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Method for judging adulteration of goat milk formula milk powder

A technology for formula milk powder and goat milk, applied in the field of food science, can solve the problems of the health threat of cow milk allergy consumers, the damage to consumers' economic interests, and the high cost of raw materials, and achieve the effects of low detection limit, intuitive results and convenient operation.

Pending Publication Date: 2021-03-30
BEIJING TECHNOLOGY AND BUSINESS UNIVERSITY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the yield of goat milk is low, the cost of raw materials is high, and it is affected by seasonal changes. Therefore, manufacturers are driven by economic interests to mix lower-priced, higher-yield cow’s milk powder into goat milk formula milk powder. appear frequently
This kind of adulteration not only damages the economic interests of consumers, but also poses a threat to the health of consumers with milk allergies.

Method used

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  • Method for judging adulteration of goat milk formula milk powder
  • Method for judging adulteration of goat milk formula milk powder
  • Method for judging adulteration of goat milk formula milk powder

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0057] This example relates to an effective identification method for goat milk formula milk powder adulterated cow milk powder, and mainly involves the establishment of the fingerprint library, OPLS-DA score scatter diagram and VIP map of aroma compounds in unadulterated goat milk and cow milk formula milk powder , and the establishment of indicator aroma compounds.

[0058] 1. Establishment of fingerprint library of aroma compounds in unadulterated goat milk and cow milk formula

[0059] (1) Y1, Y2, Y3, Y4, Y5 and Y6 are used as standard products for unadulterated goat milk formula milk powder; N1, N2, N3, N4, N5 and N6 are used as standards for unadulterated milk formula milk powder Taste.

[0060] (2) Handling of materials

[0061] Weighing 0.6g of goat milk and cow's milk formula milk powder was dissolved in water, and the volume was adjusted to 4ml to obtain a formula milk powder hydrolyzate.

[0062] (3) Reagents and instruments

[0063] N-hexane was purchased from ...

Embodiment 2

[0091] This example relates to the discrimination of adulterated milk powder mixed with different proportions of cow's milk formula in goat's milk formula milk powder. Principal component analysis (PCA) of samples.

[0092] 1) The detection of adulterated samples is based on a kind of unadulterated goat milk formula milk powder in Example 1, and a kind of cow's milk with 5%, 10%, 20%, 40%, 80% of the total weight respectively The formula replaces the same weight of unadulterated goat's milk formula, simulating the goat's milk adulterated milk powder artificially added with cow's milk formula. The sample processing and data analysis methods are the same as in Example 1, and the composition of the indicator aroma compounds in the obtained sample of this example is shown in Table 3. It is further proved that in the actual detection process, it is accurate to determine whether the goat milk formula milk powder is adulterated by detecting the indicator aroma compounds, and it can ...

Embodiment 3

[0099] This example relates to the identification of adulteration of a goat milk formula mixed with different types of cow milk formula, the comparison of the main adulterated milk powder and the non-adulterated goat milk and cow milk formula index aroma compounds and adulterated samples PCA analysis.

[0100] 1) Detection of adulterated samples Using the unadulterated goat milk formula milk powder in Example 1 as the substrate, replace the unadulterated goat milk formula milk powder of the same weight with 5% of the total weight of different varieties of cow milk formula milk powder respectively Milk powder, simulating goat milk adulterated milk powder artificially added with cow milk formula. The sample processing and data analysis methods are the same as in Example 1, and the composition of the indicator aroma compounds in the obtained sample of this example is shown in Table 4. It is accurate to determine whether goat milk formula is adulterated by detecting indicator aro...

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Abstract

The invention aims to provide a convenient method for detecting adulteration of goat milk formula milk powder. The method can accurately judge whether adulteration milk powder of milk powder is addedinto the goat milk formula milk powder or not, or the goat milk formula milk powder does not contain goat milk and is pretended by milk. The method comprises the following steps of by adopting a gas chromatography method, establishing a fingerprint spectrum library of aroma compounds in unadulterated goat milk formula milk powder and a fingerprint spectrum library of aroma compounds in an unadulterated cow milk formula milk powder, screening out characteristic aroma compounds in the unadulterated goat milk and cow milk formula milk powder, and determining the index aroma compound for identifying the goat milk formula milk powder by utilizing least square discriminant analysis. The detected aroma compounds in a sample to be detected are compared with index aroma compounds in the unadulterated goat milk and cow milk formula milk powder, whether the sample to be detected contains the goat milk or not can be determined, whether the sample to be detected is adulterated or not can be determined, and judgment can be carried out more visually and quickly by combining a principal component analysis method.

Description

technical field [0001] The invention belongs to the field of food science and technology, and particularly relates to a method for identifying whether goat milk formula milk powder is adulterated. Background technique [0002] Infants and young children are a special group, and breast milk is the most ideal food for infants and young children. Breast milk not only provides a source of nutrition, but also contains biological components that promote the normal growth and development of infants. However, due to various reasons, the breastfeeding rate of infants and young children is decreasing year by year. In the case of no breast milk or insufficient breast milk, infant formula milk powder has become the most important daily food source for infants and young children as a substitute for breast milk. [0003] The research and production of infant formula milk powder in my country started relatively late, and currently infant formula milk powder is mainly based on cow's milk. ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N30/02G01N30/06G01N30/30G01N30/34G01N30/72G01N30/86
CPCG01N30/02G01N30/06G01N30/30G01N30/34G01N30/7206G01N30/8686G01N2030/045G01N2030/062
Inventor 宋焕禄于明光汤龙
Owner BEIJING TECHNOLOGY AND BUSINESS UNIVERSITY
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