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Transfer reaction device and method for high-viscosity material

A reaction device and material technology, applied in the field of heat and mass transfer of materials and reactors, can solve the problems of material evaporation or small vaporization interface, small effective heat transfer area of ​​evaporator, difficulty in handling super viscous materials, etc., to increase effective heat transfer Effects of thermal area, shortened residence time, and broadened elastic range

Active Publication Date: 2020-03-17
FUZHOU UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, in the devices and processes involved in the prior art, the effective heat transfer area of ​​the evaporator is small, the surface renewal frequency of the material is too low, the material evaporation or vaporization interface is too small, the evaporation speed is slow, and the production capacity per unit volume of the equipment is low, etc. Technical defects; the existing devices can handle a narrow range of elasticity, which means that they cannot be applied to both low-viscosity materials and high-viscosity materials; in addition, existing devices and technologies are difficult to handle more than one million centipoise super viscous material

Method used

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  • Transfer reaction device and method for high-viscosity material
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  • Transfer reaction device and method for high-viscosity material

Examples

Experimental program
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Effect test

Embodiment 1

[0027] Such as figure 1 and image 3 As shown, a high-viscosity material transfer and reaction device includes a housing 1, a hollow shaft assembly 2, a column-shaped dispersion assembly 3 composed of hollow tubes, and the like. The shell 1 is a jacket shell, the upper part of the shell 1 is provided with a material inlet 6, and the lower part of the shell 1 is provided with a material outlet 5. The hollow shaft assembly 2 is arranged inside the housing 1, one end is rotatably connected to the upper end surface of the housing, and the other end is rotatably connected to the lower end surface of the housing.

[0028] The hollow shaft assembly includes a hollow shaft, and also includes a separator 4 separating the hollow shaft into a liquid inlet section and a liquid return section, and the liquid inlet section and the liquid return section are indirectly connected through the heat exchange pipe network. The heat exchange pipe network is divided into a liquid inlet heat exchan...

Embodiment 2

[0033] Such as figure 2 As shown, a high-viscosity material transfer and reaction device includes a housing 1, a hollow shaft assembly 2, a column-shaped dispersion assembly 3 composed of hollow tubes, and the like. The shell 1 is a jacket shell, the upper part of the shell 1 is provided with a material inlet 6, and the lower part of the shell 1 is provided with a material outlet 5. The hollow shaft assembly 2 is arranged inside the casing 1, one end is rotatably connected to the upper end surface of the casing, and the other end is suspended in the air.

[0034] The hollow shaft assembly includes an outer tube 14 and an inner tube 15 coaxially set, one of the outer tube and the inner tube is a liquid inlet pipe, and the other is a liquid return pipe, and the liquid inlet pipe and the liquid return pipe The lengths of the pipes are inconsistent; the liquid inlet pipe is connected 9 with the heat exchange medium inlet 7 through the first rotary joint, and the liquid outlet pi...

Embodiment 3

[0039]In this embodiment, maltose is used as the test material, and the heating medium is hot water to concentrate the maltose. The initial temperature of the test medium is 25°C, the outlet temperature is 80°C, the temperature rise is 55°C, vacuum operation is adopted, and the pressure is 500Pa. Other structures of this example are the same as those of Embodiment 1. Keeping the test material, heating medium and test conditions unchanged, and taking the test results of the common scraper type thin film evaporator as the reference group, this embodiment can increase the effective heat transfer area by at least 5 times, and the residence time is the original 1 / 20 of that, the renewal frequency of the material surface is greatly increased, the material evaporation or vaporization interface is too small, the heat transfer rate is increased by more than 3 times, and the production capacity per unit volume of equipment is increased by more than 5 times.

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Abstract

Relating to the field of material transfer equipment and reactors, the invention discloses a transfer and reaction device of a high-viscosity material. The transfer and reaction device comprises a jacket shell, a hollow shaft assembly and a dispersion assembly. The dispersion assembly rotates around the hollow shaft assembly in the shell, and is composed of a plurality of heat exchange pipe networks. The invention also provides a mass transfer method of a high-viscosity material. The heat exchange pipe networks with a high specific surface area rotate in an accommodating chamber holding the high-viscosity material, a heat conduction medium in the heat exchange pipe networks are distributed in the heat exchange pipe networks in an accelerated mode under the action of a centrifugal force, and ducts of the heat exchange pipe networks are communicated with an outer cooling system; and the high-viscosity material is thrown from the inner side of the dispersion assembly to the outer side through the rotary heat exchange pipe networks under the action of centrifugal force. The device and method provided by the invention have the beneficial effects of: increasing the effective heat transfer area, shortening the material retention time, broadening the elastic range of treated materials, treating super-viscous materials, reducing material coking, increasing the productivity, and increasing the equipment productivity.

Description

technical field [0001] The invention relates to the field of material heat and mass transfer and reactors, in particular to a high-viscosity material transfer and reaction device and method. Background technique [0002] There are many types and styles of evaporators, heat exchangers and reactors used in chemical, pharmaceutical and food processing processes today. Because high-viscosity materials have the characteristics of high viscosity, poor fluidity, and large changes in physical properties with temperature (viscosity-temperature characteristics), ordinary evaporators, heat exchangers and reactors have low thermal efficiency, long residence time, and Due to problems such as huge equipment, some evaporators, heat exchangers and reactors for high-viscosity materials have been continuously developed. Manufacturers include: B1awknox, Chemtron, Contro and Plandler in the United States, Luwa in Switzerland, Hitachi Manufacturing in Japan, Nissho Machinery, Sakura Manufacturi...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01J19/18B01D1/00B01D1/22B01J19/00
CPCB01J19/1887B01J19/0053B01J19/0013B01D1/223B01D1/0011B01J2219/00081Y02P20/10
Inventor 严佐毅范文龙郑辉东
Owner FUZHOU UNIV
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