Anti-yellowing bright uv paint and its production process
A production process and anti-yellowing technology, applied in the field of coatings, can solve the problems of not achieving high whiteness, yellowing of paint film, yellowing, etc., and achieve the effect of improving yellowing resistance, not easy to yellow, and small shrinkage
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Embodiment 1
[0035] Anti-yellowing bright UV paint, by weight, includes the following components, 41.2 parts of polyurethane acrylate, 20 parts of ethyl ester, 10 parts of butyl ester, 3 parts of photoinitiator, 15 parts of UV monomer, and 0.8 part of leveling agent , 10 parts of cellulose acetate butyrate, 1.5 parts of fluorescent whitening agent OB-1; among them, 7 parts of UV monomers including IBOMA and 8 parts of TMPTA.
[0036] The leveling agent is BYK-333, and the photoinitiator is photoinitiator 1173.
[0037] Fluorescent whitening agent OB-1 undergoes the following modification steps:
[0038] S1: Add fluorescent whitening agent OB-1 into water, and add 5mL of water for every 1g of fluorescent whitening agent OB-1, and ultrasonically disperse for 10min;
[0039] S2: Under the condition of uniform stirring, add water glass so that the mass concentration of water glass in the solution after adding water glass is 10%, then add concentrated sulfuric acid drop by drop to adjust the p...
Embodiment 2
[0050] The difference with embodiment 1 is:
[0051] Anti-yellowing bright UV paint, by weight, includes the following components, 35 parts of polyurethane acrylate, 15 parts of ethyl ester, 8 parts of butyl ester, 2 parts of photoinitiator, 11 parts of UV monomer, 0.4 part of leveling agent , 8 parts of cellulose acetate butyrate, 1 part of fluorescent whitening agent OB-1; among them, the UV monomer includes 6 parts of IBOMA and 5 parts of TMPTA.
[0052] In the modification treatment step S2 of fluorescent whitening agent OB-1, the mass concentration of water glass in the solution after adding water glass is 5%, then add concentrated sulfuric acid drop by drop to adjust the pH to 5, then heat it in a water bath to 40°C, and keep the temperature constant Heating for 4h, drying at 70°C for 8h, and calcining at 300°C for 8h.
[0053] In the production step S3 of the anti-yellowing bright UV paint, the temperature is raised to 80°C.
Embodiment 3
[0055] The difference with embodiment 1 is:
[0056] Anti-yellowing bright UV paint, by weight, includes the following components, 50 parts of polyurethane acrylate, 25 parts of ethyl ester, 12 parts of butyl ester, 5 parts of photoinitiator, 17 parts of UV monomer, and 1 part of leveling agent , 13 parts of cellulose acetate butyrate, 3 parts of fluorescent whitening agent OB-1; among them, UV monomers include 10 parts of IBOMA and 7 parts of TMPTA.
[0057] In the modification treatment step S2 of the fluorescent whitening agent OB-1, in S2, the mass concentration of water glass in the solution after adding water glass is 20%, then add concentrated sulfuric acid drop by drop to adjust the pH to 7, and then heat it in a water bath to 50 ℃, heated at constant temperature for 6h, dried at 80°C for 10h, and calcined at 300°C for 10h.
[0058] In the production step S3 of the anti-yellowing bright UV paint, the temperature is raised to 90°C.
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