Excellent boiling-resistant and neutral-salt-mist-resistant polyester resin for low-temperature curing type powder and preparation method thereof
A technology of polyester resin and water boiling resistance, applied in powder coatings, polyester coatings, coatings, etc., can solve the problems of water boiling resistance, neutral salt spray resistance, and inability to cure at low temperature with TGIC system, achieving outstanding performance Boiling resistance and neutral salt spray resistance, excellent boiling resistance and high activity
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[0037] Example 1
[0038] The preparation method of polyester resin for TGIC type powder coating resistant to boiling and neutral salt spray includes the following steps:
[0039] (1) Prepare each raw material, and the amount of each raw material is shown in Table 1. Add the catalyst zinc acetate, 1H, 1H, 12H, 12H-perfluoro-1,12-dodecanediol, terephthalic acid, and dodecenyl succinic anhydride into the reactor at a rate of 20°C / h Gradually increase the temperature to 150°C and keep it for 6 hours; then increase it to 190°C at a rate of 10°C / h and keep it for 5 hours;
[0040] (2) When the acid value of the reactant is 55mgKOH / g, add neopentyl glycol and isophthalic acid to the reaction kettle to carry out a sufficient esterification polymerization reaction, and slowly increase the temperature to 220°C at a rate of 7°C / h. Insulate and continue the polymerization reaction for 6 hours;
[0041] (3) When the acid value of the reactant is 55 mgKOH / g, the temperature is lowered to 210°C, ...
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[0064] Example 5
[0065] The formula of high acid value TGIC system powder coating is usually as follows in parts by weight:
[0066]
[0067]
[0068] Coating preparation: according to the formula of high acid value TGIC powder coating, the materials are mixed uniformly, extruded with a twin-screw extruder, tableted, crushed, and then the flakes are crushed and screened to make the powder coating. The powder coating is sprayed on the surface-treated aluminum plate with an electrostatic spray gun, and cured quickly at 150°C / 15min to obtain a powder coating coating.
[0069] Coating index testing is based on GB / T 21776-2008 "Powder Coatings and Coating Testing Standard Guide"; water boiling resistance test GB 5237.4-2008 "Aluminum Alloy Building Profile Part 4 Powder Coating Profile" in section 5.4.10; The neutral salt spray resistance test is based on GB / T 1771-91 "Determination of the neutral salt spray resistance of paints and varnishes".
[0070] Table 3 The basic properties of t...
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