Device and method for preparing graphene composite particles
A graphene composite and preparation device technology, applied in chemical instruments and methods, carbon compounds, inorganic chemistry, etc., can solve problems such as waste of resources, difficulty in particle screening, poor preparation effect, etc., and achieve the effect of improving fluidity
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Embodiment 1
[0046] see Figure 1-8 , a graphene composite microparticle preparation device, which includes a feeding device 1 for adding a variety of raw materials, directly below the feeding device 1 is provided with a drum stirring device 2 for stirring the raw materials, and the drum stirring device 2 A stirring and evaporating device 3 is provided directly below the stirring and evaporating device 3, and a freeze-drying and screening system 4 is provided directly below the stirring and evaporating device 3; the freeze-drying and screening system 4 includes a freeze-drying and sieving device 25 and a screening 24; The side of the freeze-drying and screening system 4 is provided with a collection system 5 . The device with the above structure can be used for the preparation of graphene composite particles. Through the above preparation device, the graphene composite particles have good dispersion, fluidity, and standardized particle size, so that graphene can be effectively and evenly w...
Embodiment 2
[0055] A method for preparing graphene composite particles using a graphene composite particle preparation device, comprising the following steps:
[0056] Step 1, adding raw materials: adding corresponding amounts of absolute ethanol, core particles and graphene powder to the inside of the absolute ethanol feeding device 6, the particle feeding device 7 and the graphene feeding device 8 according to the mixing ratio;
[0057] Step 2, mixing and stirring the raw materials: put the liquid and powder prepared in step 1 into the inside of the drum stirring device 2 after feeding, start the first rotating motor 10 and the first ultrasonic motor 14 to drive the corresponding stirring spindle, During the stirring process, the particles are disturbed longitudinally by the vertical stirring bar 13, and the particles are disturbed horizontally by the horizontal stirring plate 12, and finally the particles are fully dispersed in the absolute ethanol solution;
[0058] Step 3, heating an...
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