Electrostatic image developing toner and image forming method
An electrostatic image development and toner technology, which is applied in the directions of developers, electrographics, instruments, etc., can solve the problems of low image intensity, insufficient reduction of toner image viscosity, weakened softening effect, etc., to promote softening, Fusing Strength Guaranteed Effect
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Synthetic example 1
[0112]
[0113] For example, as shown in the following reaction formula A, 4-aminophenol and sodium nitrite are reacted under cooling to generate a diazonium salt, which is reacted with o-cresol to synthesize intermediate A (the first stage), and then the n-bromine Hexane reacts with intermediate A to obtain the azobenzene derivative (1).
[0114] [chemical formula 4]
[0115]
[0116] In the reaction formula A, by changing the raw materials used (4-aminophenol, o-cresol, n-bromohexane, etc.) into other compounds, the R represented by the general formula (1) can be obtained. 1 and R 6 Azobenzene derivatives of alkoxy groups. Those skilled in the art can synthesize desired azobenzene derivatives by appropriately making the above modifications. In addition, through the preparation method, an azobenzene derivative having an asymmetric structure can be easily obtained.
Synthetic example 2
[0117]
[0118] As shown in the following reaction formula B, the azobenzene derivative (4) can be obtained by changing o-cresol and n-bromohexane into 2-bromophenol and n-bromododecane, respectively.
[0119] [chemical formula 5]
[0120] Reaction (B)
[0121]
Synthetic example 3
[0122]
[0123] As shown in the following Reaction Formula C, the azobenzene derivative (5) can be obtained by reacting the azobenzene derivative (4) with methanol in the presence of a Pd catalyst and an alkali salt.
[0124] [chemical formula 6]
[0125] (Reaction C)
[0126]
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