Liquid-phase synthesis auxiliary system
An auxiliary system, liquid-phase synthesis technology, applied in chemical/physical/physicochemical processes, chemical/physical/physicochemical processes of energy application, chemical instruments and methods, etc., can solve the problem of unsafe ultraviolet light utilization, difficult Instrument assembly and other issues, to achieve the effect of improving the utilization rate of ultraviolet light, increasing the heat preservation effect, and easy assembly
Pending Publication Date: 2021-04-27
PEKING UNIV
View PDF6 Cites 1 Cited by
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
This method is easy to control the temperature and is stable. The synthesis effect of the model reaction is the same as the previous side-illumination method in the laboratory, or even slightly better, but it still needs to cool down the cold trap and open the low-temperature circulation device of the cold trap. It is not easy to assemble the instrument and is not safe. And the utilization rate of ultraviolet light is very low, and additional ultraviolet protection devices are required
Method used
the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View moreImage
Smart Image Click on the blue labels to locate them in the text.
Smart ImageViewing Examples
Examples
Experimental program
Comparison scheme
Effect test
Embodiment Construction
[0030]Next, the technical solutions in the embodiments of the present invention will be apparent from the embodiment of the present invention, and it is clearly described, and it is understood that the described embodiments are merely embodiments of the present invention, not all of the embodiments. Based on the embodiments of the present invention, there are all other embodiments obtained without making creative labor without making creative labor premises.
[0031]It is an object of the present invention to provide a liquid phase synthetic assist system having a feature of temperature control, easy assembly, etc., while improving the ultraviolet utilization rate during the experimental irradiation.
[0032]In order to make the above objects, features, and advantages of the present invention, the present invention will be further described in detail below with reference to the accompanying drawings and specific embodiments.
[0033]figure 1 Structure of the liquid phase synthetic auxiliary ...
the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More PUM
Login to View More Abstract
The invention relates to a liquid-phase synthesis auxiliary system. The liquid-phase synthesis auxiliary system comprises a novel reactor, a mixing device, a temperature control device and an upper computer. According to the invention, the novel reactor is arranged on the mixing device, and the mixing device and the temperature control device are electrically connected with the upper computer, so that the whole liquid-phase synthesis auxiliary system is stable in program temperature control and temperature control and easy to assemble; and the bottle body of the novel reactor sequentially comprises a reaction liner, a temperature circulating layer and a vacuum layer from inside to outside, so that the heat preservation effect can be further improved, and the ultraviolet light utilization rate in the experiment irradiation process can be remarkably improved if an illumination reaction is carried out.
Description
Technical field[0001]The present invention relates to the field of experimental equipment, and more particularly to a liquid phase synthetic auxiliary system.Background technique[0002]During the existing experimental liquid phase synthesis, agitation and temperature control are key factors affecting the experimental effect. General liquid phase experiments generally use water bath or oil temperature control, it is difficult to do programs to cool down, and need human control and regulation The speed requires the operator to take a long time, so if you can automate the temperature and the control speed will perfectly liberate your hands and improve efficiency. Also, in particular, there is a plurality of quartz reactors to carry out solution reactions when the illumination reaction is used, and the experiment is carried out in a manner in which the side is taken in the low temperature tank of the -80 ° C. During the side, a cold trace of a long arc-mercury lamp light source and a qua...
Claims
the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More Application Information
Patent Timeline
Login to View More IPC IPC(8): B01J19/24B01J19/12
CPCB01J19/24B01J19/123B01J2219/00094B01J2219/00153B01J2219/00011B01J19/18B01J2219/00689B01J19/0066
Inventor 叶新山姚文龙熊德彩
Owner PEKING UNIV