Transfer reaction device and method for high-viscosity material
A reaction device and material technology, applied in the field of heat and mass transfer of materials and reactors, can solve the problems of material evaporation or small vaporization interface, small effective heat transfer area of evaporator, difficulty in handling super viscous materials, etc., to increase effective heat transfer Effects of thermal area, shortened residence time, and broadened elastic range
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Embodiment 1
[0027] Such as figure 1 and image 3 As shown, a high-viscosity material transfer and reaction device includes a housing 1, a hollow shaft assembly 2, a column-shaped dispersion assembly 3 composed of hollow tubes, and the like. The shell 1 is a jacket shell, the upper part of the shell 1 is provided with a material inlet 6, and the lower part of the shell 1 is provided with a material outlet 5. The hollow shaft assembly 2 is arranged inside the housing 1, one end is rotatably connected to the upper end surface of the housing, and the other end is rotatably connected to the lower end surface of the housing.
[0028] The hollow shaft assembly includes a hollow shaft, and also includes a separator 4 separating the hollow shaft into a liquid inlet section and a liquid return section, and the liquid inlet section and the liquid return section are indirectly connected through the heat exchange pipe network. The heat exchange pipe network is divided into a liquid inlet heat exchan...
Embodiment 2
[0033] Such as figure 2 As shown, a high-viscosity material transfer and reaction device includes a housing 1, a hollow shaft assembly 2, a column-shaped dispersion assembly 3 composed of hollow tubes, and the like. The shell 1 is a jacket shell, the upper part of the shell 1 is provided with a material inlet 6, and the lower part of the shell 1 is provided with a material outlet 5. The hollow shaft assembly 2 is arranged inside the casing 1, one end is rotatably connected to the upper end surface of the casing, and the other end is suspended in the air.
[0034] The hollow shaft assembly includes an outer tube 14 and an inner tube 15 coaxially set, one of the outer tube and the inner tube is a liquid inlet pipe, and the other is a liquid return pipe, and the liquid inlet pipe and the liquid return pipe The lengths of the pipes are inconsistent; the liquid inlet pipe is connected 9 with the heat exchange medium inlet 7 through the first rotary joint, and the liquid outlet pi...
Embodiment 3
[0039]In this embodiment, maltose is used as the test material, and the heating medium is hot water to concentrate the maltose. The initial temperature of the test medium is 25°C, the outlet temperature is 80°C, the temperature rise is 55°C, vacuum operation is adopted, and the pressure is 500Pa. Other structures of this example are the same as those of Embodiment 1. Keeping the test material, heating medium and test conditions unchanged, and taking the test results of the common scraper type thin film evaporator as the reference group, this embodiment can increase the effective heat transfer area by at least 5 times, and the residence time is the original 1 / 20 of that, the renewal frequency of the material surface is greatly increased, the material evaporation or vaporization interface is too small, the heat transfer rate is increased by more than 3 times, and the production capacity per unit volume of equipment is increased by more than 5 times.
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