Flexible intelligent dimming film with high visible light transmittance and heat insulation and preparation method of film
An intelligent dimming and visible light technology, which is applied in optics, nonlinear optics, ion implantation plating, etc., can solve the problems of low transmittance and large-area uniformity of light-adjusting films, so as to improve visible light transmittance and suppress The effect of interface reflection
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[0035] The present invention also provides a method for preparing the above-mentioned flexible intelligent light-adjusting film, which includes the following steps:
[0036] A) Prepare two transparent substrates respectively, compound oxide layer, ultra-thin metal layer and oxide layer on the surface of said transparent substrate in sequence to obtain two flexible transparent conductive electrodes;
[0037] B) The oxide layer surfaces of the two flexible transparent conductive electrodes are coated with polymer-dispersed liquid crystals and superimposed, followed by a curing reaction, to obtain a flexible smart light-adjusting film with high visible light transmission and heat insulation.
[0038] The present invention first prepares two transparent substrates, and then composites an oxide layer, an ultra-thin metal layer and an oxide layer on the surface of the transparent substrate in sequence. Among them, the composite method is not particularly limited, and the winding magnetron ...
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[0043] Example 1
[0044] Step 1: Choose flexible transparent PET with a thickness of 125μm as the base layer;
[0045] Step 2: Using winding magnetron sputtering method to deposit laminated electrodes on the PET substrate. Both bottom and top oxides are Nb 2 O 5 , The thickness is 20-60nm, preferably 35nm; the metal layer is a Cu-doped Ag layer, the thickness is 6-18nm, preferably the thickness is 13nm, where the atomic ratio of Cu and Ag is 1:99-10:90, The preferred ratio is 5:95. Obtained PET / Nb 2 O 5 / Ag-Cu / TiO 2 The sheet resistance of the laminated electrode is 5.2Ω / sq, the average transmittance of visible light (400-800nm) is 85.1% (including the substrate), and the laminated electrode has excellent mechanical flexibility;
[0046] Step 3: Prepare polymer dispersed liquid crystal. Mix NOA65 ultraviolet curing adhesive, LC E7 liquid crystal and silica beads uniformly, and silica beads with a diameter of 20μm are used as fillers to control the thickness of the PDLC device;
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Example Embodiment
[0048] Example 2
[0049] Step 1: Choose flexible transparent PET with a thickness of 125μm as the base layer;
[0050] Step 2: Adopt winding magnetron sputtering method to deposit laminated electrodes on PET substrate. Both bottom and top oxides are Nb 2 O 5 , The thickness is 20-60nm, preferably 35nm; the metal layer is a Cu-doped Ag layer, the thickness is 6-18nm, preferably the thickness is 11nm, where the atomic ratio of Cu and Ag is 1:99-10:90, The preferred ratio is 5:95. Obtained PET / Nb 2 O 5 / Ag-Cu / TiO 2 The sheet resistance of the laminated electrode is 6.4Ω / sq, the average visible light transmittance (400-800nm) is 85.2% (including the substrate), and the laminated electrode has excellent mechanical flexibility;
[0051] Step 3: Prepare polymer dispersed liquid crystal. Mix NOA65 ultraviolet curing adhesive, LC E7 liquid crystal and silica beads uniformly, and silica beads with a diameter of 20μm are used as fillers to control the thickness of the PDLC device;
[0052] S...
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