Linden-containing polyamide fiber and preparation method thereof
A nylon fiber and bodhi technology is applied in the field of bodhi-containing nylon fiber and its preparation, which can solve the problems of poor compatibility and unsatisfactory nylon fiber distribution effect, and achieves good compatibility, not easy to contaminate, and good modification effect. Effect
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Embodiment 1
[0044]A preparation method of bodhi-containing nylon fiber includes preparation of molecular nest, preparation of molecular nest containing Bodhi extract, preparation of functional masterbatch, spinning and post-processing.
[0045]The preparation of the molecular nest includes the preparation of precursors, solvent volatilization, molecular nest shaping and modification.
[0046]For the preparation of the precursor, a predetermined number of F127 (polyoxyethylene-polyoxypropylene-polyoxyethylene triblock copolymer), deionized water, formic acid and hydrochloric acid are sequentially added to a predetermined number of THF (tetrahydrofuran) , Stir at 100RPM for 20min until it is completely dissolved, forming a clear and transparent solution. Under 400RPM stirring conditions, add a predetermined portion of TBOT (n-butyl titanate) dropwise, continue to stir for 30 minutes, the solution becomes a clear and transparent golden yellow solution.
[0047]The weight ratio of THF: F127: deionized water...
Embodiment 2
[0082]A preparation method of bodhi-containing nylon fiber includes preparation of molecular nest, preparation of molecular nest containing Bodhi extract, preparation of functional masterbatch, spinning and post-processing.
[0083]The preparation of the molecular nest includes the preparation of precursors, solvent volatilization, molecular nest shaping and modification.
[0084]For the preparation of the precursor, a predetermined number of F127 (polyoxyethylene-polyoxypropylene-polyoxyethylene triblock copolymer), deionized water, formic acid and hydrochloric acid are sequentially added to a predetermined number of THF (tetrahydrofuran) , Stir at 130RPM for 30min until it is completely dissolved, forming a clear and transparent solution. Under 500RPM stirring conditions, add a predetermined amount of TBOT (n-butyl titanate) dropwise, continue to stir for 40 minutes, the solution becomes a clear and transparent golden yellow solution.
[0085]The weight ratio of THF: F127: deionized water:...
Embodiment 3
[0120]A preparation method of bodhi-containing nylon fiber includes preparation of molecular nests, preparation of molecular nests containing Bodhi extract, preparation of functional master batches, spinning, and post-processing.
[0121]The preparation of the molecular nest includes the preparation of precursors, solvent volatilization, molecular nest formation and modification.
[0122]For the preparation of the precursor, a predetermined number of F127 (polyoxyethylene-polyoxypropylene-polyoxyethylene triblock copolymer), deionized water, formic acid and hydrochloric acid are sequentially added to a predetermined number of THF (tetrahydrofuran) , Stir at 150RPM for 30min until it is completely dissolved, forming a clear and transparent solution. Under 500RPM stirring conditions, add a predetermined number of TBOT (n-butyl titanate) dropwise, continue to stir for 40 minutes, the solution becomes a clear and transparent golden yellow solution.
[0123]The weight ratio of THF: F127: deionize...
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