Composite luminescent fiber and preparation method and application thereof

A technology of luminescent fiber and composite fiber, which is applied in the direction of fiber chemical characteristics, rayon manufacturing, single-component synthetic polymer rayon, etc., to achieve the effect of simple manufacturing process, full elasticity and high luminescence

Pending Publication Date: 2019-12-20
BEIJING INST OF NANOENERGY & NANOSYST
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The purpose of the present invention is to solve the problem of how to use AIE to obtain lum

Method used

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  • Composite luminescent fiber and preparation method and application thereof
  • Composite luminescent fiber and preparation method and application thereof
  • Composite luminescent fiber and preparation method and application thereof

Examples

Experimental program
Comparison scheme
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Example Embodiment

[0071] By adopting the preparation method provided by the invention, the composite spinning of the polymer and the aggregation-induced luminescent AIE molecule is realized to prepare the composite luminescent fiber. Because the AIE molecule has high luminescence under the excitation of ultraviolet light, and the polymer can provide the mechanical properties required by the composite fiber, the formed polymer / AIE composite luminescent fiber has excellent luminescence and mechanical properties that meet the requirements.

[0072] According to the present invention, the first solvent and the second solvent are each independently selected from at least one of dichloromethane, cyclohexane, phenol, toluene, acetonitrile, chlorobenzene, and methyl acetate.

[0073] According to the present invention, in step 4), the conditions of the pre-curing treatment are: the pre-curing temperature is 40-80° C., and the pre-curing time is 5-40 min.

[0074] In the present invention, the pre-curing treat...

Example Embodiment

[0118] Preparation example

[0119] Use as figure 1 The spinning method shown to prepare luminous fiber, the specific operation steps are:

[0120] Transfer the spinning solution into a 100ml syringe while heating the temperature of the oil bath to 150℃. The injection pump extrudes the spinning solution into the oil bath at a speed of 8ml / min. The spinning solution is rapidly solidified in the oil bath. For fiber, the curing time is 8s, then the fiber is collected on the bobbin at a linear speed of 2m / min., and finally washed and dried.

Example Embodiment

[0121] Example 1

[0122] Step 1): Prepare aggregation-induced luminescence (AIE) molecule solution: add 0.006 g of aggregation-induced luminescence (AIE) molecule II to dichloromethane to obtain an aggregation-induced luminescence (AIE) solution;

[0123] Step 2): Prepare the A-component composite solution of AIE@PDMS: add 1.82g of PDMS A-component into the aggregation-induced luminescence (AIE) molecular solution described in step 1), stir manually to make it fully mixed and uniform ; Then put the prepared composite solution into a 40 ℃ vacuum drying oven and vacuum dry for 4 hours;

[0124] Step 3): Prepare the AIE@PDMS composite solution: add 0.18 g of PDMS component B to the composite solution described in step 2), stir thoroughly to make it evenly mixed, and obtain the AIE@PDMS composite solution;

[0125] Step 4): Preparation of AIE@PDMS spinning solution: Put the AIE@PDMS composite solution described in step 3) into an oven at 60°C for 10 minutes, and then cool for 30 minutes ...

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Abstract

The invention relates to the field of flexible wearable luminescent devices, in particular to a composite luminescent fiber and a preparation method and application thereof. The composite luminescentfiber comprises a polymer and aggregation-induced emission (AIE) molecules, wherein the curing temperature of the polymer is 0-300 DEG C. According to the composite luminescent fiber, because the AIEmolecules which have high luminescent capability under ultraviolet excitation are contained in the fiber and the polymer is high in softness and stretchability, the formed composite luminescent fiberhas excellent luminescent capability and is highly stretchable.

Description

technical field [0001] The invention relates to the field of flexible wearable light-emitting devices, in particular to a composite light-emitting fiber and its preparation method and application. Background technique [0002] With the advancement of society and technology, flexible wearable devices have received more and more attention. The demand for flexible wearable devices has driven the development of related materials and fabrication techniques. These efforts include integrating functional materials into textiles, or integrating electronic components into human fabrics for special functions such as energy harvesting and storage, multifunctional sensing, communication, and light-emitting displays. Innovations in wearable devices have brought about new concepts in clothing. However, most of the current research reports focus on sensors, energy harvesting and storage, and transistors, among which there are few reports on flexible light-emitting devices. Smart wearable...

Claims

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Application Information

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IPC IPC(8): D01F6/94D01F1/10
CPCD01F1/10D01F6/94
Inventor 蒲雄万军民顾星桂丁文凤孙江曼
Owner BEIJING INST OF NANOENERGY & NANOSYST
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