A kind of epoxy resin modified high temperature resistant polyurethane potting glue
A technology of epoxy resin and high temperature resistance, applied in the field of potting glue, can solve the problems of cumbersome and inconvenient operation, affecting the use, and high viscosity of the final polymerization product, and achieves good heat resistance, good low temperature resistance and good processing performance. Effect
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[0059] A second aspect of the present invention provides a method for preparing the epoxy resin-modified high-temperature-resistant polyurethane encapsulant, comprising the following steps:
[0060] (1) Prepare component A earlier;
[0061] (2) Blend component A and component B in step (1), pour into a mold, solidify and form, and obtain the product.
[0062] Preferably, the preparation method of the epoxy resin-modified high-temperature-resistant polyurethane encapsulant comprises the following steps:
[0063] (1) Preparation of component A: Add the polyether epoxy resin into the reaction mixer, the stirring rate is 120-300r / min, the temperature is controlled at 90-130°C, the vacuum degree is -0.1-0MPa, and the stirring and dehydration is 1-4h ;
[0064] (2) Add isocyanate and the first component catalyst to step (1), control the temperature at 120-160° C., vacuum degree at -0.1-0 MPa, stirring rate at 120-300 r / min, and stir for 2-5 hours;
[0065] (3) Add component B to ...
Embodiment 1
[0068] Embodiment 1 of the present invention provides an epoxy resin-modified high-temperature-resistant polyurethane encapsulant. In parts by weight, the preparation raw materials include component A and component B; wherein, component A includes 60 parts of polyether epoxy Resin, 90 parts of isocyanate and 3 parts of the first component catalyst; B component includes polyol and 2 parts of the second component catalyst; the weight ratio of A component to B component is 6:1;
[0069] The polyether epoxy resin is 663 epoxy resin, DER663U;
[0070] The isocyanate is toluene diisocyanate;
[0071] The polyol is 7001 of Vertellus;
[0072] Both the first component catalyst and the second component catalyst are 1-methylimidazole;
[0073] The preparation method of the high temperature resistant polyurethane potting glue modified by epoxy resin comprises the following steps:
[0074] (1) Preparation of component A: Add the polyether epoxy resin into the reaction mixer, the stirri...
Embodiment 2
[0078] Embodiment 2 of the present invention provides an epoxy resin-modified high-temperature-resistant polyurethane potting glue. In parts by weight, the preparation raw materials include component A and component B; wherein, component A includes 10 parts of polyether epoxy Resin, 30 parts of isocyanate and 0.01 part of the first component catalyst; B component includes polyol and 0.05 part of the second component catalyst; the weight ratio of A component to B component is 1:1;
[0079] The polyether epoxy resin is 663 epoxy resin, DER663U;
[0080] The isocyanate is toluene diisocyanate;
[0081] The polyol is 7001 of Vertellus;
[0082] Both the first component catalyst and the second component catalyst are 1-methylimidazole;
[0083] The preparation method of the high temperature resistant polyurethane potting glue modified by epoxy resin comprises the following steps:
[0084] (1) Preparation of component A: Add the polyether epoxy resin into the reaction mixer, the s...
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