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Fluidized-bed photocatalytic nitrogen fixation reactor

A photocatalysis and reactor technology, applied in chemical instruments and methods, chemical/physical processes, etc., can solve the problems of insufficient contact, small contact area between catalysts and reactants, and achieve full contact, compact structure, and light energy. High utilization effect

Pending Publication Date: 2020-09-29
YANAN UNIV
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  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] The purpose of the present invention is to provide a fluidized bed photocatalytic nitrogen fixation reactor, which solves the problem of catalyst recovery in existing mechanically stirred reactors and the problems of small contact area and insufficient contact between catalyst and reactants in fixed bed reactors

Method used

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  • Fluidized-bed photocatalytic nitrogen fixation reactor

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Embodiment Construction

[0019] The present invention will be described in detail below in conjunction with the accompanying drawings and specific embodiments.

[0020] A kind of fluidized bed photocatalytic nitrogen fixation reactor of the present invention, as figure 1 As shown, it includes a cylinder 10, the upper end of the cylinder 10 is fixedly connected with a flange 14, the flange 14 is connected with a flat head 11 through bolts 15 and nuts 16, and the lower end of the cylinder 10 is connected with an oval head 7; The upper part of the body 10 is provided with a liquid outlet 13, the flat head 11 is provided with a gas outlet 1, and the elliptical head 7 is provided with a liquid inlet 5 and a gas inlet 6; inside the cylinder 10, there are a plurality of circular holes evenly distributed up and down. The separators 3 are connected by a plurality of vertically arranged first support tubes 8 between every two separators 3 , and a spherical micropearlescent catalyst 2 is placed between every two...

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Abstract

The invention discloses a fluidized-bed photocatalytic nitrogen fixation reactor. The fluidized-bed photocatalytic nitrogen fixation reactor comprises a cylinder, wherein the upper end of the cylinderis connected with a flat plate end socket through a flange, the lower end of the cylinder is connected with an oval end socket, a liquid outlet is formed in the cylinder, a gas outlet is formed in the flat plate end socket, and a liquid inlet and a gas inlet are formed in the oval end socket; and a plurality of circular partition plates are evenly distributed in the cylinder, LED lamp beads are installed on the partition plates, every two partition plates are connected through a supporting pipe, and a spherical micro-pearlescent catalyst is placed between every two partition plates. The fluidized-bed photocatalytic nitrogen fixation reactor disclosed by invention overcomes the problems of a small contact area and insufficient contact between reactants and catalysts in existing equipment and the problem of difficulty in catalyst recovery; the LED lamp beads are used as a light source and are arranged on the partition plates in a concentric circle manner, so illumination is uniform, anda light energy utilization rate is high; and the reactor is simple in structure, the LED lamp beads and the spherical catalyst are easy to disassemble, assemble and replace, and maintenance is convenient.

Description

technical field [0001] The invention belongs to the technical field of catalytic reaction equipment, in particular to a fluidized bed photocatalytic nitrogen fixation reactor. Background technique [0002] Ammonia is an indispensable and important raw material for industrial and agricultural production in modern society. At present, industrial ammonia synthesis is carried out through the Haber process, which requires high pressure (15-25MPa) and high-temperature (673-873K) conditions, and the process is complicated, and the raw material is pure N 2 and pure H 2 , consumes a lot of energy, and also produces a large amount of carbon dioxide, so it is of great significance to seek new technologies for the synthesis of ammonia that are environmentally friendly and energy-saving. [0003] Compared with industrial ammonia synthesis technology, photocatalytic nitrogen fixation (synthetic ammonia) technology has significant advantages: (1) It can be carried out under normal temper...

Claims

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Application Information

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IPC IPC(8): B01J8/24
CPCB01J8/24
Inventor 郭莉王丹军付峰王记江余尚乐王锋郑普胡德艳张媛媛王英仙石天鹏
Owner YANAN UNIV
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