Method for judging adulteration of goat milk formula milk powder
A technology for formula milk powder and goat milk, applied in the field of food science, can solve the problems of the health threat of cow milk allergy consumers, the damage to consumers' economic interests, and the high cost of raw materials, and achieve the effects of low detection limit, intuitive results and convenient operation.
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Embodiment 1
[0057] This example relates to an effective identification method for goat milk formula milk powder adulterated cow milk powder, and mainly involves the establishment of the fingerprint library, OPLS-DA score scatter diagram and VIP map of aroma compounds in unadulterated goat milk and cow milk formula milk powder , and the establishment of indicator aroma compounds.
[0058] 1. Establishment of fingerprint library of aroma compounds in unadulterated goat milk and cow milk formula
[0059] (1) Y1, Y2, Y3, Y4, Y5 and Y6 are used as standard products for unadulterated goat milk formula milk powder; N1, N2, N3, N4, N5 and N6 are used as standards for unadulterated milk formula milk powder Taste.
[0060] (2) Handling of materials
[0061] Weighing 0.6g of goat milk and cow's milk formula milk powder was dissolved in water, and the volume was adjusted to 4ml to obtain a formula milk powder hydrolyzate.
[0062] (3) Reagents and instruments
[0063] N-hexane was purchased from ...
Embodiment 2
[0091] This example relates to the discrimination of adulterated milk powder mixed with different proportions of cow's milk formula in goat's milk formula milk powder. Principal component analysis (PCA) of samples.
[0092] 1) The detection of adulterated samples is based on a kind of unadulterated goat milk formula milk powder in Example 1, and a kind of cow's milk with 5%, 10%, 20%, 40%, 80% of the total weight respectively The formula replaces the same weight of unadulterated goat's milk formula, simulating the goat's milk adulterated milk powder artificially added with cow's milk formula. The sample processing and data analysis methods are the same as in Example 1, and the composition of the indicator aroma compounds in the obtained sample of this example is shown in Table 3. It is further proved that in the actual detection process, it is accurate to determine whether the goat milk formula milk powder is adulterated by detecting the indicator aroma compounds, and it can ...
Embodiment 3
[0099] This example relates to the identification of adulteration of a goat milk formula mixed with different types of cow milk formula, the comparison of the main adulterated milk powder and the non-adulterated goat milk and cow milk formula index aroma compounds and adulterated samples PCA analysis.
[0100] 1) Detection of adulterated samples Using the unadulterated goat milk formula milk powder in Example 1 as the substrate, replace the unadulterated goat milk formula milk powder of the same weight with 5% of the total weight of different varieties of cow milk formula milk powder respectively Milk powder, simulating goat milk adulterated milk powder artificially added with cow milk formula. The sample processing and data analysis methods are the same as in Example 1, and the composition of the indicator aroma compounds in the obtained sample of this example is shown in Table 4. It is accurate to determine whether goat milk formula is adulterated by detecting indicator aro...
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