the mass fraction, and add it into a reaction vessel containing 145 parts of N,N-dimethylformamide to obtain N,N-dimethylformamide of N-vinylpyrrolidone Amide solution;

[0058] Step 2, add 0.24 parts of azobisisobutyronitrile according to the mass fraction to the raw material weighed in step 1, and mix uniformly;

[0059] In step 3, the mixed solution obtained in step 2 is deoxidized by bubbling argon gas for 10 minutes to obtain a deoxygenated mixed solution;

[0060] Step 4, heating the deoxidized mixed solution obtained in Step 3 to 70°C at a heating rate of 5°C / min, and keeping it at a constant temperature for 1 hour, and then naturally cooling to room temperature;

[0061] Step 5, rotary steaming for 30 minutes to remove N,N-dimethylformamide in th...

Embodiment 2

[0067] A kind of preparation method of the polymer material that is used for explosive modification, concretely carries out according to the following steps:

[0068] Step 1, weigh 45 parts of N-vinylpyrrolidone and 45 parts of vinyl acetate according to the mass fraction, and add them into a reaction vessel containing 210 parts of N,N-dimethylformamide to obtain N-vinylpyrrolidone and vinyl acetate N,N-dimethylformamide mixed solution of ester;

[0069] Step 2, add 1.5 parts of azobisisobutyronitrile to the mixed solution in step 1 according to the mass fraction, and mix well;

[0070] In step 3, the mixed solution obtained in step 2 is deoxidized by bubbling argon gas for 10 minutes to obtain a deoxygenated mixed solution;

[0071] Step 4, heating the deoxidized mixed solution obtained in Step 3 to 80°C at a heating rate of 5°C / min, and keeping it at a constant temperature for 12 hours, and then naturally cooling to room temperature;

[0072] Step five, rotary steaming for...

Embodiment 3

[0078] A kind of preparation method of the polymer material that is used for explosive modification, concretely carries out according to the following steps:

[0079] Step 1, take 1 part of N-vinylpyrrolidone, 49 parts of styrene, and 45 parts of methyl methacrylate, and add them to a reaction vessel containing 380 parts of N,N-dimethylformamide to obtain N-vinylpyrrolidone , N,N-dimethylformamide mixed solution of styrene and methyl methacrylate;

[0080] Step 2, add 4.7 parts of azobisisobutyronitrile to the mixed solution in step 1 according to the mass fraction, and mix well;

[0081] In step 3, the mixture obtained in step 2 is deoxidized by bubbling argon gas for 10 minutes to obtain a deoxidized mixture;

[0082] Step 4, heating the deoxidized mixture obtained in Step 3 to 90°C at a heating rate of 5°C / min, and keeping it at a constant temperature for 24h, and then naturally cooling to room temperature;

[0083] Step five, rotary steaming for 120 minutes to remove N,N...

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PUM

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Abstract

The invention discloses a high polymer material for modifying an explosive, wherein the material is characterized in that the molecule contains a pyrrolidone group, and the material can be prepared bycarrying out copolymerizing vinyl pyrrolidone and other polymerization monomers or by carrying out self-homopolymerization, can be matched with epoxy resins, acrylic resins and other polymer resins so as to be used as a modification material for explosives, and can be mixed with explosives in a powder form, or mixed with explosives under a heating condition. The invention further discloses a method for modifying explosives by using the polymer modification material, wherein direct mixing or heating melting mixing can be performed, and a mass ratio of an explosive material to the modificationmaterial is any ratio. The invention further discloses a method for modifying an explosive, wherein the high polymer material is adopted as an additive, and is mixed with an explosive material so as to affect the performance of the explosive material, wherein the performances comprise: mechanical performance, color, compatibility with other components, deflagration performance and the like.

Description

technical field [0001] The invention belongs to the technical field of explosive modification, and relates to a polymer material used for explosive modification, a preparation method of the polymer material used for explosive modification, and a method for explosive modification. Background technique [0002] TNT explosive has already been widely used, but due to its own problems, such as the production of toxic waste, transportation, storage and stability in use, etc., people try to find his substitutes, such as 2,4-di Nitroanisole (DNAN), (DNTF) and the like. Casting explosives is one of their important applications, and it is also the most widely used military mixed explosive at present. The solid phase particles of high-energy explosives are added to the molten explosive matrix to form a flow state for casting mixed explosives. Because of its convenient loading and good performance, cast explosives are mostly used in shells, grenades, missile warheads, etc., and occupy ...

Claims

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Application Information

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IPC IPC(8): C08F126/10C08F226/10C08F218/08C08F212/08C08F220/14C06B23/00
CPCC06B23/00C08F126/10C08F212/08C08F226/10C08F218/08C08F220/14
Inventor 欧阳晓平张乾陈卫星刘乃亮李珺鹏刘坤罗一鸣王浩
Owner XIAN UNIV OF TECH
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