Solid-liquid reaction device

A solid-liquid reaction and reactor technology, applied in chemical/physical processes, chemical instruments and methods, etc., can solve the problems of insufficient reaction, insufficient mixing of materials, incomplete reaction, etc.

Pending Publication Date: 2020-01-14
HUNAN INSTITUTE OF ENGINEERING
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] 1. The solid-liquid reaction device has a single way of stirring solid-liquid mixing. During the reaction process, the reactants and solids are not in contact and mixed enough, the reaction is not complete, and the reaction rate is low;
[0004] 2. The generated reactant is attached to the solid surface, so that the internal reactant is isolated from the liquid, resulting in insufficient reaction;
[0005] 3. The specific gravity of the solid is much greater than that of the liquid, which is easy to settle and not easy to be stirred evenly. Traditional chemical reactor stirring cannot fully mix the materials

Method used

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Embodiment 1

[0038] One of the embodiments of a solid-liquid reaction device of the present invention, such as figure 1 Said, including conical reactor 1, base 2, bubble generating device 3, gas source 4, compressor 5 and gas filter 5; the side wall of reactor 1 is provided with feeding port 11, and bubble generating device 3 is detachable Connected to the bottom of the reactor, the base 2 is cylindrical and abuts against the side wall of the reactor; the top of the reactor is closed and connected to the gas filter 6, compressor 5, gas source 4 and bubble generating device 3 in sequence through pipelines .

[0039] Thus, by installing a bubble generating device at the bottom of the reactor, the gas in the gas source is ejected at the bottom of the reactor by means of microbubbles, so that the solid reactant 7 that is easy to deposit on the bottom of the reactor is blown towards the bottom of the reactor by the impact force of the microbubbles. The upper part of the liquid 8 moves, and the...

Embodiment 2

[0044] One of the embodiments of a solid-liquid reaction device of the present invention, such as Figure 1 to Figure 2 It means that the main technical solution of this embodiment 2 is basically the same as that of embodiment 1, and the features not explained in this embodiment 2 are explained in embodiment 1, and will not be repeated here. The difference between this embodiment and embodiment 1 is:

[0045] The angle between the central axis of the reactor and the side of the reactor is 60 degrees. At this time, the reaction effect of the reactor is better when the specific gravity of the solid and the liquid is relatively large.

[0046] Preferably, micropores are distributed annularly on the top of the bubble generator, and the number of micropores is six. Such as figure 2 shown.

[0047] Specifically, the annularly distributed micropores are distributed obliquely in the vertical direction. When the bubble generator is working, it forms a vortex on the liquid, and fu...

Embodiment 3

[0051] One of the embodiments of a solid-liquid reaction device of the present invention, such as Figure 1 to Figure 2 It means that the main technical solution of this embodiment 3 is basically the same as that of embodiment 1 or embodiment 2, and the features that are not explained in this embodiment 3 are explained in embodiment 1 or embodiment 2, and are not repeated here repeat. The difference between this embodiment and Embodiment 2 is that the number of microholes 31 is twelve. Twelve ring-shaped micropores are set to further achieve the effect of dispersing solids and uniform air bubbles.

[0052] More specifically, the diameter of the micropores is set to 0.2 mm.

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Abstract

The invention provides a solid-liquid reaction device, which comprises a conical reactor, a base, a gas bubble generating device, a gas source, a compressor and a gas filter, wherein the top of the reactor is closed and is sequentially connected to the gas filter, the compressor, the gas source and the gas bubble generating device through pipelines. According to the invention, by arranging the gasbubble generating device at the bottom of the reactor, the solid reactants or catalysts deposited at the bottom of the reactor move to the upper portion of the reactor under the impact force of the micro gas bubbles, so that the solid completely and uniformly contacts the liquid; and the solid-liquid reaction device has characteristics of cyclic utilization of gas, uniform solid-liquid mixing, high reaction efficiency and energy conservation.

Description

technical field [0001] The invention relates to the technical field of chemical reaction devices, in particular to a solid-liquid reaction device. Background technique [0002] With the wide application of polymer materials in chemical industry, it is usually necessary to react solid polymer materials with chemical liquids. In the traditional liquid-solid reaction, the liquid is the reaction liquid or organic solvent, and the solid is the reactant or catalyst particles. In the prior art, there are the following technical problems: [0003] 1. The solid-liquid reaction device has a single way of stirring solid-liquid mixing. During the reaction process, the reactants and solids are not in contact and mixed enough, the reaction is not complete, and the reaction rate is low; [0004] 2. The generated reactant is attached to the solid surface, so that the internal reactant is isolated from the liquid, resulting in insufficient reaction; [0005] 3. The specific gravity of sol...

Claims

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Application Information

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IPC IPC(8): B01J8/24
CPCB01J8/245
Inventor 方正军谭盛琼邬峰
Owner HUNAN INSTITUTE OF ENGINEERING
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